• Title/Summary/Keyword: heat treatment parameter

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Effect of Photosensitive Carbon Nanotube Paste on Field Emission Properties (감광성 탄소나노튜브 페이스트의 조성과 열처리가 전계방출 특성에 미치는 영향)

  • Oh, Jeong-Seob;Kim, Dae-Jun;Jeong, Jin-Woo;Song, Yoon-Ho;Cho, Young-Rae
    • Korean Journal of Materials Research
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    • v.16 no.9
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    • pp.550-556
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    • 2006
  • Photosensitive carbon nanotube (CNT) pastes are explored to develop a CNT field emitter for field emission display (FED) application. We formulated a photosensitive paste including multi-walled CNTs (MWNTs) for screen printing. The photosensitive CNT paste was synthesized by mixing of MWNTs, inorganic fillers (nano metal), organic vehicle, monomers and photo initiator. The CNT paste films were patterned by using backside exposure technique. The CNTs were strongly fixed on a cathode by formation of carbon residue during firing process. For the CNT emitters, current-voltage(I-V) characteristics and images of field emission were evaluated. The emission properties of CNT emitters are dependent on the paste composition. A turn-on electric field for the CNT field emitters is measured to be 1 V/$\mu$m. Additionally, the effect of heat treatment parameter on field emission properties was discussed. The newly formulated photosensitive CNT paste can be potentially applicable to highly reliable CNT field emitters.

Synthesis and Characterization of ZnAl2O4 Nanopowders by a Reverse Micelle Processing

  • Hoon, Son-Jung;Sohn, Jeongho;Shin, Hyung-Sup;Bae, Dong-Sik
    • Korean Journal of Materials Research
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    • v.25 no.11
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    • pp.598-601
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    • 2015
  • Using reverse micelle processing, $ZnAl_2O_4$ nanopowders were synthesized from a mixed precursor(consisting of $Zn(NO_3)_2$ and $Al(NO_3)_3$). The $ZnAl_2O_4$ was prepared by mixing the aqueous solution at a molar ratio of Zn : Al = 1 : 2. The average size and distribution of the synthesized powders with heat treatment at $600^{\circ}C$ for 2 h were in the range of 10-20 nm and narrow, respectively. The average size of the synthesized powders increased with increasing water to surfactant molar ratio. The XRD diffraction patterns show that the phase of $ZnAl_2O_4$ was spinel(JCPDS No. 05-0669). The synthesized and calcined powders were characterized using a thermogravimetric - differential scanning calorimeter(TG-DSC), X-ray diffraction analysis (XRD), and high resolution transmission electron microscopy(HRTEM). The effects of the synthesis parameter, such as the molar ratio of water to surfactant, are discussed.

Study on crystal texture of PIT processed Bi-2223 multi-filamentary tape (PIT 공정으로 제조한 Bi-2223 다심 고온 초전도 선재의 결정 배향성에 관한 연구)

  • Choi, J.K.;Oh, S.S.;Ha, H.S.;Yang, J.S.;Yun, J.K.;Lee, N.J.;Ha, D.W.;Kwan, Y.K.
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2002.04a
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    • pp.59-63
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    • 2002
  • The purpose of this paper is to investigate the crystal texture of the 2223 phase and its relationship with PIT processing parameter. Ag-sheathed Bi-2223 multi-filament tapes were prepared by changing rolling reduction ratio. We analysed the degree of texture for 2223 phase after heat-treatment. According to X-ray pole-figure, the texture of the filaments located near surface and center were not so different each other for all rolling conditions. we found a little higher degree of texture for 60% rolling reduction. But its difference is not so high compared with those tapes with a lower rolling reduction ratio. Reaction induced texturing seemed to contribute with a large portion under present condition.

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Annealing Effect of Co/Pd Multilayers on Magnetic Properties During Interdifusion

