• Title/Summary/Keyword: high curing temperature

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Optimum Mix Design of Alkali-Activated Cement Mortar Using Bottom Ash as Binder (바텀애쉬를 결합재로 사용한 알칼리 활성화 시멘트 모르타르의 최적배합에 관한 연구)

  • Kang, Su-Tae;Ryu, Gum-Sung;Koh, Kyoung-Taek;Lee, Jang-Hwa
    • Journal of the Korea Concrete Institute
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    • v.23 no.4
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    • pp.487-494
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    • 2011
  • In this research, the possibility of using bottom ash as a binder for the alkali-activated cement mortar is studied. Several experiments were performed to investigate the variation of the material properties according to the mix proportion. In the experimental program, the flowability and compressive strength were evaluated for various values of water/ash ratio, activator/ash ratio, sodium silicate to sodium hydroxide ratio, curing temperature, and the fineness of bottom ash as the main variables. The experimental results showed that high strength of 40 MPa or greater could be achieved in $60^{\circ}C$ high temperature curing condition with proper flowability. For $20^{\circ}C$ ambient temperature curing, the 28 days compressive strength of approximately 30MPa could be obtained although the early-age strength development was very slow. Based on the results, the range of optimized mix design of bottom-ash based alkali-activated cement mortar was suggested. In addition, using the artificial neural network analysis, the flowability and compressive strength were predicted with the difference in the mix proportion of the bottom-ash based alkali-activated cement mortar.

An Experimental Study of Precast Concrete Alters Cement Types of High-Strength Concrete (시멘트종류를 변화시킨 프리캐스트 고강도 콘크리트의 실험적 연구 - 압축강도특성을 중심으로 -)

  • Park, Heung-Lee;Ki, Jun-Do;Kim, Sung-Jin;Lee, Hoi-Keun;Park, Byung-Keun;Jung, Jang-Jin
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2009.05b
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    • pp.65-68
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    • 2009
  • Recently, as architectural concrete structures become high-rise and megastructured, concrete become high-strengthened and, by ensuring products of more stability, and rationalization of construction are required.large cross-sectional precast concrete members such as columns show large temperature increase in manufacturing process not only by external heating but also by concrete itself's hydration heating. Therefore, it is expected that specimen for management to predict strength and compression strength of precast concrete member shows different strength characteristics. Concerning this, in order to suggest strength characteristics of high strength mass concrete suitable for precast concrete application, this study comprises the inclusive investigations on the relations between core strength and the strength characteristics per member cross-section dimensional value and per water-bonding material ratio value.

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Development of Pilot-Scale Manufacturing Process of SiC Fiber from Polycarbosilane Precursor with Excellent Mechanical Property at Highly Oxidation Condition and High Temperature (폴리카보실란 전구체로부터 고온 산화성분위기서 기계적물성이 우수한 파이롯-규모의 탄화규소섬유 제조공정 개발)

  • Yoon, B.I.;Choi, W.C.;Kim, J.I.;Kim, J.S.;Kang, H.G.;Kim, M.J.
    • Composites Research
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    • v.30 no.2
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    • pp.116-125
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    • 2017
  • The purpose of this study is to develop silicon carbide fiber showing an excellent mechanical properties under highly oxidative conditions at high temperature. Polycarbosilane(PCS) as a preceramic precursor was used for making the SiC fiber. PCS fiber was taken by melt spinning method followed by melting the PCS at $300{\sim}350^{\circ}C$ in N2 gas. The Curing of PCS fiber was carried out in air oxygen chamber, prior to high temperature pyrolysis. Degree of cure was calculated by characteristic peak's ratio of Si-H to $Si-CH_3$ in FT-IR spectra before and after curing of PCS fiber. The properties of SiC fiber was affected greatly by the degree of cure. The SiC fiber produced by controlling fiber tension during heat treatment showed good properties. The SiC fiber exposed to $1000^{\circ}C$ at air from 1 min. up to maximum 50 hrs showed around 60% reduction in tensile strength. We found that large amount of carbon content on the fiber surface after long-term exposure has resulted in lower tensile strength.

