• Title/Summary/Keyword: high temperature high pressure

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Enhancement of cyanoacrylate-developed marks using p-dimethylaminobenzaldehyde (DMAB) on semi-porous surfaces and analysis of the influence factors on fluorescence intensity (반다공성 재질에 유류된 지문의 CA 훈증 후 p-dimethylaminobenzealdehyde(DMAB) 형광시약 적용 시 표면적과 주변 온도, 기압이 형광착색에 미치는 효과에 관한 연구)

  • Yu, Je-Sul;Kim, Ju-Hah
    • Analytical Science and Technology
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    • v.27 no.4
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    • pp.187-195
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    • 2014
  • It is very important to minimize the damage of latent fingerprints at enhancing the contrast. This study proves the enhancement effects of cyanoacrylate-fumed latent fingerprints using p-dimethylaminobenzealdehyde (DMAB) on semi-porous surfaces and the influence factors. The latent fingerprints in experiment were developed for cyanoacrylate treatment in a vacuum chamber and used after drying at room temperature for 24 hours. For fluorescence staining, the cyanoacrylate-developed marks using DMAB were sublimated during 48 hours under the different conditions of surface area, temperature, atmospheric pressure. First experiment showed how surface area effects on the sublimation rate and fluorescence intensity by DMAB of particle size and container size. In addition, the fluorescence staining using DMAB with solvent-free contact method had the greatest fluorescence intensity after 36 hours and a low fluorescence intensity over a certain size of surface area. Second experiment showed that the evaporation of DMAB solid crystals got a satisfying result in a temperature of $20^{\circ}C$ and reduced time to get the greatest fluorescence intensity. It took a long time to get a optimum level of fluorescence intensity at $30^{\circ}C$ or more and it was less effective in fluorescence intensity. Third experiment on the pressure indicated that the fluorescence intensity of vacuum was weaker than nonvacuum but it was inapplicable to very high variations in pressure.

The Low $NO_{x}$ Characteristics of a Lean Premixed Gas Turbine Combustor (희박연소를 이용한 가스터빈 연소기의 저 $NO_{x}$ 특성)

  • Son, M.G.;Ahn, K.Y.;Kim, H.S.;Kim, Y.M.
    • Proceedings of the KSME Conference
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    • 2001.06d
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    • pp.66-70
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    • 2001
  • The combustion characteristics have been investigated to develop the low $NO_{x}$ gas turbine combustor. The lean premixed combustion technology was applied to reduce the $NO_{x}$ emission. Also, the conventional combustor was designed and tested for the baseline of low $NO_{x}$ combustor performance. The test was conducted at the condition of high temperature and ambient pressure. The combustion air which has the temperature of 500K were supplied to the combustor through the air preheater. The temperature and emissions of $NO_{x}$ and CO were measured at the exit of combustor. The premixing chamber can be operated very lean condition of equivalence ratio around 0.35. The $NO_{x}$ was decreased with decreasing the equivalence ration. The CO was decreased with decreasing the equivalence ratio, but the CO was increased with decreasing the equivalence ratio below 0.45. But, at the very lean condition of equivalence ratio below 0.35 both NOx and CO were increased because of the flame unstability. The $NO_{x}$ was decreased slightly and CO was increased with increasing inlet air flowrate. This results can be used to determine the size of combustor. The low $NO_{x}$ combustor has lower values of $NO_{x}$ and CO compared with conventional one. Consequently the performance of combustor shows the possibility of the application to the gas turbine system.