  • Kim, Jai-Young;Jan E. Evetts
    • Journal of Magnetics
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    • v.2 no.4
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    • pp.147-156
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    • 1997
  • An artificially modulated magnetic Co/Pd multilayer is one of the promising candidates for high density magneto-optic (MO) recording media, due to a large Kerr rotation angle in the wavelength of a blue laser beam. However, since multilayer structure, as well as amorphous structure, is a non-equilibrium state in terms of free energy and a MO recording technology is a kind of thermal recording which is conducted around Curie temperature (Tc) of the recording media, when the Co/Pd mulilayer is used for the MO recording media, changes in the magnetic properties are occurred as the amorphous structure do. Therefore, the assessment of the magnetic properties in the Co/Pd multilayer during interdiffusion is crucially important both for basic research and applications. As the parameter of the magnetic properties in this research, saturation magnetization and perpendicular magnetic anisotropy energy of the Co/Pd multilayer are measured in terms of Ar sputtering pressure and heat treatment temperature. Form the results of the research, we find out that the magnetic exchange energy between Co and Pd sublayers strongly affects the changes in the magnetic properties of the Co/Pd multilayers during the interdiffusion in ferromagnetic state. This discovery will provide the understanding of the magnetic exchange energy in the Co/Pd multilayer structure and suggest the operating temperature range for MO recording in the Co/Pd multilayer for the basic research and applications, respectively.

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Effect of the Raw Material and Coating Process Conditions on the Densification of 8 wt% Y2O3-ZrO2 Thermal Barrier Coating by Atmospheric Plasma Spray

  • Oh, Yoon-Suk;Kim, Seong-Won;Lee, Sung-Min;Kim, Hyung-Tae;Kim, Min-Sik;Moon, Heung-Soo
    • Journal of the Korean Ceramic Society
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    • v.53 no.6
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    • pp.628-634
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    • 2016
  • The 8 wt% yttria($Y_2O_3$) stabilized zirconia ($ZrO_2$), 8YSZ, a typical thermal barrier coating (TBC) for turbine systems, was fabricated under different starting powder conditions and coating parameters by atmospheric plasma spray (APS) coating process. Four different starting powders were prepared by conventional spray dry method with different additive and process parameter conditions. As a result, large- and small-size spherical-type particles and Donut-type particles were obtained. Dense structure of 8YSZ coating was produced when small size spherical-type or Donut-type particles were used. On the other hand, 8YSZ coating with a porous structure was formed from large-size spherical-type particles. Furthermore, a segmented coating structure with vertical cracks was observed after post heat treatment on the surface of dense structured coating by argon plasma flame at an appropriate gun distance and power condition.

Effective Interdiffusion of Co/Pd multilayers

  • Kim, Jai-Young;Jan E. Evetts
    • Journal of Magnetics
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    • v.2 no.3
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    • pp.86-92
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    • 1997
  • An artificially modulated magnetic Co/Pd multilayer is one of the promising candidates for high density magneto-optic (MO) recording media in the wavelength of a blue laser beam, due to large Kerr rotation angle. However, since the Co/Pd multilayer is a non-equilibrium state in terms of free energy and MO recording is a kind of thermal recording which is conducted around Curie temperature (Tc) of the recording media, the assessment of the thermal stability in the Co/Pd multilayer is crucially important both for basic research and applications. As the parameter of the thermal stability in this research, effective interdiffusion coefficients (Deff) perpendicular to the interface of the Co/Pd multilayers are measured in terms of Ar sputtering pressure and heat treatment temperature. From the results of the research, we find out that the magnetic exchange energy between Co and Pd sublayers strongly affects Deff of the Co/Pd multilayers. This discovery will provide the understanding of the magnetic exchange energy in the effective interdiffusion process of a magnetic multilayer structure and suggest the operating temperature range for MO recording in the Co/Pd multilayer for the basic research and applications, respectively.

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Crack-Healing Behavior of $Al_2O_3$ Ceramics for Textile Machinery (섬유기기용 $Al_2O_3$계 세라믹스의 균열치유거동)

  • An, B.G.;Kim, M.K.;Ahn, S.H.;Kim, J.W.;Park, I.D.;Nam, K.W.
    • Journal of Power System Engineering
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    • v.10 no.1
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    • pp.60-64
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    • 2006
  • Alumina ceramic for textile machinery was sintered and subjected to three-point bending. A semicircular surface crack was made on each sample. Crack-healing behavior was systematically studied, as a function of crack-healing temperature and crack size. The bending strength and fracture toughness of the crack-healed sample from $1200^{\circ}C\;to\;1400^{\circ}C$ were investigated. A statistical approach based on Weibull distribution was applied to the test data to evaluate the dispersion in the fracture toughness. Alumina ceramic for textile machinery have the ability to heal after cracking, from over $1300^{\circ}C$. The material can completely heal a $65{\mu}m$ diameter semielliptical crack. The fracture toughness could be explained by 2-parameter Weibull distribution.

