• Title/Summary/Keyword: heat treatment parameter

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Annealing Effects on the Properties of Bi-doped ZnO Thin Film (Bi-doped ZnO 박막의 열처리에 따른 특성)

  • Shin, Johngeon;Hwang, Injoo;Cho, Shinho
    • Journal of the Korean Society for Heat Treatment
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    • v.33 no.1
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    • pp.13-19
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    • 2020
  • Annealing effects on the properties of Bi-doped ZnO thin films were investigated. Bi- doped ZnO thin films were deposited on quartzs substrates at 300℃ by using radio-frequency magnetron sputtering system. Post heat treatments at 600, 700, and 800℃ were performed to evaluate the effect of annealing temperatures on the structural, optical, and electrical properties of Bi-doped ZnO thin films. FE-SEM images showed the dramatic surface morphology changes by rearrangement of elements at high heat treatment temperature of 800℃. X-ray diffraction analysis indicated that the peaks of the Bi-doped ZnO thin films were same as the peaks of the (002) planes of ZnO peak-positioned at 2θ=34.0° and peak intensities and FWHMs were improved as the annealing temperatures increased. The optical transmittance was improved with increasing annealing temperatures and was over 80% in the wavelength region between 435 and 1100 nm at the annealing temperature of 700 and 800℃. With increasing annealing temperature, the electron concentrations and electron mobilities were increased. On the other hand, electric resistivity of the films were decreased with increasing annealing temperatures. These results showed that the heat treatment temperature is an important parameter to improve the structural, optical, and electrical properties of Bi-doped ZnO thin films.

Direct Heat Treatment of Alloyed Steel Forging (가공열을 이용한 합금강 단조품의 열처리)

  • Kwon, Y.N.;Kim, T.O.;Kwon, Y.C.;Park, D.G.;Lee, S.G.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2008.10a
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    • pp.431-434
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    • 2008
  • In the present study, direct quenching of alloyed steel after hot forging was simulated using commercial finite element program, $FORGE^{TM}$. A typical heat treatment of alloyed steels consists of quenching for hard martensite and subsequent tempering for toughness. In the practice, forgings which cool down to room temperature are heated to temperature of austenite regime. As investigated in the present study, direct quenching of hot forged stock would be beneficial in terms of energy saving. This process has already been propose and termed as ausforging or forged hardening. However, it is well known that quenching temperature would be the most critical factor to control heat treated forging properties. And it is very difficult to control quenching temperature when forged stock gets directly quenched after forging. In this study, we have calculated final forging temperature of stock. Also, quenching simulation was conducted using a series of material parameter which were also calculated using JMATpro, a commercial program for physical properties of materials.

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Microstructural Evolution in CuCrFeNi, CuCrFeNiMn, and CuCrFeNiMnAl High Entropy Alloys

  • Hyun, Jae Ik;Kong, Kyeong Ho;Kim, Kang Cheol;Kim, Won Tae;Kim, Do Hyang
    • Applied Microscopy
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    • v.45 no.1
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    • pp.9-15
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    • 2015
  • In the present study, microstructural evolution in CuCrFeNi, CuCrFeNiMn, and CuCrFeNiMnAl alloys has been investigated. The as-cast CuCrFeNi alloy consists of a single fcc phase with the lattice parameter of 0.358 nm, while the as-cast CuCrFeNiMn alloy consists of (bcc+fcc1+fcc2) phases with lattice parameters of 0.287 nm, 0.366 nm, and 0.361 nm. The heat treatment of the cast CuCrFeNiMn alloy results in the different type of microstructure depending on the heat treatment temperature. At $900^{\circ}C$ a new thermodynamically stable phase appears instead of the bcc solid solution phase, while at $1,000^{\circ}C$, the heat treated microstructure is almost same as that in the as-cast state. The addition of Al in CuCrFeNiMn alloy changes the constituent phases from (fcc1+fcc2+bcc) to (bcc1+bcc2).

Effects of Heat-treatment Parameters on Mechanical Properties of A3003 Al Alloy Tubes for Heat-exchangers by High Frequency Induction Welding (고주파유도 용접된 A3003 알루미늄합금 튜브의 기계적 특성에 미치는 열처리조건의 영향)

  • Gook, Jin-Seon;Yoon, Dong-Ju;Kim, Byung-Il
    • Journal of the Korean Society for Heat Treatment
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    • v.19 no.3
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    • pp.156-162
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    • 2006
  • The aim of this study is to investigate the full annealing parameter for A3003 Al alloy welded tubes. The A3003 Al alloy tubes with 34 mm in external diameter and 1.3 mm in thickness for OPC drum were manufactured by high frequency induction welding with the V shaped convergence angle $6.7^{\circ}$ and power input 50 kW. The tensile and yield strength decreased with increasing the annealing temperature and time remarkably, but elongation increased remarkably. Vickers hardness in welds and base metal decreased with increasing the annealing temperature and time remarkably. In a certain experimental condition, the welds line in A3003 alloys disappeared at $520^{\circ}C$ for 4hr because of the same mechanical properties and structures between welds and base metal.

