• Title/Summary/Keyword: high porosity

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Porosity Prediction of the Coating Layer Based on Process Conditions of HVOF Thermal Spray Coating (HVOF 용사 코팅 공정 조건에 따른 코팅층의 기공도 예측)

  • Jeon, Junhyub;Seo, Namhyuk;Lee, Jong Jae;Son, Seung Bae;Lee, Seok-Jae
    • Journal of Powder Materials
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    • v.28 no.6
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    • pp.478-482
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    • 2021
  • The effect of the process conditions of high-velocity oxygen fuel (HVOF) thermal spray coating on the porosity of the coating layer is investigated. HVOF coating layers are formed by depositing amorphous FeMoCrBC powder. Oxygen pressure varies from 126 to 146 psi and kerosene pressure from 110 to 130 psi. The Microstructural analysis confirms its porosity. Data analysis is performed using experimental data. The oxygen pressure-kerosene pressure ratio is found to be a key contributor to the porosity. An empirical model is proposed using linear regression analysis. The proposed model is then validated using additional test data. We confirm that the oxygen pressure-kerosene pressure ratio exponentially increases porosity. We present a porosity prediction model relationship for the oxygen pressure-kerosene pressure ratio.

Surface Image Analysis for Evaluating Porosity and Permeability Coefficient of Permeable Concrete Block (투수 콘크리트 블록 공극률 및 투수계수 평가를 위한 표면 이미지 분석 기법 개발)

  • Jo, Sangbeom;Son, Younghwan;Kim, Donggeun;Jeon, Jihun;Kim, Taejin
    • Journal of The Korean Society of Agricultural Engineers
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    • v.65 no.2
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    • pp.47-57
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    • 2023
  • The increase of impermeable area ratio is causing hydrologic cycle problems in urban areas and groundwater depletion in rural areas, permeable pavements are getting attention to expand permeable areas. The performance of the permeable concrete block pavement, which is part of the permeable pavement, is greatly affected by the porosity. In addition, the permeability coefficient is a major factor when designing permeable concrete block pavement. Existing porosity and permeability test methods have problems such as uneconomical or poor field applicability. The object of this study was to develop a methodology for evaluating porosity and permeability coefficient using a surface image of a permeable concrete block. Specimens are manufactured with various porosity ranges and porosity and permeability tests are performed. After surface image preprocessing, normalization and binarization methods were compared. Through this, the method with the highest correlation with the lab test result was determined. From the results, the PDR (pore determined ratio) was obtained. Simple linear regression analysis is performed with PDR and lab test results. The results showed a high correlation of R2 more than 0.8, and the errors were also low.

Reduction Method of Porosity Formed by Instability of Keyhole in High Power $CO_2$ Laser Welding (고출력 $CO_2$레이저 용접에서 키홀의 불안정으로 발생한 기공의 절감방법)

  • 김정일;조민현
    • Journal of Advanced Marine Engineering and Technology
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    • v.26 no.4
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    • pp.464-471
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    • 2002
  • Porosity formation in partial penetration welds by high power lasers is a serious problem in industry. There are two main causes that induce porosity formation. One form of porosity is due to gases (e.g. hydrogen, oxygen) dissolving into the weld pool because of the high temperature and then the rapid solidification traps gases as a bubble in the weld metal. The second problem is voids formed by the keyhole collapsing due to unstable keyhole fluid dynamics. The voids that form at the bottom of the keyhole are relatively large and irregular in shape compared to the gas bubbles; this void formation is the primary concern in this paper. The reduction of voids formed by keyhole collapse is achieved by improving the stability of keyhole. Two methods to improve keyhole stability are discussed in this paper: pulse modulation and beam incident angle. Pulse modulation of the laser beam was performed between 100 Hz and 500 Hz to find out the optimum frequency for the keyhole dynamics. The incident beam angle changed the impact angle of the laser beam to the work surface in a range of 0 to 25 degrees. Glycerin in a semi-solidified state is used as a medium for performing the welding because its transparency allows of visualization of the keyhole.

