• Title/Summary/Keyword: high curing temperature

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The study on cure behavior and dielectric property of Ceramic (BNT)-Polymer (BCB) composite material (세라믹(BNT)-폴리머(BCB) 복합체의 경화 거동과 유전특성에 대한 연구)

  • Kim, Un-Yong;Chun, Myoung-Pyo;Cho, Jung-Ho;Kim, Byung-Ik;Myoung, Sung-Jae;Sin, Dong-Uk
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.17 no.6
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    • pp.251-255
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    • 2007
  • We made $(1-x)BCB-xBNT(BaNd_2Ti_4O_{12})$ (x=20, 30, 40, 50 vol%) composite thick film with a high dielectric constant and low loss by the hand casting method. Dielectric constant and dielectric loss of prepared thick film are measured at 1MHz and curing behavior of the film are observed through thermal analysis such as DSC. We investigated the effect of contents of BNT filler and curing behavior of film on dielectric properties of BCB-BNT composite. Dielectric constant increased with increasing BNT filler from 20 to 50 vol% and dielectric loss ($tan{\delta}$) decreased with increasing BNT filler. Dielectric constant and loss ($tan{\delta}$) of composite material was not nearly dependent on the curing behavior. But as a result of TCC (Temperature Characteristics of Coefficient) decreased with increasing the curing temperature, we confirmed that the curing of these composite system is most stable above $250^{\circ}C$.

THERMAL CHANGE AND MICROHARDNESS IN CURING COMPOSITE RESIN ACCORDING TO VARIOUS CURING LIGHT SYSTEM (광중합기에 따른 복합레진 중합시 온도 변화와 미세경도에 관한 연구)

  • Lee, Dong-Jin;Kim, Dae-Eop;Yang, Yong-Sook;Lee, Kwang-Hee
    • Journal of the korean academy of Pediatric Dentistry
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    • v.31 no.3
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    • pp.391-399
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    • 2004
  • The purpose of this study was to compare curing efficiency of newly developed curing units to traditional halogen curing unit by measuring thermal change and surface microhardness according to curing light system. Materials and mathods : The types of curing units were traditional low intensity halogen light(Optilux 360), plasma arc light(Flipo), low heat plasma arc light(Aurys), low intensity LED(Starlight), and high intensity LED(Freelight2). Temperature at the tip of light guide was measured by a digital thermometer using K-type thermocouple. And after resin was filled to 2, 3, 4mm teflon mold, bottom temperature measured during curing. After 24 hours, microhardness of top surface and bottom surface of each resin specimen were measured. Results : The result of this study can be summarized as follows, 1. As measuring temperature of curing unit tips, Flipo is the highest as $52.4^{\circ}C,\;Freelight2(37.86^{\circ}C),\;Optilux360(32.68^{\circ}C),\;Aurys(32.34^{\circ}C),\;and\;Starlight(26.14^{\circ}C)$ were followed. 2. Flipo and Freelight2 were the highest similarly and Optilux360 and Aurys were similarly next and Starlight was lowest in temperature of bottom surface of resin mold. 3. Microhardness of top surface were generally similar, and Aurys was relatively low. 4. Optilux 360 and Freelight2 were the highest, and Flipo, Starlight, and Aurys were followed in microhardness of bottom surface. Conclusions : The results suggest that careful use of Flipo and Freelight2 might be able to cure greater depth of resin composite and do not cause thermal problems than other curing units.

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The Mechanical Properties of High Strength Concrete in Massive Structures

  • Park, Ki-Bong
    • Architectural research
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    • v.15 no.1
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    • pp.53-58
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    • 2013
  • High strength concrete is being used increasingly in mass structure projects. The purpose of this study is to investigate the influence of temperature during mixing, placing and curing on the strength development, hydration products and pore structures of high strength concrete in mass structures. The experiments were conducted with two different model walls, viz.: 1.5 m and 0.3 m under typical summer and winter weather conditions. The final part of this study deal with the clarification of the relationship between the long-term strength loss and the microstructure of the high strength concrete at high temperatures. Test results indicated that high elevated temperatures in mass concrete structures significantly accelerate the strength development of concrete at the early ages, while the long-term strength development is decreased. The long-term strength loss is caused by the decomposition of ettringite and increased the total porosity and amount of small pores.

