• Title/Summary/Keyword: grain direction

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Transmission Electron Microscopy Observation of Twin Variant Selection in Austenitic Twinning-Induced Plasticity Steel

  • Han, Jung-Hoon;Oh, Juhyun;Yoon, Sangmoon;Kim, Yanghoo;Han, Heung Nam;Kim, Miyoung
    • Applied Microscopy
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    • v.46 no.4
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    • pp.238-243
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    • 2016
  • Twinning-induced plasticity (TWIP) steels with the austenite structure containing high manganese exhibit both good strength and excellent formability. Such properties originate from crystallographic slip and mechanical twins produced when the austenite structure is under mechanical stress. There are 12 twin systems, referred to as twin variants, when slip is induced. These twin systems include twin planes and twin directions and play an important role in determining strength and ductility of the material by strongly influencing texture formation of the austenite structure. In the present study, twins produced in a high-Mn TWIP steel as a result of uniaxial tension were observed using a transmission electron microscope; a comparative analysis was performed through interaction energy calculations. Electron diffraction was used to determine the twin system with respect to the uniaxial tension direction in each grain. Both the Schmid factors and interacting energies required for the generation of twins were calculated and subsequently compared with experimental results. This approach demonstrated the possibility of predicting the deformation behavior of the material.

A Study on the Environment Change of Tidal Flat in the Cheonsu Bay Using Remotely Sensed Data (원격탐사 자료를 이용한 천수만 간석지 환경변화에 관한 연구)

  • Jang, Dong-Ho;Chi, Kwang-Hoon;Lee, Hyoun-Young
    • Journal of Environmental Impact Assessment
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    • v.11 no.1
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    • pp.51-66
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    • 2002
  • The purpose of this study is to analyze the geomorphological environment changes of tidal flat in the Cheonsu Bay. Especially, it centers on the changes in the sedimentary environment using remote sensing data. Multi-temporal Landsat data and topographic maps were used in this study. The results are summarized as follows: the tidal flat of Cheonsu Bay changes in many ways depending on the direction of the tidal current. In the neighborhood of Ganwoldo, the scale of the tidal flat has continuously been expanded due to the superiority of sedimentation after a tide embankment was built. When we analyzed the grain size of sediments and implemented in-situ field survey, it was found that the innermost part of the bay consists of a mud flat, with the midway part mixed flat, and the nearest part to the sea sand flat. On the other hand, in the neighborhood of Seomot isle and its beach, sedimentation is superior in the eastern part whereas erosion is superior in the western part. In other words, the western coast of the beach is contacted with the open seas and under much influence of ocean wave. The eastern coast is placed at the entrance of the bay and has sand bar and tidal flat developed due to submarine deposits that are accumulated on the sea floor by the tidal current. In conclusions, remote sensing methods can be effectively applied for quantitative analysis of geomorphological changes in tidal flat, and it is expected that the proposed schemes can be applied to another geomorphological environments such as beach, sand dune, and sand wave.

Electron beam weldability of Niobium (니오븀의 전자빔 용접성)

  • An, Byung-Hun;Yoon, Jong-Won;Kim, Sook-Hwan
    • Laser Solutions
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    • v.11 no.2
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    • pp.15-19
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    • 2008
  • Electron beam (EB) weldability of pure grade Nb sheet was studied. One of Nb sheets was as-annealed and the other was cold rolled. Microstructures, Vickers hardness, and transverse weld tensile test were carried out for the base metal, the heat affected zone (HAZ) and weld metal. In the case of the EB welds made using the annealed Nb sheeet, fine equiaxed grains and coarse grains were dominant at the base metal and the HAZ, respectively, and columnar grains were observed at the weld metal. For the EB welds made using the cold rolled Nb sheet, elongated grains in the rolling direction at the base metal, and the microstructures of the weld metal and the HAZ are similar to those of the EB welds made using the annealed Nb sheet, respectively. For both annealed and cold rolled Nb sheet, the width of the HAZs are unusually wide in spite of using high density heat source, i.e. electron beam, and the grain sizes of both HAZs are similar. When tensile test was carried out using the transverse weld specimens, the failure occurred at the HAZ for both EB welds made using Nb sheets annealed and cold rolled, respectively and the tensile strengths of both specimens were 161MPa. Vickers hardness of EB welds made using annealed Nb was 56-57 Hv at both base metal and weld metal, 52-53 Hv at the HAZ. On the other hand, Vickers hardness of EB welds made using cold rolled Nb was 97-99 Hv at the base metal, but the hardness values of weld metal were similar to those obtained at the weld metal of annealed Nb.