Effect of Die Casting Condition on the Mechanical Properties of AZ91HP Mg Alloy (AZ91HP 마그네슘합금의 기계적성질에 미치는 다이캐스팅 조건의 영향)

  • Ahn, Yong-Sik;Klein, F.
    • Journal of Korea Foundry Society
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    • v.22 no.4
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    • pp.155-159
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    • 2002
  • Magnesium alloys have high strength to weight ratio and are extremely attractive for applications in transport industry. Most of structural magnesium alloys are manufactured by die casting process. The tensile properties of AZ91HP magnesium alloy were investigated after die casting under various die casting conditions. After die casting by using cold chamber machine, the volume porosity of specimens was examined with density method. With the increase of the volume porosity of specimens, both the tensile strength and elongation were significantly decreased, however the 0.2% offset strength was almost independent of the amount of porosity. With the increase of crystal pressure from 500 to 900 bar during die casting, the volume porosity was decreased, which resulted in the increase of the tensile strength. The mould temperature within the range of $150{\sim}250^{\circ}C$ has not influenced the microstructure with the eutectic phase and tensile properties of specimens. The tensile strength was the highest at 90m/sec of gate speed.

Study for Permanent Mold Design Technology and Porosity Defect Prediction Method by Multi-Phase Flow Numerical Simulations (다상유체해석을 통한 기포결함 예측과 금형설계기술)

  • Choi Y. S.;Cho I. S.;Hwang H. Y.;Choi J. K.;Hong J. H.
    • Transactions of Materials Processing
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    • v.14 no.3 s.75
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    • pp.224-232
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    • 2005
  • The high-pressure die-casting is one of the most effective methods to produce a large amount of products in short cycle time. This process, however, has a problem that the gas porosity defect appears easily. The generation of gas porosity is known mainly due to the air entrapment during the injection stage. Most of numerical simulations for the molten metal flow pattern observations have done in the treating of one phase fluid flow but the gas-liquid interface is essentially multi- phase phenomenon. In this paper, the two-phase fluid flow numerical simulation methods have been adapted to predict the gas porosity generations in the molten metal. The accuracy and the usefulness of the new simulation module have been emphasized and verified through some comparison experiments.

Minimization of Porosity in Ceramic Coating on a Hydraulic Cylinder (유압실린더 세라믹코팅 기공률 최소화 방안)

  • Jung, Youngho;Moon, Seung-Jae;Yoo, Hoseon
    • Plant Journal
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    • v.6 no.4
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    • pp.63-71
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    • 2010
  • The best way to prevent the corrosion of piston rod is a selection of quality of the material and method of construction which minimize the porosity. The high velocity oxy fuel(HVOF) method, which generates lower porosity than existing plasma spray, was applied to ceramic laminated bond layer. Porosity percentage fell to bellow 2%, lower than that of plasma spray at 7%. Coating material of ceramic-coated main layer was selected as the $Cr_2O_3$ affiliation material, which is more dense than $Al_2O_3$ affiliation. To fill up the pores formed after the coating process, we sealed the bond layer and main layer. Sealing process was performed twice, once after the coating and once after the grinding. Upon the anti-corrosion test on the sealed sample and on the non-sealed sample, it is confirmed that the sealed sample was not corroded for 1,000 hours while the non-sealed sample was corroded within 48 hours.

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Monolithic porous carbon materials prepared from polyurethane foam templates

  • Pires, Joao;Janeiro, Andre;Oliveira, Filipe J.;Bastos, Alexandre C.;Pinto, Moises L.
    • Carbon letters
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    • v.18
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    • pp.11-17
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    • 2016
  • Monolithic carbon foams with hierarchical porosity were prepared from polyurethane templates and resol precursors. Mesoporosity was achieved through the use of soft templating with surfactant Pluronic F127, and macroporosity from the polyurethane foams was retained. Conditions to obtain high porosity materials were optimized. The best materials have high specific surface areas (380 and 582 m2 g-1, respectively) and high electrical conductivity, which make them good candidates for supports in sensors. These materials showed an almost linear dependence between the potential and the pH of aqueous solutions.

