• Journal of the Korean Society of Safety
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• v.24 no.3
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• pp.1-6
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• 2009

Recently power plants and oil refineries are focusing on capacity enlargement for better efficiency through higher temperature and higher pressure. Thickness of boiler tubes becomes lessened due to oxidation and erasion caused by high temperature bums gas flowing over tubes outside. Accordingly, mechanical stress of tubes is increasing and that is a critical factor to make a crack and fracture. To prevent those sorts of accidents, aging assessment for proper periodic repair and replacement should be conducted reliably and reasonably. We performed IIT test on Cr-Mo steel, one of the most heat-resistant materials for facilities in power plants, and we report the test result and the considerable effectiveness of IIT test.

• Proceedings of the KSME Conference
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• 2001.06a
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• pp.231-236
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• 2001

A newly developed Advanced Indentation System (AIS), which is a portable and nondestructive system for evaluating tensile properties, was used to measure mechanical behavior of materials used under high temperature and pressure conditions. This test measures indentation load-depth curve during indentation and analyzes the mechanical properties related to deformation and fracture. Aging effects of Cr-Mo and Cr-Mo-V steel at high temperature were simulated. Tensile properties including yield strength and tensile strength at various temperature are obtained from the test. For all test materials and conditions, the AIS-derived results were in good agreement with those from conventional standard test method. Examples of the test results ate given and potential applications of the AIS to assess the integrity of aging structures are briefly discussed.

• Journal of the Korean Society for Heat Treatment
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• v.7 no.3
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• pp.190-198
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• 1994

In order to study the effect of retained austenite on rolling contact fatigue in high-carbon chromium bearing steel, retained austenite was controlled by only tempering temperature, individually 200, 220 and $240^{\circ}C$. Among various microstructural alteration during rolling contact fatigue test, plate-like carbide most related to the flaking at sub-surface of contact pressure. The plate-like carbides formed during rolling contact fatigue test decrease with increasing tempering temperature, and fatigue life is much more improved. The retained austenite was decreased with the tempering temperature, and that decreased plate-like carbide formation. Therefore fatigue life is much more improved with decreasing retained austenite.

• Journal of Surface Science and Engineering
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• v.50 no.4
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• pp.272-276
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• 2017

The response of AISI 310 type austenitic stainless steel to the novel low temperature plasma carburizing process has been investigated in this work. This grade of stainless steel shows better corrosion resistance and high temperature oxidation resistance due to its high chromium and nickel content. In this experiment, plasma carburizing was performed on AISI 310 stainless steel in a D.C. pulsed plasma ion nitriding system at different temperatures in $H_2-Ar-CH_4$ gas mixtures. The working pressure was 4 Torr (533Pa approx.) and the applied voltage was 600 V during the plasma carburizing treatment. The hardness of the samples was measured by using a Vickers micro hardness tester with the load of 100 g. The phase of carburized layer formed on the surface was confirmed by X-ray diffraction. The resultant carburized layer was found to be precipitation free and resulted in significantly improved hardness and corrosion resistance.

• Journal of Powder Materials
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• v.10 no.3
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• pp.168-171
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• 2003

Interpenetrating phase composites of $TiB_2$-Cu system were produced via Spark-Plasma Sintering (SPS) oi nanocomposite powders. Under simultaneous action of pressure, temperature and electric current titanium diboride nanoparticles distributed in copper matrix move, agglomerate and form a fine-grained skeleton. Increasing SPS-temperature and he]ding time promote densification due to local melting of copper matrix When copper melting is avoided the compacts contain 17-20% porosity but titanium diboride skeleton is still formed representing the feature of SPS . High degree of densification and formation of titanium diboride network result in increased hardness of high-temperature SPS-compacts.

• Journal of ILASS-Korea
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• v.2 no.3
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• pp.25-31
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• 1997

This experiment was undertaken to investigate the spray characteristics of the conventional injection system and the ultrasonic energy added injection system. Test fuels include light oil and mixed light-BC oil. The mixed light-BC oil was injected at the normal temperature$(20^{\circ}C)$ and the high temperature$(95{\pm}2^{\circ}C)$ and injection pressure was $120kg/cm^2$. Sauter mean diameter was measured under the variation of the spray distance. To measure the droplet size, we used the Malvern system 2600C. Droplet size distribution was analyzed from the result data of Malvern system. It is also found that the condition of the ultrasonic energy added injection and high temperature injection generates the smaller droplets than that of the conventional injection.

