• Title/Summary/Keyword: heat aging test

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Arrhenius Kinetic Constants Analysis of BKNO3 under Accelerated Aging (가속노화에 따른 BKNO3의 아레니우스 동역학 상수 분석)

  • Jang, Seung-gyo;Kim, Jun-hyung;Ryu, Byung-tae;Hwang, Jung-min
    • Journal of the Korean Society of Propulsion Engineers
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    • v.20 no.4
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    • pp.34-39
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    • 2016
  • Arrhenius kinetic constants, the activation energy and the pre-exponential factor, of energetic material $BKNO_3$ are estimated using Differential Scanning Calorimetry (DSC). Different from the conventional way, the activation energy was estimated more precisely through DSC aging trial, and the consumed fraction by heat was calculated by comparing the integration of heat flow. We suggested the condition of accelerated aging test for the energetic material $BKNO_3$ and reconsidered the meaning of the thermal accelerated aging.

Changes in Insulation Performance of Organic Insulating Materials for Building Construction by Accelerated Durability Test Conditions (가속내구성 조건에 따른 건축용 유기계 단열재의 단열성능 변화)

  • Lim, Soon-Hyun;Lee, Gun-Cheol
    • Journal of the Korea Institute of Building Construction
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    • v.16 no.6
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    • pp.595-601
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    • 2016
  • The insulation performance of the insulation currently used in building structures is reflected only during design based on initial performance and the reduction in heat insulation performance due to the degradation of long-term durability is not reflected. This study reviewed the degradation of heat insulation performance due to the durability degradation of insulating materials through the accelerated durability test. The study findings showed that the foamed polystyrene insulation bead method did not show performance degradation due to aging in the standard environmental condition and laboratory accelerated test condition but the performance is degraded in the freeze-thaw test condition. On the other hand, in the case of the extrusion method, the degradation of the heat insulation performance was less in the freeze-thaw test condition, but the rapid performance degradation was caused by the release of the internal gas at the beginning of aging. In addition, the hard polyurethane foam insulation showed better initial insulation performance than other insulation materials, but the performance was found to be degraded somewhat under laboratory accelerated test conditions and freeze-thaw test conditions.

The Study of Restoration Technique of Wax-Treated Volume for the Annals of the Joseon Dynasty (III) -Evaluation of Durability of Korean Traditional Paper using Moist-heat Aging Treatment- (조선왕조실록 밀랍본 복원기술 연구(제3보) -습열열화처리를 이용한 복원용 한지의 내구성 평가-)

  • Jeong, Seon-Hwa;Jeong, Sun-Young;Seo, Jin-Ho;Jeong, So-Young
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.45 no.5
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    • pp.49-55
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    • 2013
  • To explore the paper materials for restoration of the Annals of the Joseon Dyansty, durability of the three type of the traditional Korean Papers were estimated in this study, through moist heat artificial aging test. Three types(D, F, and G) which showed the best preservation performance in dry heat and UV treatment in the previous study were selected and artificial accelerated aging treatment with moist-heat process was conducted; the viscosity change rate was D>G>F; folding endurance G>D>F; $L^*$ value F>D>G; $a^*$ and $b^*$ change rate D>G>F; brightness decrease rate D>G>F, suggesting paper F showed the least change rate in physical/optical properties. Also the CLSM image observation showed fair coherence among fibers and confirmed paper mulberry. And in FDI extraction from each sample, paper F showed the highest value. Overall, paper F (traditional glossy paper) showed the highest stability against thermal treatment. It confirms that paper F is suitable as restoration paper for tributary remains including the annals of the Joseon Dynasty for its steady strength/viscosity decrease rate and color change rate.

A Study on the Degradation of Mechanical Properties in High Nitrogen Steel Following Heat Treatments and Welding (고질소계 강의 열처리재 및 용접부의 기계적성질 저하에 관한 연구)

  • 권일현;윤재영;정세희
    • Journal of Welding and Joining
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    • v.16 no.3
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    • pp.121-128
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    • 1998
  • The degradation of mechanical properties in the high nitrogen steel HN3 developed for nuclear fusion reactor has been evaluated quantitatively using the small punch(SP) test, X-ray diffraction (XRD) analysis has also been conducted to identify carbides or nitrides precipitated on grain boundaries of the heat treated samples. Mechanical properties of the steel HN3 significantly decreased with increasing heat treatment time and temperature or with decreasing testing temperature. Combination of XRD and metallurgical observation, revealed that the material degradation in the thermally aged steel was caused by precipitation of carbides on the grain boundaries. While the weld metal showed the lowest mechanical properties among various microstructures in GTA weldments. By combining SP test and XRD analysis, cryogenic fracture behaviors and aging degradation for high nitrogen steel could be successfully evaluated in nondestructive manner.

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Design of LED TV Multi Test Unit (LED TV 통합검사유닛의 설계)

  • Kouh, Hoon-Joon
    • Journal of Digital Convergence
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    • v.10 no.4
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    • pp.37-43
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    • 2012
  • LED TV integration test unit are the equipment for testing LED BLU as LED BLU's operation, error check, AGING work. The previous test unit were inconvenient because it must change test unit in production line according to LCD's kind and size. This paper develops by integration style test unit that can accommodate various LED TV BLU model of 32 ~ 52 inch that is not one LED TV BLU model. We make that output current is various to dimension of 80 ~ 215 mA. We make functions that are LED BLU state check, Diming and heat occurrence mitigation. Also we develop firmware program and that the program can be upgraded and that can support new panel.