Ultrasonic Phase Velocity and Attenuation Coefficient Predicted by Biot's Theory and the MBA Model in Cancellous Bone

  • Lee Kang Il;Yoon Suk Wang
    • Proceedings of the Acoustical Society of Korea Conference
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    • autumn
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    • pp.183-186
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    • 2004
  • Biot's theory and a modified Biot-Attenborough (MBA) model are applied to predict the dependences of acoustic characteristics on frequency and porosity in cancellous bone. The phase velocity and the attenuation coefficient predicted by both theories are compared with previous in vitro experimental measurements in terms of the mixed, the fast, and the slow waves. Biot's theory successfully predicts the dependences of phase velocity on frequency and porosity in cancellous bone, whereas a significant discrepancy is observed between predicted and measured attenuation coefficients. The MBA model is consistent with reported measurements for both dependences of phase velocity and attenuation coefficient on frequency and porosity. Based on the theoretical predictions from the MBA model, it is suggested that the attenuation coefficient of the mixed wave is dominated by the fast wave in the low-porosity region while it is dominated by the slow wave in the high-porosity region. This provides a qualitative explanation for the nonlinear relationship of attenuation of the mixed wave with porosity in cancellous bone.

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Change of Phase Transformation and Microstructure of Alumina Membrane: I. Effect by Porosity of Support (알루미나 여과막의 상전이와 미세구조 변화: I. 지지체의 기공율에 의한 영향)

  • Cheong, Hun;Hwang, Kwang-Taek;Choi, Duck-Kyun;Cheong, Deock-Soo
    • Korean Journal of Materials Research
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    • v.12 no.3
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    • pp.205-210
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    • 2002
  • The HPS(High Porosity Support, 39.3%) and the LPS( Low Porosity Support, 18.7%) were fabricated to investigate the phase transformation and the chance of microstructure with porosity of alumina support. Alumina sol was made using aluminum tri-sec $butoxide(ATSB,\; Al(O-Bu)_3)$, the membrane on porous support with different porosity and the membrane without support were fabricated. The $\theta$-to ${\alpha}-A1_2O_3$ phase transformation in the membranes was investigated using thin film X-ray diffraction (XRD), and the change of microstructure was observed using scanning electron microscopy(SEM). XRD patterns showed that the membrane on LPS and HPS had 10$0^{\circ}C$, 5$0^{\circ}C$ higher $\theta$-to ${\alpha}-A1_2O_3$ transformation temperature compared to the unsupported membrane. A similar effect was also observed in microstructure of the membranes, theoritical temperature difference were 97$^{\circ}C$ and 44$^{\circ}C$ by Crapeyron equation.

Effect of Microstructure on Mechanical and Electrical Properties in Ni-YSZ of Anode Supported SOFC (연료극 지지체식 고체산화물 연료전지의 기계적 및 전기적 특성에 미치는 Ni-YSZ의 미세구조의 영향)

  • Choi, Mi-Hwa;Choi, Jin-Hyeok;Lee, Tae-Hee;Yoo, Young-Sung
    • Journal of Hydrogen and New Energy
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    • v.22 no.5
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    • pp.592-598
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    • 2011
  • Electrode of solid oxide fuel cell must have sufficient porosity to allow gas transport to the interface with electrolyte effectively but high porosity has a negative impact on structural stability in electrode support. Thus, the upper limit of porosity is based on consideration of mechanical strength of electrode. In this study, the effect of microstructure of Ni-YSZ anode supported SOFC on the mechanical and electrical property was investigated. LSCF composite cathode and 8YSZ electrolyte were used. The porosity of the anode was modified by the amount of graphite powder and added graphite contents were 24, 18, 12 vol%, respectively. The higher the porosity, the better the electrical performance, $P_{max}$. While the flexural strength decreased with increasing the amount of graphite. But the rate of increase in electrical performance and the rate of decrease in mechanical strength were not directly proportional to amount of graphite. The optimum graphite content incorporating both electrical and mechanical performance was 18 vol%.