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Properties of Nb-doped TiO2 Transparent Conducting Oxide Film Fabricated by RF Magnetron Sputtering (RF 마그네트론 스퍼터링에 의해 합성된 Nb-doped TiO2 투명전극의 특성)

  • Kim, Min-Young;Cho, Mun-Seong;Lim, Dong-Gun;Park, Jae-Hwan
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.25 no.3
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    • pp.204-208
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    • 2012
  • $TiO_2$ ($Ti_{1-x}Nb_xO_2$, x= 0.04~0.06) transparent conducting oxide film was fabricated by RF magnetron sputtering process and their electrical, optical, stability properties were studied. When the Nb 4 at% sputtering target was used with RF power 120 W, pressure 8 mTorr, post-annealing temperature $600^{\circ}C$, the resistivity of TNO film was $4{\times}10^{-4}\;{\Omega}-cm$. The optical transmittance in the visible wavelength was ca. 86%. TNO films require heat treatment during or after the deposition process. When the film was deposited at room temperature and post-annealed at $600^{\circ}C$, the lowest resistivity was obtained. When the TNO film was exposed to high temperature and humidity, the resistivity of the film was rather decreased. The stability to temperature and humidity implies that the TNO film could be a appropriate candidate for In-free, ZnO-free transparent conducting oxide materials.

A short-term supranutritional vitamin E supplementation alleviated respiratory alkalosis but did not reduce oxidative stress in heat stressed pigs

  • Liu, Fan;Celi, Pietro;Chauhan, Surinder Singh;Cottrell, Jeremy James;Leury, Brian Joseph;Dunshea, Frank Rowland
    • Asian-Australasian Journal of Animal Sciences
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    • v.31 no.2
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    • pp.263-269
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    • 2018
  • Objective: Heat stress (HS) triggers oxidative stress and respiratory alkalosis in pigs. The objective of this experiment was to study whether a short-term supranutritional amount of dietary vitamin E (VE) can mitigate oxidative stress and respiratory alkalosis in heat-stressed pigs. Methods: A total of 24 pigs were given either a control diet (17 IU/kg VE) or a high VE (200 IU/kg VE; HiVE) diet for 14 d, then exposed to thermoneutral (TN; $20^{\circ}C$, 45% humidity) or HS ($35^{\circ}C$, 35% to 45% humidity, 8 h daily) conditions for 7 d. Respiration rate and rectal temperature were measured three times daily during the thermal exposure. Blood gas variables and oxidative stress markers were studied in blood samples collected on d 7. Results: Although HiVE diet did not affect the elevated rectal temperature or respiration rate observed during HS, it alleviated (all p<0.05 for diet${\times}$temperature) the loss of blood $CO_2$ partial pressure and bicarbonate, as well as the increase in blood pH in the heat-stressed pigs. The HS reduced (p = 0.003) plasma biological antioxidant potential (BAP) and tended to increase (p = 0.067) advanced oxidized protein products (AOPP) in the heat-stressed pigs, suggesting HS triggers oxidative stress. The HiVE diet did not affect plasma BAP or AOPP. Only under TN conditions the HiVE diet reduced the plasma reactive oxygen metabolites (p<0.05 for diet${\times}$temperature). Conclusion: A short-term supplementation with 200 IU/kg VE partially alleviated respiratory alkalosis but did not reduce oxidative stress in heat-stressed pigs.

Evaluation of Heat Processing Temperature and Time on Functional Properties of Garlic Juice

  • Lee, Youn-Ri;Lee, Yun-Kyoung;Hwang, In-Guk;Woo, Koan-Sik;Han, Chung-Su;Jeong, Heon-Sang
    • Preventive Nutrition and Food Science
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    • v.13 no.4
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    • pp.327-333
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    • 2008
  • To develop a functional juice using garlic (Allium sativum L.), heated garlic juice was investigated using a central composite design set with variables of treatment temperature (110, 115, 120, 125, and $130^{\circ}C$) and time (1, 2, 3, 4, and 5 hr) using high temperature and pressure treatment apparatuses. Total soluble solid, total acidity, reducing sugar, total pholyphenol contents, electron donating activity (EDA), and ascorbic acid equivalent antioxidant capacity (AEAC) in heated garlic juice were increased with increasing heating temperature and time. The highest total soluble solid content was $17.81\;^{\circ}brix$ at $123.10^{\circ}C$ for 1.10 hr. The highest total acidity was 1.43% at $127.35^{\circ}C$ for 4.35 hr. The highest reducing sugar content was 86.67 mg/mL at $119.90^{\circ}C$ for 4.35 hr. The highest total polyphenol content was 8.42 mg/mL at $127.75^{\circ}C$ for 4.26 hr. The highest EDA and AEAC were 60.09%, and 7.40 mg AA eq/mL at $127.85^{\circ}C$ for 4.23 hr, and $128.10^{\circ}C$ for 4.18 hr, respectively.