An Experimental Study on Hydration Temperature Property of High-strengthConcrete Cured by Steam (증기양생을 실시한 고강도 콘크리트의 수화온도특성에 관한 실험적 연구 -시멘트 종류 및 양생조건을 중심으로-)

  • Park, Heung-Lee;Kim, Sung-Jin;Paik, Min-su;Lee, Hoi-Keun;Park, Byung-Keun;Jung, Sang-Jin
    • Proceedings of the Korea Concrete Institute Conference
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    • 2009.05a
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    • pp.267-268
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    • 2009
  • s manufacturing the Precast Concrete simulation structure, we generally investigated the temperature characteristics of the concrete according to diversity of the cement and heat curing condition respectively.

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The ink jet printing of high conductivity circuits on various substrates using polymer capped nano-particle silver

  • Edwards, Charles O.;Howarth, James;James, Anthony
    • 한국정보디스플레이학회:학술대회논문집
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    • 2005.07a
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    • pp.814-816
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    • 2005
  • In this paper, we describe how specially developed polymer capped, nano-particle silver inks can be used to print circuitry for applications like displays, RFID antennas and "disposable electronics". The requirements of printing on temperature sensitive flexible substrates (such as polymer films and papers) that require low temperature curing is also discussed.

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Analysis of Thermal Stresses in Polymeric Thin Film (고분자 박막에서의 열응력 해석)

  • 이상순
    • Proceedings of the Computational Structural Engineering Institute Conference
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    • 2003.10a
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    • pp.389-394
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    • 2003
  • In this study, the stress singularity factors generated during cooling down from high curing temperature to room temperature have been analyzed for the viscoelastic thin film. The time domain boundary element method has been employed to investigate the behavior of stresses for the whole interface. Within the context of a linear viscoelastic theory, a stress singularity exists at the point where the interface between the elastic substrate and the viscoelastic thin film intersects the free surface.

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An Experimental Study on Developing Ultra-High Strength Powder Concrete Using Low-heat Portland Cement (저열 포틀랜드 시멘트를 사용한 초고강도 분체 콘크리트 개발에 관한 실험적 연구)

  • Jo, Byung-Wan;Yoon, Kwang-Won;Kim, Heoun;Park, Jin-Mo
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.13 no.6 s.58
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    • pp.135-147
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    • 2009
  • In order to develop the ultra high strength concrete over 400Mpa at 28 day, Low-heat portland cement, ferro-silicon, silica-fume and steel fiber were mixed and tested under the special autoclave curing conditions. Considering the influence of Ultra high strength concrete. normal concrete is used as a comparison with low water-cement ratio possible Low-heat portland cement. Additionally, as a substitution of aggregates, we analyzed the compressive strength of Ferro Silicon by making the states of mixed and curing conditions differently. In addition, SEM films testified the development of C-S-H hydrates of Type III & Type IV, and tobermolite, zonolite due to the high temperature, high pressure of autoclave curing. Fineness of aggregate, filler and reactive materials in concrete caused 420Mpa compressive strength at 28day successfully.

Evaluation on In-Site Compressive Strength of High-Strength Concrete Mass Elements under Cold Weather (혹한기 고강도 콘크리트 매스부재의 현장 압축강도 평가)

  • Mun, Jae-Sung;Yang, Keun-Hyeok;Kim, Do-Gyeu
    • Journal of the Korea Institute of Building Construction
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    • v.15 no.6
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    • pp.589-595
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    • 2015
  • This study evaluated the in-site compressive strength development of high-strength concrete developed for the mass structures under cold weather condition. Two mock-up wall specimens with $2.0{\times}1.2{\times}1.0m$ in dimension were cured under an average temperature of $5^{\circ}C$. Core strengths measured at different locations of the mock-up walls were compared with the companion standard cylinder strengths. Test results revealed that the core strength of mock-up walls at an age of 3 days is higher by approximately 30% than the companion cylinder strength because of the high curing temperature effect generated from the heat of hydration of cementitious materials. Furthermore, comparisons with the prediction models based on maturity function confirmed that the effect of hydration heat on the curing temperature increase needs to be reflected to reasonably evaluate the on-site compressive strength development of concrete for mass elements.