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Effects of Annealing and Neutron Irradiation on Micostructural and Mechanical Properties of High Burn-up Zr Claddings (고연소도 신형 Zr피복관의 미세조직과 기계적 특성에 미치는 열처리 및 중성자 조사의 영향)

  • Baek, Jong Hyuk;Kim, Hyun Gil;Jeong, Yong Hwan
    • Journal of the Korean Society for Heat Treatment
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    • v.17 no.3
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    • pp.151-164
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    • 2004
  • The changes of microstructural and mechanical properties were evaluated for the high burn-up fuel claddings after the neutron irradiation of $1.8{\sim}3.1{\times}10^{20}n/cm^2$ (E>1.0 MEV) in HANARO research reactor. After the irradiation, the spot-type dislocations (a-type dislocations) were easily observed in most claddings, and the density of the dislocations was different depending on the grains and was higher at grain boundaries than within grains. As the final annealing temperature increased, the density of spot-type dislocations increased and the line-type dislocations (c-type dislocations) which was perpendicular to the <0002> direction, appeared sporadically in some claddings. However, the types of precipitates in the fuel claddings after the irradiation were not changed from that in unirradiated claddings. The mechanical properties including the hardness, strength and elongation after the irradiation were changed due to the formation of spot-type dislocations. That is, the increase in hardness and strength as well as the decrease in elongation after the irradiation was occurred simultaneously with increasing the final annealing temperature. Owing to the Nb contribution to the formation of spot-type dislocation during the irradiation, the increase in hardness and strength in higher Nb-contained Zr alloys after the irradiation was higher than that in lower Nb-contained Zr alloys.

Incipient motion criteria of uniform gravel bed under falling spheres in open channel flow

  • Khe, Sok An;Park, Sang Deog;Jeon, Woo Sung
    • Proceedings of the Korea Water Resources Association Conference
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    • 2018.05a
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    • pp.149-149
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    • 2018
  • Prediction on initial motion of sediment is crucial to evaluate sediment transport and channel stability. The condition of incipient movement of sediment is characterized by bed shear stress, which is generated from force of moving water against the bed of the channel, and by critical shear stress, which depends on force resisting motion of sediment due to the submerged weight of the grains. When the bed shear stress exceeds the critical shear stress, sediment particles begin rolling and sliding at isolated and random locations. In Mountain River, debris flow frequently occurs due to heavy rainfall and can lead some natural stones from mountain slope into the bed river. This phenomenon could add additional forces to sediment transport system in the bed of river and also affect or change direction and magnitude of sediment movement. In this paper, evaluations on incipient motion of uniform coarse gravel under falling spheres impacts using small scale flume channel were conducted. The drag force of falling spheres due to water flow and length movement of falling spheres were investigated. The experiments were carried out in flume channel made by glass wall and steel floor with 12 m long, 0.6 m wide, and 0.6 m deep. The bed slopes were selected with the range from 0.7% to 1.5%. The thickness of granular layer was at least 3 times of diameter of granular particle to meet grain placement condition. The sphere diameters were chosen to be 4cm, 6 cm, 8 cm, 10 cm. The spheres were fallen in to the bed channel for critical condition and under critical condition of motion particle. Based on the experimental results, the Shields curve of particles Reynold number and dimensionless critical shear stress were plotted. The relationship between with drag force and the length movement of spheres were plotted. The pathways of the bed material Under the impact of spheres falling were analyzed.

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Investigation of axial-injection end-burning hybrid rocket motor regression

  • Saito, Yuji;Yokoi, Toshiki;Neumann, Lukas;Yasukochi, Hiroyuki;Soeda, Kentaro;Totani, Tsuyoshi;Wakita, Masashi;Nagata, Harunori
    • Advances in aircraft and spacecraft science
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    • v.4 no.3
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    • pp.281-296
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    • 2017
  • The axial-injection end-burning hybrid rocket proposed twenty years ago by the authors recently recaptured the attention of researchers for its virtues such as no ${\zeta}$ (oxidizer to fuel mass ratio) shift during firing and good throttling characteristics. This paper is the first report verifying these virtues using a laboratory scale motor. There are several requirements for realizing this type of hybrid rocket: 1) high fuel filling rate for obtaining an optimal ${\zeta}$; 2) small port intervals for increasing port merging rate; 3) ports arrayed across the entire fuel section. Because these requirements could not be satisfied by common manufacturing methods, no previous researchers have conducted experiments with this kind of hybrid rocket. Recent advances in high accuracy 3D printing now allow for fuel to be produced that meets these three requirements. The fuel grains used in this study were produced by a high precision light polymerized 3D printer. Each grain consisted of an array of 0.3 mm diameter ports for a fuel filling rate of 98% .The authors conducted several firing tests with various oxidizer mass flow rates and chamber pressures, and analysed the results, including ${\zeta}$ history, using a new reconstruction technique. The results show that ${\zeta}$ remains almost constant throughout tests of varying oxidizer mass flow rates, and that regression rate in the axial direction is a nearly linear function of chamber pressure with a pressure exponent of 0.996.

As ZnO2 Thin Film Manufacturing Time Increases, the Thin Film Particle Growth Plane and a Study on the Direction of Particle Growth (ZnO2 박막 제조 시간의 증가에 따라 박막 입자 성장면과 입자 성장 방향에 관한 연구)

  • Jung, Jin
    • Journal of Integrative Natural Science
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    • v.14 no.1
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    • pp.1-5
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    • 2021
  • A zinc oxide thin film was made by varying the deposition time on the silicon(110) substrate by using a radio frequency sputtering time of 60 minutes, 120 minutes and 180 minutes. As a result of analyzing the grain growth surface of the ZnO2 thin film using an X-ray diffraction apparatus, the directions of the main growth plane (002) and (103) planes of the thin film were significantly affected by the deposition time. As a result of observing the particle growth of the ZnO2 thin film through an electron scanning microscope, it was observed that in the initial stage of deposition of the ZnO2 thin film, an incubation time was required during which growth was stagnant, and then particle growth occurred again after a certain period of time. As a result of chemical analysis of the ZnO2 thin film, the increase in the deposition time did not change with the amount of oxygen in the ZnO2 thin film, but a change in the composition of Zn was observed, indicating that the deposition time of the thin film had an effect on the Zn component in the thin film.

