• Journal of the Korean Society for Nondestructive Testing
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• v.33 no.2
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• pp.193-197
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• 2013

In this study, ultrasonic nonlinear characteristics in the heat-treated aluminum alloy have been evaluated. The nonlinearity of ultrasonic wave has been measured as the acoustic nonlinear parameter ${\beta}$, depending upon the amplitude ratio of the second-order harmonic and the fundamental frequency component of ultrasonic wave propagating through the materials. The parameter ${\beta}$ measurement has been carried out with the reflected signals from the back-wall of specimens at the same plane using the contact-type transducers. The heat-treatment, aging, has been achieved at $300^{\circ}C$ for various durations in the range of 1 to 50 hours. The tensile strength and elongation are obtained by the tensile test and then compared with the parameter ${\beta}$. There is a peak of the acoustic nonlinear parameter ${\beta}$ on 5 hours aging and the ${\beta}$ decreases thereafter, exhibiting closed relations with tensile strength and elongation. Also, the heat-treatment time showing peak in the parameter ${\beta}$ was identical to that showing severe change in the ${\sigma}-{\varepsilon}$ curve. These results suggest that the acoustic nonlinear parameter ${\beta}$ can be used for monitoring the strength variations with aging of aluminum alloys.

• Journal of the Korean Society for Heat Treatment
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• v.7 no.3
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• pp.155-159
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• 1994

As Cr-Mo-V steels have excellent mechanical and creep properties at elevated temperatures, they are extensively used in power plants. However, the steam turbine components are supposed to have suffered material degradation during long-term service at elevated tenperatures. Many efforts have been made to assess the safety and residual life of these components by means of non-destructive methods such as plastic replication, hardness and electric resistance techniques. Recently, a parameter correlating hardness changes during long-term heating to those during creep was introduced and it was named 'G parameter'. The electric resistivity as well as hardness are affected by damage accumulation, but there have been no efforts to correlate G parameter to resistivity changes. In this study, relationship between G parameter and changes in electric resistivity was investigated using artificially aged Cr-Mo-V steel. It is well understood that G parameter can be applied to electric: resistance techmique.

• Journal of Industrial Technology
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• v.18
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• pp.203-208
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• 1998

Fatigue tests were performed to examine the 4 parameter method for specimens prepared by various heat treatment which resulted in different mechanical properties. Obtained main results are as follows. (1) Samples treated by austempering did not show the expected improvement of fatigue limit although hardness and strength increased. This is attributed to the fact that defect sensitivities of materials increase as increasing of hardness and tensile strength, it is also shown that the graphites acting as stress concentration place become larger by austempering heat treatment than by normal annealing. (2) It is very reasonable to predict the fatigue limit of ductile irons with 4 parameter method based on ${\sigma}_{TS}$, $H_v$, ${\Delta}K_{th}$ and ${\sqrt{area}}_{max}$. (3) The half-austempering treatment appeared to be more useful than the full-austempering method to improve the fatigue limit in the spheroidal graphite cast iron with multi defective material.

• Journal of Ocean Engineering and Technology
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• v.23 no.6
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• pp.105-110
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• 2009

The objective of this paper is to investigate the statistical properties of Vickers hardness (HV) for friction welded parts in a Ni-based super alloy (Alloy718). In the case of post weld heat treatment (PWHT) parts, hardness tests were repeated for three different applied loads, 100, 200, and 300 g, with a duration time of 10 seconds. The arithmetic means of the Vickers hardness in heat affected zone (HAZ) materials were smaller than those of the base metal (BM) in all of the applied loads. The coefficient of variation (COV) for the BM and HAZ decreased by increasing the applied load. The probability distribution of the Vickers hardness followed the Weibull distribution well. The distribution of the Vickers hardness was not found to be symmetric. The shape parameter and scale parameter increased by increasing the applied load at both the BM and HAZ.

• Journal of the Korean Applied Science and Technology
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• v.33 no.3
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• pp.411-420
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• 2016

The objective of this study was to determine the effect of drinking water containing trimethyl glycine or ascorbic acid on growth performance and blood parameter profiles of duck exposed to scorching heat stress. A total of 480 ducks were randomly assigned to the following eight experiment groups for 42 days : control group C with general water, treatment group 1 (T1) with drinking water containing 100 ppm ascorbic acid, treatment group 2 (T2) with drinking water containing 200 ppm ascorbic acid, treatment group 3 (T3) with drinking water containing 300 ppm ascorbic acid, treatment group 4 (T4) with drinking water containing 400 ppm trimethyl glycine, treatment group 5 (T5) with drinking water containing 800 ppm trimethyl glycine, treatment group 6 (T6) with drinking water containing 1,200 ppm trimethyl glycine, treatment group 7 (T7) with electrolytes of KCl (0.5%) + $NaHCO_3$ (1.0%)+NaCl (0.5%). Our results revealed that the body weights and feed intakes of treatment groups, especially T3 and T6, were increased compared to the control group, where as the feed conversion ratios of treatment groups were decreased (p<0.05). Blood levels of total cholesterol, triglyceride, LDL-C, glucose, AST, ALT and pH in treatment groups were lower compared to those in the control group (p<0.05). Blood levels of red blood cell, platelets profiles, electrolyte and gas in treatment groups were higher compared to those of the control group (p<0.05).