Chemorheological Behavior of Cyanate Ester Resin and Properties of Carbon Fiber Reinforced Polymer Composites (시아네이트 에스터 수지의 화학유변학적 거동 및 탄소섬유강화 고분자 복합재료의 물성)

  • Na, Hyo Yeol;Yoon, Byung Chul;Kim, Seung Hwan;Lee, Seong Jae
    • Elastomers and Composites
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    • v.48 no.2
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    • pp.133-140
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    • 2013
  • Carbon fiber reinforced polymer (CFRP) composites consist of carbon fibers in a polymer matrix. Recently, CFRP composites having high thermal stability and low outgassing are finding their use in high performance materials for aerospace and electronics applications under high temperature and high vacuum conditions. Cyanate ester resin is one of the most suitable matrix resins for this purpose. In this study, proper combination of cyanate ester and catalyst, curing behavior, and cure cycle were determined by chemorheology. Optimum condition was found to be catalyst content of 100 ppm and curing temperature of $150^{\circ}C$. Thermal stability and outgassing of cured resin composition were analyzed and the results showed thermal decomposition temperature of $385^{\circ}C$ and total mass loss of 0.29%. The CFRP prepregs and subsequent composites were fabricated by predetermined resin composition and the cure condition. Tensile moduli of the composites were compared with theoretical models and the results were very consistent.

Effect of ages and season temperatures on bi-surface shear behavior of HESUHPC-NSC composite

  • Yang Zhang;Yanping Zhu;Pengfei Ma;Shuilong He;Xudong Shao
    • Advances in concrete construction
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    • v.15 no.6
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    • pp.359-376
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    • 2023
  • Ultra-high-performance concrete (UHPC) has become an attractive cast-in-place repairing material for existing engineering structures. The present study aims to investigate age-dependent high-early-strength UHPC (HESUHPC) material properties (i.e., compressive strength, elastic modulus, flexural strength, and tensile strength) as well as interfacial shear properties of HESUHPC-normal strength concrete (NSC) composites cured at different season temperatures (i.e., summer, autumn, and winter). The typical temperatures were kept for at least seven days in different seasons from weather forecasting to guarantee an approximately consistent curing and testing condition (i.e., temperature and relative humidity) for specimens at different ages. The HESUHPC material properties are tested through standardized testing methods, and the interfacial bond performance is tested through a bi-surface shear testing method. The test results quantify the positive development of HESUHPC material properties at the early age, and the increasing amplitude decreases from summer to winter. Three-day mechanical properties in winter (with the lowest curing temperature) still gain more than 60% of the 28-day mechanical properties, and the impact of season temperatures becomes small at the later age. The HESUHPC shrinkage mainly occurs at the early age, and the final shrinkage value is not significant. The HESUHPC-NSC interface exhibits sound shear performance, the interface in most specimens does not fail, and most interfacial shear strengths are higher than the NSC-NSC composite. The HESUHPC-NSC composites at the shear failure do not exhibit a large relative slip and present a significant brittleness at the failure. The typical failures are characterized by thin-layer NSC debonding near the interface, and NSC pure shear failure. Two load-slip development patterns, and two types of main crack location are identified for the HESUHPC-NSC composites tested in different ages and seasons. In addition, shear capacity of the HESUHPC-NSC composite develops rapidly at the early age, and the increasing amplitude decreases as the season temperature decreases. This study will promote the HESUHPC application in practical engineering as a cast-in-place repairing material subjected to different natural environments.