An Experimental Study on Strength Development of Micro Grinding Fly-ash Mortar - Effect of Alkali Activator and High Temperature Curing on the Compressive Strength of Concrete - (미분쇄한 플라이애시 모르타르의 강도증진 방안에 관한 연구 - 알칼리 자극제와 고온양생이 강도에 미치는 영향 -)

  • Cho, Hyun-Dae;Jaung, Jae-Dong
    • Journal of the Korea Institute of Building Construction
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    • v.10 no.1
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    • pp.39-47
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    • 2010
  • Fly ash has the advantages, among others, of improving the characteristics of concrete, reducing the price of concrete products, improving the durability, and reducing hydration heat. However, when added in mass, it leads to problems such as insufficient concrete intensity, increase of AE use, and others, resulting in a limitation of the use volume. Therefore, this study is undertaken to solve the problems associated with themass use of fly ash through the high concentration powder ($4000{\sim}8000cm^2/g$) of fly ash, curing method, the addition of an alkali stimulation agent and others for the purpose of increasing the added value of the fly ash. The research showed that the intensity manifestation has an outstanding status, with the hydrates reaching a very stable condition if the rate of addition of a stimulation agent is appropriately used with the heightening of the fineness of the fly ash in the temperature range of $40^{\circ}C$, and if the applicable study is continued, it is likely to result ineffective value generation on the massive replacement of fly ash.

Experimental Study on Bond Strength between Carbon Fiber Sheet and Concrete (탄소섬유쉬트와 콘크리트의 부착강도 실험연구)

  • 유영찬;최기선;최근도;이한승;김긍환
    • Journal of the Korea Concrete Institute
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    • v.13 no.2
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    • pp.168-174
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    • 2001
  • Carbon fiber sheet(CFS) has been widely used for strengthening of the concrete building structures due to its excellent physical properties such as high strength, light weight and high durability. Bond strength or behavior, on the other hands, between carbon fiber sheet and concrete is very important in strengthening the concrete member using CFS. Therefore the bond failure mechanism between CFS and concrete should be fully verified and understood. This study is to investigate the bond strength of CFS to the concrete by the direct pull-out test and the tensile-shear test. In the direct pull-out tests, the bond strength under the various environmental conditions such as curing temperature, surface condition on concrete and water content of concrete are evaluated. Also, the effective bond length, lu and the average bond stress, $\tau$y are examined in the tensile-shear tests. Based on the test results, it is concluded that the curing temperature is the most critical element for the bond strength between CFS and concrete. And, the proper value of lu and $\tau$y is recommended with 15 cm and 9.78∼ 11.88 kgf/$\textrm{cm}^2$ respectively.

Effects of Hardeners and Catalysts on the Reliability of Copper to Copper Adhesive Joint (Cu-Cu 접착부의 고온고습 내구성에 미치는 경화제 및 촉매제의 영향)

  • Min, Kyung-Eun;Kim, Hae-Yeon;Bang, Jung-Hwan;Kim, Jong-Hoon;Kim, Jun-Ki
    • Korean Journal of Materials Research
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    • v.21 no.5
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    • pp.283-287
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    • 2011
  • As the performance of microelectronic devices is improved, the use of copper as a heat dissipation member is increasing due to its good thermal conductivity. The high thermal conductivity of copper, however, leads to difficulties in the joining process. Satisfactory bonding with copper is known to be difficult, especially if high shear and peel strengths are desired. The primary reason is that a copper oxide layer develops rapidly and is weakly attached to the base metal under typical conditions. Thus, when a clean copper substrate is bonded, the initial strength of the joint is high, but upon environmental exposure, an oxide layer may develop, which will reduce the durability of the joint. In this study, an epoxy adhesive formulation was investigated to improve the strength and reliability of a copper to copper joint. Epoxy hardeners such as anhydride, dihydrazide, and dicyandiamide and catalysts such as triphenylphosphine and imidazole were added to an epoxy resin mixture of DGEBA and DGEBF. Differential scanning calorimetry (DSC) analyses revealed that the curing temperatures were dependent on the type of hardener rather than on the catalyst, and higher heat of curing resulted in a higher Tg. The reliability of the copper joint against a high temperature and high humidity environment was found to be the lowest in the case of dihydrazide addition. This is attributed to its high water permeability, which led to the formation of a weak boundary layer of copper oxide. It was also found that dicyandiamide provided the highest initial joint strength and reliability while anhydride yielded intermediate performance between dicyandiamide and dihydrazide.

Characteristics of Temperature History of Slab concrete by the Change of Hot wire Heat Capacity at -10℃ (-10℃ 조건에서의 열선 열용량 크기 변화에 따른 슬래브 콘크리트의 온도이력 특성)

  • Jung, Eun-Bong;Ahn, Sang-Ku;Jung, Sang-Hyun;Koh, Kyung-Taek;Han, Min-Cheol;Han, Cheon-Goo
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2013.05a
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    • pp.75-77
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    • 2013
  • In this study, the characteristics of temperature history was evaluated for three hot wires with different capacity installed in slab concrete which are relatively thin. Results can be summarized as follows. First, for the case of material using 5W hot wire, all decreased to below zero at or around 24 hours. Similarly, the material using 20W hot wire decreased to 2℃ below zero at or around 80 hours but satisfied the accumulative temperature of 45° D·D at 7 days of material age. On the other hand, the case of 30W hot wire, the biggest capacity, showed the high temperature history of 5℃ in average at all areas except the corners. Thus, the target accumulative temperature was secured at or around the 3 days of material age. Considering the above, the initial damage by freezing can be prevented only if 20W or higher hot wires are used for the slabs at -10℃ of extremely low temperature environment.