Influence of Heat Treatment Conditions on Temperature Control Parameter ((t1) for Shape Memory Alloy (SMA) Actuator in Nucleoplasty (수핵성형술용 형상기억합금(SMA) 액추에이터 와이어의 열처리 조건 변화가 온도제어 파라미터(t1)에 미치는 영향)

  • Oh, Dong-Joon;Kim, Cheol-Woong;Yang, Young-Gyu;Kim, Tae-Young;Kim, Jay-Jung
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.34 no.5
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    • pp.619-628
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    • 2010
  • Shape Memory Alloy (SMA) has recently received attention in developing implantable surgical equipments and it is expected to lead the future medical device market by adequately imitating surgeons' flexible and delicate hand movement. However, SMA actuators have not been used widely because of their nonlinear behavior called hysteresis, which makes their control difficult. Hence, we propose a parameter, $t_1$, which is necessary for temperature control, by analyzing the open-loop step response between current and temperature and by comparing it with the values of linear differential equations. $t_1$ is a pole of the transfer function in the invariant linear model in which the input and output are current and temperature, respectively; hence, $t_1$ is found to be related to the state variable used for temperature control. When considering the parameter under heat treatment conditions, $T_{max}$ was found to assume the lowest value, and $t_1$ was irrelevant to the heat treatment.

Multi- effect air gap membrane distillation process for pesticide wastewater treatment

  • Pangarkar, Bhausaheb L.;Deshmukh, Samir K.;Thorat, Prashant V.
    • Membrane and Water Treatment
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    • v.8 no.6
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    • pp.529-541
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    • 2017
  • A multi-effect air gap membrane distillation (ME-AGMD) module for pesticide wastewater treatment is studied with internal heat recovery, sensible heat of brine recovery, number of stages and the use of fresh feed as cooling water in a single module is implemented in this study. A flat sheet polytetrafluroethylene (PTFE) membrane was used in the 4-stage ME-AGMD module. The maximum value of permeate flux could reach $38.62L/m^2h$ at feed -coolant water temperature difference about $52^{\circ}C$. The performance parameter of the module like, specific energy consumption and gain output ratio (GOR) was investigated for the module with and without heat recovery. Also, the module performance was characterized with respect to the separation efficiency of several important water quality parameters. The removal efficiency of the module was found to be >98.8% irrespective water quality parameters. During the experiment the membrane fouling was caused due to the deposition of the salt/crystal on the membrane surface. The membrane fouling was controlled by membrane module washing cycle 9 h and also by acidification of the feed water (pH=4) using 0.1M HCl solution.

Heat Treatment for Improvement of Hardness Uniformity of Standard Hardness Blocks (경도 기준편의 경도 균일성 향상을 위한 열처리)

  • Hahn, J.H.;Hwang, N.M.;Kim, J.J.;Moon, H.G.
    • Journal of the Korean Society for Heat Treatment
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    • v.2 no.2
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    • pp.33-37
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    • 1989
  • In order to improve hardness uniformity of standard-hardness blocks. experimental procedure was designed using Taguchi Method. For this purpose the following factors were studied: austenitizing temperature, tempering condition, grinding condition, subzero treatment, lapping time, $15{\mu}m$ polishing time, final polishing time. These factors were processed and then ten hardness values were measured on each specimen. SN (signal to noise) ratio for each condition was calculated with standard variations of these values. Finally, from the calculated value of ANOVA on SN ratios, the lapping time was found to be the main factor Better uniformity with longer lapping time implies that residual stress that was formed after quenching is a dominent parameter that affects on the uniformity of hardness. Therefore, step-quenching method was adapted to minimize the residual stress. By this modification of quenching procedure, the hardness uniformity was improved remarkably and the yield ratio was increased from 55% to 88%.