Performance Analysis of Methanol Fueled Marine Solid Oxide Fuel Cell and Gas Turbine Hybrid Power System (메탄올 연료형 SOFC/GT 하이브리드시스템의 성능 평가)

  • Oh, Sae-Gin;Lim, Tae-Woo;Kim, Jong-Su;Kil, Byung-Lea;Park, Sang-Kyun;Kim, Mann-Eung;Lee, Kyung-Jin;Oh, Jin-Suk;Kim, Myoung-Hwan
    • Journal of Advanced Marine Engineering and Technology
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    • v.34 no.8
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    • pp.1040-1049
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    • 2010
  • The strengthened regulations for atmospheric emissions from ships have caused a necessity of new, alternative power system in ships for the low pollutant emissions and the high energy efficiency. Recently, new kinds of propulsion power system such as fuel cell system, which use hydrogen as an energy source, have been sincerely considered. The purpose of this work is to predict the performance of methanol fueled SOFC/GT hybrid power system and to analyze the influence of operating temperature of stack, current density of stack, pressure ratio of turbine, temperature effectiveness of recuperator, turbine inlet temperature.

Prediction of Combined Forced and Natural Turbulent Convection in a Vertical Plane Channel with an Elliptic-Blending Second Moment Closure (타원-혼합 2차모멘트 모형에 의한 강제와 자연대류가 복합된 수직 평판 난류유동의 예측)

  • Shin, Jong Keun;An, Jeong Soo;Choi, Young Don
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.29 no.11 s.242
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    • pp.1265-1276
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    • 2005
  • The elliptic conceptual second moment models for turbulent heat fluxes, which are proposed on the basis of elliptic-blending and elliptic-relaxation equations, are applied to calculate the combined forced and natural turbulent convection in a vertical plane channel. The models satisfy the near-wall balance between viscous diffusion, viscous dissipation and temperature-pressure gradient correlation, and also have the characteristics of approaching its respective conventional high Reynolds number model far away from the wall. Also the models are closely linked to the elliptic blending model which is used for the prediction of Reynolds stress. In order to calibrate the heat flux models, firstly, the distributions of mean temperature and scala flux in fully developed channel flow with constant wall difference temperature are solved by the present models. The buoyancy effect on the turbulent characteristics including the mean velocity and temperature, the Reynolds stress tensor, and the turbulent heat flux vector are examined. In the opposing flow, the turbulent transport is greatly enhanced with both the Reynolds stresses and the turbulent heat fluxes being remarkably increased; whereas, in the aiding flow, the opposite change is observed. The results of prediction are directly compared to the DNS to assess the performance of the model predictions and show that the behaviors of the turbulent heat transfer in the whole flow region are well captured by the present models.

Conversion of Wood Waste into Solid Biofuel Using Catalytic HTC Process (촉매 열수탄화(Hydrothermal carbonization)공정을 이용한 폐목재의 고형연료 제조 및 특성 연구)

  • Joo, Bokyoung;Yeon, Hyejin;Lee, Sangil;Ahn, Soojeung;Lee, Kyeongjae;Jang, Eunsuk;Won, JongChoul
    • New & Renewable Energy
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    • v.10 no.2
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    • pp.12-18
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    • 2014
  • The objective of this work is to produce solid biofuel from sawdust using the HTC (Hydrothermal carbonization) process. The HTC process of feedstock involves the raw material coming into contact with high temperature and pressurized water. The HTC process could produce gaseous, liquefied and solid products, but this study focused on solid product only as an alternative to coal. In this study, sawdust used for a feedstock and its moisture content was under 5%. Water was added with the feedstock to raise moisture content to 80% and also used catalysts. The HTC process was performed at temperature range from 200 to $270^{\circ}C$ and reaction time was 15 to 120 min. Rising temperature resulted in increasing the higher heating value (HHV) of HTC product. In case of adding catalyst, HHV of solid biofuel was higher and reaction occurred at lower temperature and pressure. Also, HTC solid product had been characterized and found to be hydrophobic, increased HHV (over 40%), and pelletized easily compared to raw material.