• Journal of the Korean Society of Food Science and Nutrition
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• v.23 no.2
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• pp.238-243
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• 1994

Changes of lipid components in modified oleoresin during cooking at high temperature were investigated. In preparation of the modified oleoresin, dried red pepper was milled to 100 mesh of size particle and extracted oily compounds by reduced pressure steam distillation . The rest part was reextracted and concentrated and concentrated. The extracts were combined. The same volume of water and 4% of polyglycerol condensed ricinoleate (PGDR) were added to the combined extract, and emulsified to make oleresin red pepper. Non-polar lipid components were quantified 3 times higher in the oleoresin than polar lipid components . The components of non-polar lipd was mainly triglyceride comprising 75.8%. The level of phosphatidyl choline and phosphatidyl ethanolamine were 38.6and 26.1%, respectively. linoleic acid was distinctively abundant (63.1%) and followed by palmitic acid, oleic acid, linolenic acid and stearic acid in the oleoresin. Oxidation of lipid at high temperature was principally affected by temperature rather than oxygen existence . With the result of oxidation , palmitic acid and myristic acid increased, however, oleic acid, linoleic acid, and linolenic acid decreased.

• Bulletin of the Korean Chemical Society
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• v.30 no.12
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• pp.2921-2926
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• 2009

Cu-BTC[$Cu_3(BTC)_2(H_2O)_3$, BTC = 1,3,5-benzenetricarboxylate], one of the most well-known metal-organic framework materials (MOF), has been synthesized under atmospheric pressure and room temperature by using ultrasound. The Cu-BTC can be obtained in 1 min in the presence of DMF (N,N-dimethylformamide), suggesting the possibility of continuous production of Cu-BTC. Moreover, the surface area and pore volume show that the concentration of DMF is important for the synthesis of Cu-BTC having high porosity. The morphology and phase also depend on the concentration of DMF : Cu-BTC cannot be obtained at room temperature in the absence of DMF and aggregated Cu-BTC (with low surface area) is produced in the presence of high concentration of DMF. It seems that the deprotonation of benzenetricarboxylic acid by base (such as DMF) is inevitable for the room temperature syntheses.

• Journal of the Korean Society of Combustion
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• v.16 no.2
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• pp.16-22
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• 2011

It is a challenging task to apply large detailed chemical mechanisms of fuel oxidation in simulation of complex combustion phenomena. There exist a few systematic methodologies to reduce detailed chemical mechanisms to smaller sizes involving less computational load. This research work concerns generation of a skeletal chemical mechanism by a directed relation graph with specified accuracy requirement. Two sequential stages for mechanism reduction are followed in a perfectly stirred reactor(PSR) for high temperature chemistry and to consider the autoignition delay time for low and high temperature chemistry. Reduction was performed for the detailed chemical mechanism of n-heptane consisting of 561 species and 2539 elementary reaction steps. Validation results show acceptable agreement for the autoignition delay time and the PSR calculation in wide parametric ranges of pressure, temperature and equivalence ratio.

• Proceedings of the Korean Society of Propulsion Engineers Conference
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• 2010.11a
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• pp.686-691
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• 2010

Flash boiling takes place when the thermodynamic state of the liquid deviates from its saturation limit over which the liquid temperature exceeds by a certain degree of superheat. The liquid jet introduced into the lower pressure zone than the liquid saturation pressure experiences a sequence of the atomization and disintegrated into numerous faster and smaller droplets. In the present study spray characteristics for a flash swirl spray were experimentally investigated. Injectant temperature is raised by a high frequency dielectric heating method and local spray characteristics are instantly measured by Global Sizing Velocimetry (GSV, TSI Inc.). Dependence of dimensionless superheat degree and injection pressure on total and local SMDs and mean droplet size is quantitatively examined. The flash swirl spray has the relation in the injection pressure and nozzle diameter in order to determine the spray quality, including the dimensionless superheat degree. Small droplets occur in the void core and local droplet size distributions largely depend on the dimensionless superheat degree and the injection pressure.