• Journal of Surface Science and Engineering
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• v.51 no.4
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• pp.249-255
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• 2018

High temperature and low temperature gaseous nitriding was performed in order to study of the surface hardening and wear properties of the nitrided AISI 410 Martensitic stainless steels. High temperature gaseous nitiridng (HTGN) was carried out using partial pressure $N_2$ gas at $1,100^{\circ}C$ for 10 hour, and Low temperature gaseous nitiridng (LTGN) was conducted in a gas mixture of NH3 and N2 at $470^{\circ}C$ for 10 hour. The nitrided samples were characterized by microhardness measurements, optical microscopy and scanning electron microscopy. The phases were identified by X-ray diffraction and nitrogen concentration was analyzed by GD-OES. The HTGN specimen had a surface hardness of about $700HV_{0.1}$, $350{\mu}m$ of case depth. A ${\sim}50{\mu}m$ thick, $1,250HV_{0.1}$ hard nitrided case formed at the surface of the AISI 410 steel by LTGN, composed nitrogen supersaturated expanded martensite and ${\varepsilon}-Fe_{24}N_{10}$ iron nitrides. Additionally, the results of the wear tests, carried out LTGN specimen was low friction coefficient and high worn mass loss of ball. The increase in wear resistance can be mainly attributed to the increase in hardness and to the lattice distortion caused by higher nitrogen concentration.

• Journal of the Korean Society of Manufacturing Technology Engineers
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• v.18 no.3
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• pp.285-293
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• 2009

Thermal infrared cameras have been conducted actively in various application areas, such as military, medical service, industries and cars. Because of their characteristic of sensing the radiant heat emitted from subjects in the range of long-wavelength($3{\sim}5{\mu}m$ or $8{\sim}12{\mu}m$), and of materializing a vision system, when general optics materials are used, they don't react to the light in the range of long-wavelength, and can't display their optic functions. Therefore, the materials with the feature of higher refractive index, reacting to the range of long-wavelength, are to be used. The kinds of materials with the characteristic of higher refractive index are limited, and their features are close to those of metals. Because of these metallic features, the existing producing method of optical systems were direct manufacturing method using grinding method or CAD/CAM, which put limit on productivity and made it difficult to properly cope with the increasing demand of markets. GASIR, a material, which can be molded easily, was selected among infrared ray optics materials in this study, and the optical system was designed with two Aspheric lenses. Because the lenses are molded in the environment of high temperature and high pressure, they require a special metallic pattern. The metallic pattern was produced with materials with ultra hardness that can stand high temperature and high pressure. As for the lens mold, GMP(Glass Molding Press) of the linear transfer method was used in order to improve the productivity of optical systems for thermal infrared cameras, which was the goal of this paper.

• Preventive Nutrition and Food Science
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• v.19 no.3
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• pp.220-226
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• 2014

In the present report, the effects of blanching, steaming, and high temperature/high pressure processing (HTHP) on the amino acid contents of commonly consumed Korean root vegetables, leaf vegetables, and pulses were evaluated using an Automatic Amino Acid Analyzer. The total amino acid content of the samples tested was between 3.38 g/100 g dry weight (DW) and 21.32 g/100 g DW in raw vegetables and between 29.36 g/100 g DW and 30.55 g/100 g DW in raw pulses. With HTHP, we observed significant decreases in the lysine and arginine contents of vegetables and the lysine, arginine, and cysteine contents of pulses. Moreover, the amino acid contents of blanched vegetables and steamed pulses were more similar than the amino acid contents of the HTHP vegetables and HTHP pulses. Interestingly, lysine, arginine, and cysteine were more sensitive to HTHP than the other amino acids. Partial Least Squares-Discriminate Analyses were also performed to discriminate the clusters and patterns of amino acids.

• Proceedings of the Materials Research Society of Korea Conference
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• 2009.05a
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• pp.28.1-28.1
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• 2009

The superior properties of ZnO such as high exciton binding energy, high thermal and chemical stability, low growth temperature and possibility of wet etching process in ZnO have great interest for applications ranging from optoelectronics to chemical sensor. Particularly, vertically well-aligned ZnO nanorods on large areas with good optical and structural properties are of special interest for the fabrication of electronic and optical nanodevices. Currently, low-dimensional ZnO is synthesized by metal-organic chemical vapor deposition (MOCVD), molecular beam epitaxy (MBE), thermal evaporation, and sol.gel growth. Recently, our group has been reported about achievement the growth of Ga-doped ZnO nanorods using ZnO seed layer on p-type Si substrate by RF magnetron sputtering system at high rf power and high growth temperature. However, the crystallinity of nanorods deteriorates due to lattice mismatch between nanorods and Si substrate. Also, in the growth of oxide using sputtering, the oxygen flow ratio relative to argon gas flow is an important growth parameter and significantly affects the structural properties. In this study, Phosphorus (P) doped ZnO nanorods were grown on c-sapphire substrates without seed layer by radio frequency magnetron sputtering with various argon/oxygen gas ratios. The layer change films into nanorods with decreasing oxygen partial pressure. The diameter and length of vertically well-aligned on the c-sapphire substrate are in the range of 51-103 nm and about 725 nm, respectively. The photoluminescence spectra of the nanorods are dominated by intense near band-edge emission with weak deep-level emission.