Low Temperature Hermetic Packaging using Localized Beating (부분 가열을 이용한 저온 Hermetic 패키징)

  • 심영대;김영일;신규호;좌성훈;문창렬;김용준
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2002.10a
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    • pp.1033-1036
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    • 2002
  • Wafer bonding methods such as fusion and anodic bonding suffer from high temperature treatment, long processing time, and possible damage to the micro-scale sensor or actuators. In the localized bonding process, beating was conducted locally while the whole wafer is maintained at a relatively low temperature. But previous research of localized heating has some problems, such as non-uniform soldering due to non-uniform heating and micro crack formation on the glass capsule by thermal stress effect. To address this non-uniformity problem, a new heater configuration is being proposed. By keeping several points on the heater strip at calculated and constant potential, more uniform heating, hence more reliable wafer bonding could be achieved. The proposed scheme has been successfully demonstrated, and the result shows that it will be very useful in hermetic packaging. Less than 0.2 ㎫ contact Pressure were used for bonding with 150 ㎃ current input for 50${\mu}{\textrm}{m}$ width, 2${\mu}{\textrm}{m}$ height and 8mm $\times$ 8mm, 5mm$\times$5mm, 3mm $\times$ 3mm sized phosphorus-doped poly-silicon micro heater. The temperature can be raised at the bonding region to 80$0^{\circ}C$, and it was enough to achieve a strong and reliable bonding in 3minutes. The IR camera test results show improved uniformity in heat distribution compared with conventional micro heaters. For gross leak check, IPA (Isopropanol Alcohol) was used. Since IPA has better wetability than water, it can easily penetrate small openings, and is more suitable for gross leak check. The pass ratio of bonded dies was 70%, for conventional localized heating, and 85% for newly developed FP scheme. The bonding strength was more than 30㎫ for FP scheme packaging, which shows that FP scheme can be a good candidate for micro scale hermetic packaging.

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Synthesis and Characterization of Fe Doped TiO2 Nanoparticles by a Sol-Gel and Hydrothermal Process

  • Kim, Hyun-Ju;Jeong, Kwang-Jin;Bae, Dong-Sik
    • Korean Journal of Materials Research
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    • v.22 no.5
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    • pp.249-252
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    • 2012
  • Fe doped $TiO_2$ nanoparticles were prepared under high temperature and pressure conditions by mixture of metal nitrate solution and $TiO_2$ sol. Fe doped $TiO_2$ particles were reacted in the temperature range of 170 to $200^{\circ}C$ for 6 h. The microstructure and phase of the synthesized Fe doped $TiO_2$ nanoparticles were studied by SEM (FE-SEM), TEM, and XRD. Thermal properties of the synthesized Fe doped $TiO_2$ nanoparticles were studied by TG-DTA analysis. TEM and X-ray diffraction pattern shows that the synthesized Fe doped $TiO_2$ nanoparticles were crystalline. The average size and distribution of the synthesized Fe doped $TiO_2$ nanoparticles were about 10 nm and narrow, respectively. The average size of the synthesized Fe doped $TiO_2$ nanoparticles increased as the reaction temperature increased. The overall reduction in weight of Fe doped $TiO_2$ nanoparticles was about 16% up to ${\sim}700^{\circ}C$; water of crystallization was dehydrated at $271^{\circ}C$. The transition of Fe doped $TiO_2$ nanoparticle phase from anatase to rutile occurred at almost $561^{\circ}C$. The amount of rutile phase of the synthesized Fe doped $TiO_2$ nanoparticles increased with decreasing Fe concentration. The effects of synthesis parameters, such as the concentration of the starting solution and the reaction temperature, are discussed.