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A Study on Properties of Early Strength Development of the Concrete (콘크리트의 조기강도 발현특성에 관한 연구)

  • Kang, Chang-Woon;Lee, Jae-Sam;Kim, Jung-Sik;Sung, Yong-Hwan;Ryu, Deug-Hyun
    • Proceedings of the Korea Concrete Institute Conference
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    • 2008.11a
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    • pp.541-544
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    • 2008
  • Recently, due to the increase of high-rise buildings construction, many researches for making harden of concrete earlier and remove of forms faster are being performed to reduce construction period. The purpose of this study is to analysis which mixing condition and curing temperature of early strength concrete. Porperties of concrete by the different factors, such as the type of active admixtures, mineral admixtures, curing temperature, the amount of binder, etc. Through the test of concrete using the different type of admixture, PC type was more excellent than PNS type admixture. The concrete Strength remarkably will be able to confirm that decreases from temperature below 12$^{\circ}C$.

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Estimation of Radio Frequency Electric Field Strength for Dielectric Heating of Phenol-Resorcinol-Formaldehyde Resin Used for Manufacturing Glulam (구조용 집성재 제조용 접착제(Phenol-Resorcinol-Formaldehyde Resin) 유전 가열을 위한 고주파 전기장 세기 추산)

  • Yang, Sang-Yun;Han, Yeonjung;Park, Yonggun;Eom, Chang-Deuk;Kim, Se-Jong;Kim, Kwang-Mo;Park, Moon-Jae;Yeo, Hwanmyeong
    • Journal of the Korean Wood Science and Technology
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    • v.42 no.3
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    • pp.339-345
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    • 2014
  • For enhancing productivity of glulam, high frequency (HF) curing technique was researched in this study. Heat energy is generated by electromagnetic energy dissipation when HF wave is applied to a dielectric material. Because both lamina and adhesives have dielectric property, internal heat generation would be occurred when HF wave is applied to glulam. Most room temperature setting adhesives such as phenol-resorcinol-formaldehyde (PRF) resin, which is popularly used for manufacturing glulam, can be cured more quickly as temperature of adhesives increases. In this study, dielectric properties of larch wood and PRF adhesives were experimentally evaluated, and the mechanism of HF heating, which induced the fast curing of glue layer in glulam, was theoretically analyzed. Result of our experiments showed relative loss factor of PRF resin, which leads temperature increase, was higher than that of larch wood. Also, it showed density and specific heat of PRF, which are resistance factors of temperature increase, were higher than those of wood. It was expected that the heat generation in PRF resin by HF heating would occur greater than in larch wood, because the ratio of relative loss factor to density and specific heat of PRF resin was greater than that of larch wood. Through theoretical approach with the experimental results, the relative strengths of ISM band HF electric fields to achieve a target heating rate were estimated.

Fabrication of High Density and High Uniformity Irradiation Light Source for Exposure Curing System Using 365 nm and 385 nm Wavelength SMD LED and High Transmittance Silicone Resin TIR Bar Type Lens (365 nm 및 385 nm SMD LED와 TIR 바형 렌즈를 이용하는 고밀도 고균일성 특성의 경화용 광원모듈 제작 )

  • Pil Hong Jeong;Beom Jin Kim;Yeong Jin Kim;Dong Gyu Jeon;Hyo Min Kim;Jae Hyeon Kim;Hyeong Min Kim;Gyu Seong Lee;Kawan Anil;Eung Ryul Park;Soon Jae Yu;Min Jun Ann;Do Won Hwang
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.37 no.4
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    • pp.394-399
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    • 2024
  • An irradiator is developed using two UVA wavelength ranges of SMD LEDs as a curing light source. This module has dimensions of 545×111×300 mm3 and is equipped with a TIR bar-shaped lens made of PDMS silicone resin. The developed irradiator offers high uniformity, with 89% in the centerline of the horizontal axis direction, for two different wavelength ranges of 365 nm and 385 nm. The radiation intensity from the light source module shows highly directional characteristics, and the irradiator provides a maximum irradiance of 1,634 mW/cm2 at a working distance of 50 mm. During the initial 5 minutes of operation, the irradiance experiences a rapid decrease. However, this issue is addressed by optimizing the LED's current reduction characteristics and managing the Transistor's temperature rise in the constant current circuit. After continuous operation for approximately 60 minutes. The highest temperature, near the central part of the irradiating surface, reaches 69.7℃, while the lowest temperature, near the edges, is 41.1℃.