• The Korean Journal of Ceramics
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• v.5 no.3
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• pp.260-264
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• 1999

Effect of the particle size of $MgTiO_3$ and $CaTiO_3$ on the microstructural evolution during sintering of $0.93MgTiO_3-0.07CaTiO_3$ system was investigated. Microwave dielectric characteristics of the sintered ceramics were also measured. The microstructural evolutions were explained with an emphasis on the entrapping behavior of $CaTiO_3$ grain into the $MgTiO_3$ grain and were correlated with microwave dielectric characteristics. With an increasing particle size ratio between $CaTiO_3$and $MgTiO_3$, the fraction of entraped $CaTiO_3$ grains increased, which grain growth of $MgTiO_3$were concurrently accelerated due to decreasing drag force of its boundary migration. Besides, $CaTiO_3$-grain entrapment into the $MgTiO_3$grain interior led to decreaseing quality factor values.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2009.10a
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• pp.89-92
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• 2009

As a class of materials, Ni-base superalloys are among the most difficult metal alloys to forge together with refractory metals and cobalt-base superalloys. The mechanical properties of Ni-base superalloys depend very much on grain size and the strengthening phases, $\gamma$' ($Ni_3$(Al,Ti)-type) and $\gamma$".($Ni_3$Nb-type). Especially, the control of grain size remains as a sole means for the control of mechanical properties. The grain size and distribution changes of the wrought superalloys during hot working and heat treatment are mainly controlled by the recrystallization and grain growth behaviors. In this presentation, prediction technology of grain size through the computer-aided process design, and numerical modeling for predicting the microstructure evolution of Ni-base superalloy during hot working were introduced. Also, some case studies were dealt with actual forming processes of Ni-base superalloys.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2007.10a
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• pp.53-56
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• 2007

Computer simulation of microstructure evolution during hot forging process is of great interest in recent years. Recrystallization model and grain growth model which use a phenomenological approach were summarized. For the waspaloy, upsetting process and cogging process were simulated using $DEFORM^{TM}$ and the change in grain size were investigated in each deformation procedure.

• Transactions of Materials Processing
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• v.13 no.3
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• pp.248-252
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• 2004

The mechanical properties of polycrystalline thin-films, critical for Micro-Electro-Mechanical Systems (MEMS) components, are known to have the size effect and the scatter in the length scale of microns by the numbers of intensive investigation by experiments and simulations. So, the consideration of the microstructure is essential to cover these length scale effects. The lattice based stochastic model for the microstructure evolution is used to simulate the actual microstructure, and the fast and reliable algorithm is described in this paper. The kinetics parameters, which are the key parameters for the microstructure evolution based on the nucleation and growth mechanism, are extracted from the given micrograph of a polycrystalline material by an inverse method. And the method is verified by the comparison of the quantitative measures, the number of grains and the grain size distribution, for the actual and simulated microstructures. Finite element mesh is then generated on this lattice based microstructure by the developed code. And the statistical finite element analysis is accomplished for selected microstructure.

• Journal of Korea Foundry Society
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• v.25 no.6
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• pp.249-253
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• 2005

The present study focuses on 7075 aluminum wrought alloy to investigate the potential industrial applications of thixoextrusion process. The microstructural evolution of 7075 aluminum wrought alloy for thixoextrusion has been investigated as a function of isothermal holding temperature and time in the partially remelted semisolid state. The results showed that the liquid fraction increased with increasing isothermal holding temperature and time while the average grain size was inversely proportional to isothermal holding temperature and time up to 5min. However, there was no big change of liquid fraction and average grain size with respect to isothermal holding temperature and time. The important fact that the liquid fraction and average grain size were almost uniform after 5 min holding time is considered very useful for thixoextrusion in terms of process control.

• Transactions of Materials Processing
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• v.9 no.6
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• pp.663-669
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• 2000

A material model has been presented, at the continuum level, for the representation of superplastic deformation coupled with microstructural evolution. The model presented enables the effects of the spatial variation of distributions of grain size to be predicted at the process level. The model has been tested under conditions of both homogeneous and inhomogeneous stress and strain by carrying out detailed comparison of predicted distributions of grain size and their evolutions with experimentally obtained data. Experimental measurements have shown the extent of the spatial variation of the distribution of grain size that exists in the titanium alloy, Ti-6Al-4V. It is shown that whilst not large, the variations in grain size distributions are sufficient to lead to the development of inhomogeneous deformation in test pieces, which ultimately result in localisation of strain and failure.

• Interaction and multiscale mechanics
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• v.2 no.1
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• pp.15-30
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• 2009

The theoretical framework of the interaction fields for multiple scales based on field theory is applied to one-dimensional problem mimicking dislocation substructure sensitive intra-granular inhomogeneity evolution under fatigue of Cu-added steels. Three distinct scale levels corresponding respectively to the orders of (A)dislocation substructures, (B)grain size and (C)grain aggregates are set-up based on FE-RKPM (reproducing kernel particle method) based interpolated strain distribution to obtain the incompatibility term in the interaction field. Comparisons between analytical conditions with and without the interaction, and that among different cell size in the scale A are simulated. The effect of interaction field on the B-scale field evolution is extensively examined. Finer and larger fluctuation is demonstrated to be obtained by taking account of the field interactions. Finer cell size exhibits larger field fluctuation whereas the coarse cell size yields negligible interaction effects.

• Transactions of Materials Processing
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• v.10 no.4
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• pp.338-346
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• 2001

Evaluation of microstructural changes is important for process control during open die forging of heavy ingots. The control of forging parameters, such as shape of the dies, reduction, temperature and sequence of passes, is to maximize the forging effects and to minimize inhomogeneities of mechanical properties. The hot working die steel is produced by using the multistage open die forging. The structure is altered during forging by subsequent Precesses of plastic deformation, recrystallization and grain growth. A numerical analysis using an rigid visco-plastic finite element model was performed to predict microstructural evolution of hot working die steel.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2001.05a
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• pp.131-135
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• 2001

Evaluation of microstructural changes during open die forging of heavy ingots is important for process control. The objective of the control of forging parameters, such as shape of the dies, reduction, temperature and sequence of passes, is to maximize the forging effects md to minimize inhomogeneities of mechanical properties. The hot working die steel is produced by using the multistage open die forging. The structure is altered during forging by subsequent processes of plastic deformation, recrystallization and grain growth. A numerical analysis using an rigid visco-plastic finite element model was performed to predict microstructural evolution of hot working die steel.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2008.10a
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• pp.38-41
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• 2008

To investigate the evolution of microstructure and texture in AZ31 Mg alloy, direct/indirect extrusion process was carried out at $300^{\circ}C$ with various extrusion speeds. The distribution of grain size depends on extrusion method and extrusion speed. More homogeneous grain site can be obtained at higher extrusion speed of indirect extrusion process. Extrusion speed does not affect significantly texture evolution during extrusion process regardless of extrusion method. ODF section is more useful to understand texture evolution during extrusion process compared with pole figure.