• Journal of the Korean Society for Precision Engineering
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• v.20 no.7
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• pp.26-35
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• 2003

This study explains the effects of lubricant and surface treatment on hot forging die life. The mechanical and thermal load, and thermal softening which is happened by the high temperature of die, in hot and warm forging, cause die wear, heat checking and plastic deformation, etc. This study is fur the effects of solid lubricants and surface treatment condition for hot forging die. Because cooling effect and low friction are essential to the long life of dies, optimal surface treatment and lubricant are very important to improve die life for hot forging process. The main factors, which affect die hardness and heat transfer, are surface treatments and lubricants, which are related to thermal diffusion coefficient and heat transfer coefficient, etc. For verifying these effects, experiments are performed for hot ring compression test and heat transfer coefficient in various conditions as like different initial billet temperatures and different loads. The effects of lubricant and surface treatment for hot forging die life are explained by their thermal characteristics. The new developed technique in this study for predicting tool life can give more feasible means to improve the tool life in hot forging process.

• Journal of the Korean Society for Heat Treatment
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• v.35 no.5
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• pp.239-245
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• 2022

The purpose of this study is to evaluate the degree of microstructural change of materials using ultrasonic nonlinear parameters. For microstructure change, isothermal heat-treated ferritic 2.25Cr steel and low-cycle fatigue-damage copper alloy were prepared. The variation in ultrasonic nonlinearity was analyzed and evaluated through changes in hardness, ductile-brittle transition temperature, electron microscopy, and X-ray diffraction tests. Ultrasonic nonlinearity of 2.25Cr steel increased rapidly during the first 1,000 hours of deterioration and then gradually increased thereafter. The variation in non-linear parameters was shown to be coarsening of carbides and an increase in the volume fraction of stable M6C carbides during heat treatment. Due to the low-cycle fatigue deformation of oxygen-free copper, the dislocation that causes lattice deformation developed in the material, distorting the propagating ultrasonic waves, and causing an increase in the ultrasonic nonlinear parameters.

• Proceedings of the KSME Conference
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• 2007.05a
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• pp.683-688
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• 2007

Surface heat treatment of SM45C round bar by diode laser was simulated to find it's condition by using commercial finite element code MARC. Due to axisymmetric geometry, a quarter of model for SM45C round bar was considered and user subroutines were applied to boundary condition for the heat transfer. Material properties such as conductivity, specific heat and mass density were given as a function of temperature. Rotation speed of round bar and feed rate of beam were considered to design heat source model. Shape parameter values of heat source were determined by beam profile. As results, Three dimensional heat source model for diode laser beam conditions of surface hardening has been designed by the comparison between the finite element analysis results and experimental data on SM45C round bar. Diode laser surface hardening for SM45C round bar was successfully simulated and it should be useful to determine optimal heat treatment condition.

• Journal of the Korean Society for Heat Treatment
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• v.31 no.1
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• pp.12-17
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• 2018

We investigated the corrosion behavior of commercially pure cold working processed (CP)-Ti with coarse-grained (CG) microstructure heat-treated at $400^{\circ}C$ and $600^{\circ}C$, respectively. It is observed that corrosion resistance of as-received CP-Ti heat-treated at $400^{\circ}C$, at which recrystallization proceeds, is largely improved. Interestingly, the mechanical property of CP-Ti sample at $400^{\circ}C$ was scarcely deteriorated. It is attributed to the decrease of the defects such as strain variance and dislocation density. On the other hand, the annealing treatment at $600^{\circ}C$ of CP-Ti plate causes to grain growth with the noticeable reduction of mechanical property. Hence, it is considered that defect density such as strain and dislocation density is important microstructural parameter for the improvement of corrosion resistance. The introduction of proper annealing treatment can help to improve corrosion resistance without scarifying mechanical property of CP-Ti.

• Journal of Powder Materials
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• v.11 no.1
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• pp.22-27
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• 2004

The Indium Tin Oxide(ITO) nano powders were prepared by spray drying and heat treatment process. The liquid solution dissolved Indium and Tin salts was first spray dried to prepare chemically homogeneous recursor powders at the optimum spray drying conditions. Subsequently, the precursor powders were subjected to eat treatment process. The nano size ITO powders was synthesized from the previous precursor powders and the npuities also were decreased with increasing heat treatment temperature. Furthermore, the lattice parameter of TO nano powders was increased by doping Tin into Indium with increasing heat treatment temperature. The par icle size of the resultant ITO powders was about 20∼50nm and chemical composition was composed of In:Sn =86:10 wt.％ at 80$0^{\circ}C$.