• Title/Summary/Keyword: glycol process

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Incorporation of Tobacco Chloroplasts into Soybean Protoplasts (콩 원형질체내로의 담배 엽록체 이입)

  • 차현철
    • Journal of Plant Biology
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    • v.25 no.4
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    • pp.181-188
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    • 1982
  • Chloroplasts isolated from tobacco (Nicotiana tabacum L. cv. Virginia 115) leaves have been transferred into protoplasts of soybean (Glycine max Merr. cv. Jangyeop) suspension-cultured cells with the help of polyethylene glycol (PEG). The increased yield in protoplasts of chloroplast uptake was depended upon the concentration of both PEG 4,000 and PEG 6,000. The highest yield(36%) occurred at 50% of both PEG, and the yield was decreased above this concentration. The rate of uptake with the incubation time was highest at one hour, then decreased. The process of the chloroplast uptake into the protoplasts was similar with that of a protoplast fusion, except forming invagination during uptake.

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Use of Graphite Plate for Homogeneous Sample Preparation in Matrix/Surface-assisted Laser Desorption and Ionization of Polypropyleneglycol and Polystyrene

  • Kim, Jeong Hwan;Gang, Wi Gyeong
    • Bulletin of the Korean Chemical Society
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    • v.21 no.4
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    • pp.401-404
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    • 2000
  • Matrix/Surface-assisted laser desorption/ionization (M/SALDI) mass spectrometry of polypropylene glycol and polystyrene, directly deposited on graphite plate, is demonstrated. Graphite plate is effective both as an en-ergy transfer medium and robu st sampling support for LDI of polymers. Mass spectra ofpolymers can be easily obtained due to homogeneous distribution on graphite surface and their ion signals are long-lived by large ef-fective desorption volume enough to investigate M/SALDI process.

Measurements of Flow Meniscus Movement in a Micro Capillary Tube (마이크로 원형 모세관에서 계면 이동 현상의 측정)

  • Lee, Sukjong;Sung, Jaeyong;Lee, Myeong Ho
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.22 no.1
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    • pp.15-21
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    • 2013
  • In this paper, a high-speed imaging and an image processing technique have been applied to detect the position of a meniscus as a function of time in the micro capillary flows. Two fluids with low and high viscosities, ethylene glycol and glycerin, were dropped into the entrance well of a circular capillary tube. The filling times of the meniscus in both cases of ethylene glycol and glycerin were compared with the theoretical models - Washburn model and its modified model based on Newman's dynamic contact angle equation. To evaluate the model coefficients of Newman's dynamic contact angle, time-varying contact angles under the capillary flows were measured using an image processing technique. By considering the dynamic contact angle, the estimated filling time from the modified Washburn model agrees well with the experimental data. Especially, for the lower-viscosity fluid, the consideration of dynamic contact angle is more significant than for the higher-viscosity fluid.

Inkjet Printing of Customized Silver Ink for Cellulose Electro Active Paper (셀룰로오스 EAPap 용 은잉크 제조 및 잉크젯 프린팅)

  • Mun, Seongcheol;Khondoker, Mohammad Abu Hasan;Kafy, Abdullahil;Mohiuddin, M.d.;Kim, Jaehwan
    • Journal of the Korean Society for Precision Engineering
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    • v.31 no.8
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    • pp.737-742
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    • 2014
  • This paper reports a customized silver ink and its inkjet printing process on a cellulose electro-active paper (EAPap). To synthesize a silver ink, silver nanoparticle is synthesized from silver nitrate, polyvinylpyrrolidone and ethylene glycol, followed by adding a viscosifier, hydroxyethyl-cellulose solution, and a surfactant, diethylene glycol. The silver ink is used in an inkjet printer (Fujifilm Dimatix DMP-2800 series) to print silver electrodes on cellulose EAPap. After printing, the electrodes are heat treated at $200^{\circ}C$. The sintered electrodes show that the thickness of the electrodes linearly increases as the number of printing layers increases. The electrical resistivity of the printed electrodes is $23.5{\mu}{\Omega}-cm$. This customized ink can be used in inkjet printer to print complex electrode patterns on cellulose EAPap to fabricate flexible smart actuators, flexible electronics and sensors.

Characteristics of SBN Thin Films Prepared by Sol-Gel Process (졸겔법으로 제조된 SBN박막의 특성연구)

  • 이동근;김태중;이해욱;이희영;김정주;조상희
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2001.07a
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    • pp.1030-1035
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    • 2001
  • Strontium barium niobate, (Sr$\sub$0.5/Ba$\sub$0.5/Nb$_2$O$\sub$6/), thin films of various composition were prepared by the sol-gel method. Solution derived from acetate powders and niobium ethoxide in a mixture of acetic acid, ethylene glycol and 2-methoxyehanol was spin-coated onto bare silicon, Pt-coated silicon and fused silica substrates. Processing parameters were optimized to develop stable solutions which yielded films with relatively low crystallization temperatures. It was determined that ethylene glycol was a necessary component of the solution to increase stability against precipitation and to decrease the crystallization temperature of the films as confirmed by XRD and FT-IR analyses.