• Journal of the Korean Society of Propulsion Engineers
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• v.23 no.2
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• pp.118-125
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• 2019

Metals exposed to high temperature/high pressure/oxidant excess environment of an oxygen excess pre-combustor may undergo rapid oxidation. In this study, the test facility to simulate the high temperature/high pressure/oxidant excess environment was constructed and the oxidation resistance evaluation was carried out for various metal materials. As a result, the discoloration of the metallic materials, the change in the surface roughness and the peeling of the metal surface were observed, and the weight change was also observed. The resulst showed that oxidation-resistant coating of a metal material of the combustor is indispensably required, and the use of XM-19, which has the highest content of Cr and Ni, is expected to provide more structural stability.

• KSCE Journal of Civil and Environmental Engineering Research
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• v.44 no.3
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• pp.271-276
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• 2024

Traditional oil, a depleting resource, accounts for only one-third of the world's oil reserves, so research and cases of utilizing non-traditional oil as a resource are continuously increasing. However, unconventional oil contains bitumen containing solid particles such as sand, and because it is exposed to a high temperature and high pressure environment, deformation can frequently occur in oil pipelines. Therefore, variables such as material, thickness, and angle that can affect the deformation of the oil pipeline were derived and applied to the oil pipeline, and finite element analysis was performed using the Ansys program. As a result of finite element analysis, deformation and maximum load capacity were derived. Afterwards, the same analysis was performed by modeling an optimized oil pipeline by combining the factors with the best deformation resistance and maximum load capacity. As a result of the analysis, the effect of reducing deformation and increasing the maximum load capacity by about 30 % was confirmed, and factors for suppressing deformation when analyzing oil pipelines were derived.

• Journal of the Korean Society of Food Science and Nutrition
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• v.32 no.8
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• pp.1221-1226
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• 2003

High hydrostatic Pressure was applied to Foxtail Millet Yakju to investigate the effects of high pressure on inactivation of microorganisms and enzymes. Total bacteria, lactic acid bacteria and yeast in untreated Yakju were $1.5{\times}$10$^4$,1.9${\times}$10$^4$ and 1.4${\times}$10$^4$ CFU/mL, respectively. Total bacterial count was reduced to 4.1${\times}$l0$^2$ CFU/mL, while lactic acid bacteria and yeast were sterilized completely in Yakju heated at $65^{\circ}C$ for 15 min. Lactic acid bacteria and yeast decreased greatly with the increase of treatment pressure, and were sterilized completely in Yakju treated at more than 300 ㎫ for 10 min/$25^{\circ}C$. Total bacteria were not completely sterilized with pressurization of even 600 ㎫ at room temperature and reduced to 2 log cycle even at $65^{\circ}C$. Total bacteria decreased by 2∼3 log cycle with the increase of treatment time from 10 to 60 min at $25^{\circ}C$/300 ㎫. Pressurization of Yakju caused a partial inactivation of $\alpha$ -amylase and glucosamylase, and the activities of $\alpha$ -amylase and glucoamylase decreased by 18.1% and 21.1%, respectively at $25^{\circ}C$/600 ㎫/10 min. Activities of $\alpha$ -amylase and glucoamylase decreased with the increase of temperature, and 22.2% and 32.1% of the original activity were remained with the treatment at $65^{\circ}C$/300 ㎫/10 min, respectively. Enzyme activities decreased slightly with the increase of treatment time at $65^{\circ}C$/300 ㎫.

• Transactions of the Korean Society of Mechanical Engineers B
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• v.41 no.9
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• pp.563-570
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• 2017

Experimental and numerical studies were performed to investigate the performance and internal flow characteristics of a supersonic second throat exhaust diffuser (STED) with back pressure ($P_a$). An ejector system was used to vary the back pressure ($P_a$) conditions. The operating gas for the STED and the ejector was high pressure nitrogen at room temperature. When the back pressure ($P_a$) at a constant nozzle inlet pressure $P_0$) decreases, the pressure recovery location moves downstream. If the pressure ratio $P_0/P_a$) is the same, even if the nozzle inlet pressures $P_0$) are different, the diffuser's internal flow pattern and starting pressure ratio ($(P_0/P_a)_{st}$) are almost the same.

• Proceedings of the KSME Conference
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• 2007.05b
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• pp.2638-2641
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• 2007

The magnetohydrodynamic(MHD) pressure drop along a liquid sodium flow was measured in a rectangular duct under a transverse magnetic field. The test section was made of a 3 mm thick stainless steel SUS304 with a $74{\times}5mm^2$ rectangular flow channel. The range of experimental parameters was roughly B=0${\sim}$0.18T and U=0${\sim}$0.9m/s at around $200^{\circ}C$. The differential pressure was measured by a diaphragm seal-type pressure transmitter filled with a high temperature silicon oil within 0.1MPa. The experimental results show a similar pressure drop with the theoretical estimation according to a change of the flow velocity and the magnetic field.

• Journal of the Mineralogical Society of Korea
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• v.9 no.1
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• pp.35-42
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• 1996

Polycrystalline ZrH2 in tetragonal crystal system has been compressed in a modified Bassett-type diamond anvil cell up to 36.0 GPa at room temperature. X-ray diffraction data did not indicate any phase transitions at the present pressure range. The pressure dependence of the a-axis, c-axis, c/a and molar volume of ZrH2 was determined at pressures up to 36.0 GPa. Assuming the pressure derivative of the bulk modulus (K0') to be 4.11 from an ultrasonic value on Zr, bulk modulus (K0) was determined to be 160Gpa by fitting the pressure-volume data to the Birch-Murnaghan equation of state. Same sample was heated at $500^{\circ}C$ at the pressure of 9.8 GPa in a modified Sung-type diamond anvil cell. Unloaded and quenched sample revealed that the original tetragonal structure transforms into a hexagonal structured phase with a zero-pressure molar volume change of ~115.5%.