Development of Micro-Tubular Perovskite Cathode Catalyst with Bi-Functionality on ORR/OER for Metal-Air Battery Applications

  • Jeon, Yukwon;Kwon, Ohchan;Ji, Yunseong;Jeon, Ok Sung;Lee, Chanmin;Shul, Yong-Gun
    • Korean Chemical Engineering Research
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    • v.57 no.3
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    • pp.425-431
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    • 2019
  • As rechargeable metal-air batteries will be ideal energy storage devices in the future, an active cathode electrocatalyst is required with bi-functionality on both oxygen reduction reaction (ORR) and oxygen evolution reaction (OER) during discharge and charge, respectively. Here, a class of perovskite cathode catalyst with a micro-tubular structure has been developed by controlling bi-functionality from different Ru and Ni dopant ratios. A micro-tubular structure is achieved by the activated carbon fiber (ACF) templating method, which provides uniform size and shape. At the perovskite formula of $LaCrO_3$, the dual dopant system is successfully synthesized with a perfect incorporation into the single perovskite structure. The chemical oxidation states for each Ni and Ru also confirm the partial substitution to B-site of Cr without any changes in the major perovskite structure. From the electrochemical measurements, the micro-tubular feature reveals much more efficient catalytic activity on ORR and OER, comparing to the grain catalyst with same perovskite composition. By changing the Ru and Ni ratio, the $LaCr_{0.8}Ru_{0.1}Ni_{0.1}O_3$ micro-tubular catalyst exhibits great bi-functionality, especially on ORR, with low metal loading, which is comparable to the commercial catalyst of Pt and Ir. This advanced catalytic property on the micro-tubular structure and Ru/Ni synergy effect at the perovskite material may provide a new direction for the next-generation cathode catalyst in metal-air battery system.

CO2 Laser Scribing Process of Soda Lime Glass (소다석회유리의 CO2 레이저 스크라이빙 가공)

  • Kang, Seung-Gu;Shin, Joong-Han
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.18 no.5
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    • pp.74-81
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    • 2019
  • This study reports the CW $CO_2$ laser scribing of soda lime glass. In this study, scribing experiments are carried out at different laser powers, scan speeds, and focal positions to investigate the effect of the process parameters on the interaction characteristics between a laser beam and glass. In particular, the interaction characteristics are analyzed and described with the input laser energy per unit length. According to the experimental results, the damage threshold for the glass surface was found to exist between 0.072 and 0.08 J/mm. The input laser energy in this region induced partial melting of the surface and grain-shaped cracks. These cracks tended to increase as the input laser energy increased. At the laser input energy larger than 1 J/mm, a huge crack propagating along the scan direction was produced, and the volume below the scribed area was fully melted. The growth of this crack finally resulted in the complete cutting of the glass at the input laser energy above 8 J/mm. It was found that both the width and depth of the scribed line increased with increasing input laser energy. For the beam focusing at the rear surface, the width of the scribed line varied irregularly. This could be ascribed to the increased asymmetry of the beam intensity distribution when the laser beam was focused at the rear surface. Under this condition, a large burr was only produced on one side of the scribed line.

Effect of Rolling Conditions on Microstructure and Mechanical Properties of HCC AZ31 Alloy Plate (압연조건에 따른 AZ31 연주판재의 미세조직 및 기계적 특성 변화)

  • Kim, Young Min;Chun, Eun Young;Yim, Chang Dong;You, Bong Sun;Lee, Je-hyun
    • Korean Journal of Metals and Materials
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    • v.46 no.4
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    • pp.189-198
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    • 2008
  • The changes in microstructure and mechanical properties of AZ31 alloy subjected hot-rolling process were investigated. The AZ31 plates fabricated by horizontal continuous casting process were prepared and have hot-rolled from 30 mm to 1 mm in thickness under different processing conditions. At the rolling temperature of $400^{\circ}C$, little surface and side crack was observed up to 20% reduction rate. As total reduction and reduction rate increase to more than 75% and 20% pass, respectively, Grains were more uniformly refined through overall thickness, and particularly lots of shear bands were appeared to be inclined at less than $20^{\circ}C$ along the rolling direction. Average grain size of less than $5{\mu}m$ and tensile properties of YS ${\geq}$ 250 MPa, UTS ${\geq}$ 300 MPa and El. ${\geq}$ 13% were acquired for hot-rolled AZ31 sheets without post-heat treatment. Maximum intensity of (0002) pole figure was decreased with an increase in reduction rate, indicating the improvement of texture by means of high reduction rate.