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The Interaction between Hexadecyltrimethylammonium Bromide to Poly (Ethylene Glycol) with Different Molecular Weights and Some Schiff-Bases Investigated by Surfactant Ion Selective Electrode

  • Ghoreishi, Sayed Mehdi;Naeimi, Hossein;Navid, Mohammad Davodi
    • Bulletin of the Korean Chemical Society
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    • v.26 no.4
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    • pp.548-552
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    • 2005
  • The interaction between ionic surfactants and different nonionic molecules and polymers are studied using ion surfactant selective electrode. From the experimental data, critical concentrations of the interaction and binding process are evaluated. The interaction between hexadecyltrimethylammonium bromide (HTAB) with polyethylene glycol (PEG) in three molecular weights (1000, 10000 and 100000) and also schiff-bases, 2-[2-carboxyphenyl nitrilomethylidyne]-phenol (ortho CNP), 2-[3-carboxyphenyl nitrilomethylidyne]-phenol (meta CNP)and 2-[4-carboxyphenyl nitrilomethylidyne]-phenol (para CNP) with the potentiometric method were investigated using HTAB membrane selective electrode. In the case of PEG with increasing molecular weights more interaction to HTAB occurs. The electromotive force (EMF) data also showed that interaction between para CNP with HTAB is more than the other schiff-bases. It seems this case related to less space interference of COOH group for that compound. The onset of binding ($T_1$) of course is the same for three schiffbase molecules.

Nano-sized $Gd_{2}O_{3}:Eu$ phosphor particles of high brightness

  • Lee, Chang-Hee;Roh, Hyun-Sook;Kang, Yun-Chan;Park, Hee-Dong;Park, Seung-Bin
    • 한국정보디스플레이학회:학술대회논문집
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    • 2003.07a
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    • pp.791-794
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    • 2003
  • To synthesize $Gd_{2}O_{3}:Eu$ phosphor powder of nano size and high luminescence efficiency under UV (ultraviolet) and VUV (vacuum ultraviolet) light, organic additives such as citric acid and ethylene glycol and $Na_{2}CO_{3}$ flux were introduced in large-scale spray pyrolysis and critical conditions for forming nano-sized particles were investigated. The $Gd_{2}O_{3}:Eu$ phosphor particles prepared from solutions with organic additives such as citric acid and ethylene glycol had micron size and spherical shape. However, the particles prepared from polymeric precursor solution with $Na_{2}CO_{3}$ flux had nano size and non-aggregation characteristics. The as-prepared spherical particles with micron size turned into nano-sized particles during post-treatment by recrystallization process. The nano-sized $Gd_{2}O_{3}:Eu$ phosphor particles showed higher brightness than the commercial $Y_2O_3:Eu$ phosphor product under both UV light of 254nm and VUV light of 147 nm.

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Development of sacrificial layer wet etch process of TiNi for nano-electro-mechanical device application

  • Park, Byung Kyu;Choi, Woo Young;Cho, Eou Sik;Cho, Il Hwan
    • JSTS:Journal of Semiconductor Technology and Science
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    • v.13 no.4
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    • pp.410-414
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    • 2013
  • We report the wet etching of titanium nickel (TiNi) films for the production of nano-electro-mechanical (NEM) device. $SiO_2$ and $Si_3N_4$ have been selected as sacrificial layers of TiNi metal and etched with polyethylene glycol and hydrofluoric acid (HF) mixed solution. Volume percentage of HF are varied from 10% to 35% and the etch rate of the $SiO_2$, $Si_3N_4$ and TiNi are reported here. Within the various experiment results, 15% HF mixed polyethylene glycol solution show highest etch ratio between sacrificial layer and TiNi metal. Especially $Si_3N_4$ films shows high etch ratio with TiNi films. Wet etching results are measured with SEM inspection. Therefore, this experiment provides a novel method for TiNi in the nano-electro-mechanical device.

Study on the Effect of Performance Factors on the Finned Tube Type Regenerator for Liquid Desiccant Dehumidification (액체 건조제 제습을 위한 핀튜브형 재생기의 성능인자 영향 연구)

  • Jang, Jun-Oh;Park, Moon-Soo;Kang, Kyung-Tae;Lee, Shin-Pyo;Lee, Jin-Soo
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.27 no.7
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    • pp.845-852
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    • 2003
  • Liquid desiccant dehumidification system can be used effectively to save energy consumed in air conditioning as an alternative compared with conventional air conditioning systems by reducing latent heat load. The dehumidifier and the regenerator from the heart of this system. The latent part of the cooling load is handled using liquid desiccant. In this study, the experimental regenerator has been designed to study the regeneration characteristics of the aqueous triethylene glycol(TEG) system. The performance factors of the regenerator with finned tube heat exchanger were evaluated by a series of experimental runs. The regeneration process is highly dependent on the liquid desiccant conditions, such as, temperature, concentration and flow rate. In addition, the effects of the inlet air temperature, humidity and flow rate were discussed. Data obtained are useful for design guidance and performance analysis of a regenerator, particularly for a liquid desiccant cooling system.

Monitoring of the Content of Imidazoline-Containing Corrosion Inhibitor

  • Zadorozhny, P.A.;Sukhoverkhov, S.V.;Markin, A.N.;Savin, K.I.;Prokuda, N.A.
    • Corrosion Science and Technology
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    • v.16 no.4
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    • pp.161-166
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    • 2017
  • The qualitative composition of active components of the corrosion inhibitor CGW-85567 was studied. It was found that С18:2 and С18:1 imidazolines and the corresponding imidazolin-amides are the major components. The HPLC/MS technique was developed for their determination in the water solutions of monoethylene glycol (MEG). Industrial application of the inhibitor showed that MEG solution retained high concentration of the inhibitor for a long time after ceasing its addition into pipelines. Low values of the partition coefficients (0.010-0.014) of imidazolines in the system "water solution of MEG (concentration of MEG 62-85% v/v) - gas condensate" have allowed to pass on from the technology of continuous pumping of the inhibitor into protected pipelines to the periodic dosing technology. Taking into account a long time of circulation in the system and high temperatures during MEG regeneration process possible degradation products of the inhibitor were studied. N, N-dimethyl-dodecanamine-1, and N, N-dimethyl-tetradecanamine-1 were identified as major degradation products of the corrosion inhibitor CGW-85567.