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Effects of Quenching and Tempering Process Conditions on the Microstructure and Hardness of SCM420 Alloy steel (SCM420 합금강의 미세조직 및 경도에 미치는 급냉 및 템퍼링 공정조건의 영향)

  • Jun-Ha Lee;Kyung-Sik Shin;Jeong-Min Kim
    • Journal of the Korean Society for Heat Treatment
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    • v.37 no.4
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    • pp.182-187
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    • 2024
  • To improve and control the mechanical properties of low alloy steel, the influence of quenching and tempering process conditions was investigated. In the case of quenching heat treatment, a comparison was made between the conventional method of heating to the austenite region followed by single quenching and a method involving double quenching, followed by high-temperature tempering. It was observed that specimens subjected to double quenching exhibited significantly finer tempered microstructures compared to those subjected to conventional quenching, resulting in noticeably higher hardness. Additionally, a study was conducted to investigate the variation in hardness with changes in tempering temperature and time after the same conventional quenching treatment. As expected, an increase in tempering temperature or time led to a decrease in hardness, and the correlation between hardness and the Hollomon-Jeffe Parameter was confirmed. It was also observed that during high-temperature tempering, the size of carbides significantly increased.

Effect of Alloying Elements and Heat Treatment Temperatures on the Retained Austenite of Austempered Ductile iron (오스템퍼드구상흑연주철(球牀黑鉛鑄鐵)의 잔류(殘留)오스테나이트 조직(組織)에 미치는 합금원소(合金元素) 및 열처리온도(熱處理溫度)의 영향(影響)에 관한 연구(硏究))

  • Kim, Deog-Ryul;Cheon, Byung-Wook;Kim, Chang- Gue;Choi, Chang-Ock
    • Journal of Korea Foundry Society
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    • v.13 no.1
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    • pp.50-61
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    • 1993
  • Retained austenite in matrix of austempered ductile iron has been well-known as a parameter in controlling mechanical properties, but investigation to obtain quantitative relationship with mechanical properties lack. Therefore, this study executed austempering treatment at various temperatures on ductile iron alloyed with Mo, Ni, Cu. In consequence, microstructure of retained austenite transformed coarse, and quantity increased according as austempering temperature increased. After heat-treatment, microstructure of specimen alloyed with Ni was fine, and toughness improved. At austempering temperature up to $400^{\circ}C$, carbide precipitation started in retained austenite. In consequence, afforded cause of hardness increase, a lot of increase did not arise for coarse structure.

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Effects of Short-term Acute Heat Stress on Physiological Responses and Heat Shock Proteins of Hanwoo Steer (Korean Cattle)

  • Baek, Youl-Chang;Kim, Minseok;Jeong, Jin-Young;Oh, Young-Kyoon;Lee, Sung-Dae;Lee, Yoo-Kyung;Ji, Sang-Yun;Choi, Hyuck
    • Journal of Animal Reproduction and Biotechnology
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    • v.34 no.3
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    • pp.173-182
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    • 2019
  • This study was performed to evaluate the effect of heat stress on the status of physiological responses, blood parameter, serum T3 and cortisol, and heat shock proteins (HSP 27, 70, and 90) of Hanwoo cattle. Six Hanwoo steers (242.8 ± 7.2 kg of BW) were housed in the climate-controlled respiration chambers. The experiment consisted of 7 days (control; 0 day) at thermoneutral (air temperature (Ta) of 15℃ and relative humidity (RH) of 60%; temperature-humidity index (THI) = 64), and by 3 and 6 days (treatment groups) at heat stress (Ta of 35℃ and RH of 60%; THI = 87). Body temperature of each parts (frank, rump, perineum and foot) and rectal temperature elevated in heat stress groups (3 days and 6 days) than the control group (0 day). Respiration rates increased in 3 days and 6 days (88.5 ± 0.96 bpm and 86.3 ± 0.63 bpm, respectively) from 0 days (39.5 ± 0.65 bpm). Feed intake significantly decreased in heat stress groups (3 days and 6 days, 3.7 ± 0.14 kg and 4.0 ± 0.15 kg, respectively) than the control group (0 day, 5.0 ± 0.00 kg). In addition, final BW significantly decreased in heat stress groups (3 days and 6 days, 211.8 ± 4.75 kg and 215.5 ± 3.50 kg, respectively) than the control group (0 day, 240.0 ± 25.00 kg). However, heat stress has no significant effect on blood parameter, serum T3 and cortisol. Nevertheless, heat stress increased HSPs mRNA expression in liver tissue, and serum concentration of HSPs. Despite Hanwoo cattle may have high adaptive ability to heat stress, our results suggested that heat stress directly effect on body temperature and respiration rate as well as serum and tissue HSPs. Therefore, we are recommended that HSPs could be the most appropriate indicators of Hanwoo cattle response to heat stress.