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A Case Study on the Reduction of Noise and Vibration at the Backpass Heat Surface in the Power Plant Boiler (300MW급 증기터빈의 베어링 윤활유 온도조정에 의한 오일휩 제거방법에 관한 연구)

  • Hwang, Dal-Yeon;Moon, Seung-Jae;Lee, Jae-Heon
    • Plant Journal
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    • v.4 no.4
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    • pp.56-61
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    • 2008
  • The phenomena of oil whip in steam turbines take place for the unbalance force between a rotor shaft and bearing oil film. The several parameters that affect onset of oil whip have been well known. However, the major parameter of oil whip is shaft mis-alinement. A oil whip causes the high vibration and the shutdown of rotor system. We mostly stop the steam turbine to adjust a shaft re-alinement concerning oil whip. In this case, it needs many costs for maintenance and long shutdown times. In this study, we study and observe the oil whip of the 300MW steam turbine in many years and we conduct the field test for another steam turbine for reducing vibration from oil whip. The results of this study are that a oil whip takes place with a particular rotating speed or a particular turbine output and the oil temperature change is a very effective method for on-line oil whip treatment.

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Choline chloride-Glycerol (1:2 mol) as draw solution in forward osmosis for dewatering purpose

  • Dutta, Supritam;Dave, Pragnesh;Nath, Kaushik
    • Membrane and Water Treatment
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    • v.13 no.2
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    • pp.63-72
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    • 2022
  • Choline chloride-glycerol (1:2 mol), a natural deep eutectic solvent (NADES) is examined as a draw solution in forward osmosis (FO) for dewatering application. The NADES is easy to prepare, low in toxicity and environmentally benign. A polyamide thin film composite membrane was used. Characterization of the membrane confirmed porous membrane structure with good hydrophilicity and a low structural parameter (722 ㎛) suitable for FO application. A dilute solution of 20% (v/v) NADES was enough to generate moderate water flux (14.98 L m-2h-1) with relatively low reverse solute flux (0.125 g m-2h-1) with deionized water feed. Application in dewatering industrial wastewater feed showed reasonably good water flux (11.9 L m-2h-1) which could be maintained by controlling the external concentration polarization and fouling/scaling mitigation via simple periodic deionized water wash. In another application, clarified sugarcane juice could be successfully concentrated. Recovery of the draw solute was accomplished easily by chilling utilizing thermo responsive phase transition property of NADES. This study established that low concentration NADES can be a viable alternative as a draw solute for dewatering of wastewater and other heat sensitive applications along with a simple recovery process.

Effects of Sprinkler and Fan Cooling System in Loose Barn on the Physiological Parameter and Milk Productivity in Holstein Cows During Summer (개방식우사내 Fan과 Sprinkler설치가 착유우의 생리적 변화 및 유생산성에 미치는 영향)

  • 정태영;이현민;김종민;김동일;이연섭;이인형
    • Journal of Animal Environmental Science
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    • v.2 no.1
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    • pp.41-52
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    • 1996
  • This experiment was carried out to study the effect of sprinkler and fan cooling system on the physiological parameter, milk production and milk composition for Holstein cows in hot, humid climates. Thirty cows were assigned to one of two sections of open-sided loose barn. Water nozzles of sprinkler system were spaced in line at 1.2m intervals. Forced air was provided by 85cm diameter fans at rate of 3.4㎥/sec. The results obtained from these experiments are as follows: 1. There was no significant difference in meteorological data between control and fan + sprinkler cooling system(treatment group). 2. Skin temperature and rectal temperature of the treatment group were significantly lower than those of the control group (32.96 : 39.53$^{\circ}C$ vs 34.02 : 41.21$^{\circ}C$ respectively) (P<0.05). 3. Serum cortisol concentration of the treatment group(0.90$\mu\textrm{g}$/dL) was lower than that of control group(1.44$\mu\textrm{g}$/dL)(P<0.05). 4. Milk production of cows cooled with a sprinkler and fan cooling system was significantly higher than that of no cooling system (P<0.0l). 5. Lactose, protein and solid-not-fat content of milk were not changed by the treatments. Milk fat content of the control(3.23%) was low compared with the treatment group(3.38%). Somatic cell count was reduced by 26.63% in the treatment. The results indicate that a sprinkler and fan cooling systems can provide an effective means to relieve heat stress and enhance productivity of lactating Holstein cows during hot and humid summer season.

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