A Study on Degradation Behavior of 1Cr-1Mo-0.25V Steel (1Cr-1Mo-0.25V 강의 열화거동에 관한 연구)

  • 석창성;구재민;김동중;안하늘;박은수
    • Journal of the Korean Society of Safety
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    • v.15 no.4
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    • pp.8-14
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    • 2000
  • The remaining life estimation for the aged components in power plants as well as chemical plants are very important because mechanical properties of the components are degraded with time of service exposure in the high temperature. Since it is difficult to take specimens from the operating components to evaluate mechanical properties of components, accelerated aging technique are needed to estimate and analyse the material degradation. In the this study, test materials with 4 different degradation levels were prepared by isothermal aging heat treatment at $630^{\circ}C$. And tensile test, $k_{IC}$ test, hardness test and Scanning Electron Microscope analysis were performed in order to evaluate the degradation of 1Cr-1Mo-0.25V steels.

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The Effect of Solution Heat Treatment and Aging Treatment on the Mechanical Properties of Backward Extruded A6061 Alloy for Pressure Vessels (고압용기로 사용되는 후방압출된 알루미늄 6061합금의 기계적 특성에 미치는 용체화처리 및 시효처리의 영향)

  • Kwon, Eui Pyo;Woo, Kee Do;Moon, Min Seok;Kang, Duck Soo;Nam, Gung Cheon;Yoo, Gye Hyoung
    • Korean Journal of Metals and Materials
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    • v.47 no.3
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    • pp.175-181
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    • 2009
  • Mechanical properties and precipitation behavior of backward extruded 6061 Al alloy for pressure vessel were investigated using tensile test, transmission electron microscopy (TEM) and differential scanning calorimeter (DSC). In this study, solution heat treatment (SHT) was performed at $535^{\circ}C$ for 30~90 min and aging treatment was conducted at 177 and $190^{\circ}C$ for 1~7 h. Maximum tensile strength of $36.6kgf/mm^2$ and yield strength of $33.29kgf/mm^2$ were achieved at the aging time of 5 h at $190^{\circ}C$. TEM observation showed that fine needle-like ${\beta}^{{\prime}{\prime}}$ phase which has 35~45 nm of length was uniformly distributed in the aged 6061 Al alloy specimen. From tensile test, TEM and DSC analysis, it is expected that aging time of 2~5 h at $190^{\circ}C$ is suitable for the extruded A6061 used as pressure vessels.

Small Punch Test for the Evaluation of Thermal Aging Embrittlement of CF8 Duplex Stainless Steel

  • Cheon, Jin-Sik;Kim, In-Sup;Jang, Jae-Gyoo;Kim, Joon-Gu
    • Proceedings of the Korean Nuclear Society Conference
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    • 1996.05c
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    • pp.79-84
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    • 1996
  • Small punch test was performed on CF8 duplex stainless steel aged at 370 and 400$^{\circ}C$ up to 5,000 h to evaluate the degree of the thermal aging embrittlement. At room temperature, the SP load-displacement curve was in a similar shape to those of ferritic steels and had a good reproducibility in spite of two-phase structure. The aging heat treatment resulted in a slight increase of the yield strength. As test temperature was lowered, the SP load showed a sudden drop followed by serrations before the SP specimen was fractured, resulting from the cracking of ferrite phase. The extent of thermal embrittlement was assessed in terms of the SP energy. Aging treatment at higher temperature led to a larger shift in the transition temperature and the corresponding change in the fracture mode. The main cause of the degradation was the embrittlement of ferrite phase. Additionally the phase boundary separation profoundly contributed to the degradation of the specimen aged at 400$^{\circ}C$.

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Effects of Rare Earth Metals Addition and Aging Treatment on the Corrosion Resistance and Mechanical Properties of Super Duplex Stainless Steels

  • 박용수;김순태;이인성;송치복
    • Transactions of Materials Processing
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    • v.8 no.3
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    • pp.309-309
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    • 1999
  • Effects of rare earth metals addition and aging treatment on corrosion resistance and mechanical properties of super duplex stainless steels were investigated using optical/SEM/TEM metallographic examination, an X-ray diffraction test, a potentiodynamic anodic polarization test and a tensile test. The performance of the experimental alloy with 0.32% REM addition was compared with commercial super duplex stainless steel such as SAF 2507 when they were exposed to solution annealing heat treatment and aging treatment. The corrosion resistance in CF environments and mechanical properties of the experimental alloy were found superior to those of the commercial duplex stainless steel. The REM with larger atomic radii than those of Cr, Mo and W may fill vacancies inside the matrix and around the grain boundaries, retarding formation of harmful intermetallic σ and χ phases. In addition, fine REM oxides/oxy-sulfides (1-3㎛) seemed to enhance the retardation effects. With REM additions, strength and ductility increased due to the phase and grain refinement caused by fine REM oxides and oxy-sulfides.

Analysis of Photovoltaic module's Phenomena of aging with Acceleration Test (외부환경적 가속시혐에 의한 PV모듈의 열화성능 분석)

  • Kang, Gi-Hwan;Kim, Kyung-Soo;Park, Chi-Hong;Yu, Gwon-Jong;Ahn, Hyung-Gun;Han, Deuk-Young
    • Proceedings of the KIEE Conference
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    • 2006.07b
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    • pp.1151-1152
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    • 2006
  • In this paper, we examined 10 domestic samples of three different model using thermal, humidity freeze, thermal-endurance and damp heat test under IEC61215 photovoltaic module environmental endurance test condition. Three was almost no changes on power generation. Insulation resistance capacity was much higher than judgement standard but, showed unstable results depending on environmental test items. On external appearance test, there were two models which showed bubble, humidity penetration, seal melted frame phenomenon. From this results, the degree of aging under the external environment is a main cause that shortens photovoltaic module life time. So it is considered that the efforts for finding optimum condition of manufacturing process should be needed.

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