• 제목/요약/키워드: glycerin

검색결과 212건 처리시간 0.03초

글리세린이 복합레진의 중합 후 표면경도에 미치는 영향 (Effect of glycerin on the surface hardness of composites after curing)

  • 박현희;이인복
    • Restorative Dentistry and Endodontics
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    • 제36권6호
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    • pp.483-489
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    • 2011
  • 연구목적: 본 연구의 목적은 글리세린의 도포가 복합레진의 중합 후 표면경도에 미치는 효과를 알아보고자 하였다. 연구 재료 및 방법: 디스크 형태의 황동 몰드에 복합레진(Z-250, 3M ESPE)을 충전 후 다음과 같이 광중합 하였다. 1군(대조군)은 복합레진 표면을 공기 중에 노출한 후 40초 동안 광조사, 2군은 표면을 Mylar strip으로 덮은 후 40초 광조사, 3군은 표면을 glycerin으로 도포 후 40초 광조사, 4군은 공기 중에 노출시켜 20초 광조사한 다음 시편 표면에 glycerin으로 도포한 후 추가로 20초 동안 광조사 하였다. 각 그룹당 20개의 시편을 준비하였고, 연마 후 또는 연마를 하지 않고 시편의 표면경도를 측정하였다. 5일 후 각 시편의 표면경도를 재 측정하였다. 데이터는 three-way ANOVA와 Tukey's post hoc test를 이용하여 분석하였다. 결과: 중합 직 후, 연마하지 않은 시편의 표면경도는 2군 > 3군 > 4군 > 1군의 순이었다. 연마한 경우 각 군 사이의 유의한 차이는 없었다. 같은 군 내에서는 5일 후 표면경도가 중합 직 후 보다 증가하였고 연마한 경우가 연마하지 않은 경우보다 더 높은 표면경도를 나타냈다. 결론: 중합 후 복합레진의 표면경도를 증가시키기 위한 가장 좋은 방법은 연마였고, 중합 전 Mylar strip의 사용이나 glycerin의 도포 역시 중합된 복합레진의 표면경도를 증가시켰다.

친수성 소프트 콘택트렌즈의 물리적 특성에 미치는 습윤성 재료의 영향 (Influence of Wetting Agents on Physical Properties of Soft Contact Lens)

  • 이민제;성아영;김태훈
    • 한국안광학회지
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    • 제19권1호
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    • pp.43-49
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    • 2014
  • 목적: 본 연구는 glycerin과 PVP(polyvinylpyrrolidone)을 각각 첨가제로 사용하였을 때 친수성 콘택트렌즈의 물성 변화를 평가하였다. 방법: Glycerin과 PVP(polyvinylpyrrolidone)를 각각 첨가제로 사용하여 교차결합제인 EGDMA (ethylene glycol dimethacrylate) 기본적인 모노머인 HEMA(2-hydroxyethyl methacrylate)와 그리고 개시제인 AIBN(azobisisobutyronitrile)을 기본 조합으로 하여 공중합하였다. 결과: 생성된 고분자의 물리적 특성을 측정한 결과 PVP(polyvinylpyrrolidone)의 경우, 굴절률은 1.4382~1.4288로, 인장강도는 0.3446~0.2542 kgf로 각각 감소하였으며, 접촉각은 21.44% 감소되고 함수율은 13.49% 증가하였다. 또한 glycerin의 경우, 굴절률 1.4330~1.4328로, 인장강도는 0.2974~0.2854 kgf로, 함수율은 35.58~36.53%로 큰 변화를 보이지 않았으며, 접촉각의 경우 37.64%가 감소되었다. 결론: 본 실험결과로 볼 때, 생성된 공중합체는 고 습윤성 안 의료용 렌즈 재료로 사용이 가능하며, 또한 glycerin을 첨가제로 사용하였을 때, 함수율과 굴절률의 변화를 최소화시킴과 동시에 친수성 렌즈의 습윤성을 증가시켰다.

비페닐디메칠디카르복실레이트의 가용화 및 연질캅셀제로의 설계 (Solubilization and Fomulation as Soft Gelatine Capsule of Biphenyldimethyldicarboxylate)

  • 박기배;정채경;이광표
    • Journal of Pharmaceutical Investigation
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    • 제26권1호
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    • pp.1-11
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    • 1996
  • Biphenyldimethyldicarboxylate (PMC), which has been used to treat hepatitis, is insoluble in water, therefore it has low bioavailability after oral administration. For the purpose of increasing the dissolution rate of PMC, the physical mixtures and inclusion complexes of PMC and $dimethyl-{\beta}-cyclodextrin\;(DM\;{\beta}CD)\;or\;hydroxypropyl-{\beta}-cyclodextrin\;(HP{\beta}CD)$ in molar ratio of 1 : 1 and 1 : 2 were prepared by solvent evaporation method. Mixed micelles of PMC were prepared by reacting PMC with bile salts [sodium cholate(NaC), sodium glycocholate (NaGC)] and oleic acid (OA) or palmitoylcarnitine chloride(PCC). Chloroform/water partition coefficient (PC) of PMC was 36.14 in artificial gastric juice (AGJ) and 33.47 in artificial intestinal juice (AIJ), respectively, on the other hand octanol/water PC was 63.36. PMC formulation was prepared by reacting PMC with PEG400-glycerin system(95 : 5, 90 : 10, respectively) and PEG400-PEG4000-glycerin system (70 : 25 : 5, 65 : 25 : 10, respectively). Dissolution test was performed in AGJ and AIJ by paddle method at $37{\pm}0.5^{\circ}C$. The dissolution rates of PMC tablets on the market were 5.74% and 8.26% at AGJ and AIJ, respectively and marketed PMC capsules were 22.14% and 28.64% at AGJ and AIJ, respectively. The dissolution rates of inclusion complexes of PMC with $DM{\beta}CD$ and $HP{\beta}CD$ in a molar ratio of 1 : 1 were more fast than those of corresponding physical mixtures. The decreasing order of dissolution rates was as follows; PMC-PEG400-PEG4000-glycerin formulation > PMC-PEG400-glycerin formulation > mixed micelles > CD inclusion complexes. The dissolution rates of PMC-PEG400-glycerin and PMC-PEG400-PEG4000-glycerin formulation were most fast and the percentage of dissolution was almost 100% within 20 minutes. And their dissolution rates after 120 minutes were markedly increased as compared with capsules on the market (4.0-fold and 3.2-fold in PMC-PEG400-glycerin formulation at AGJ and AIJ, respectively, and 4.8-fold and 3.7-fold in PMC-PEG400-PEG4000-glycerin formulation at AGJ and AIJ, respectively).

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만성회음부 통증 치료를 위한 지주막하 페놀글리세린 차단 후 발생한 배변 및 배뇨장애 -증례 보고- (Failure of Urination and Defecation after Intrathecal Phenol-glycerin Block for Management of Chronic Perineal Pain -A case report-)

  • 안현정;김종일;이상곤;반종석;민병우
    • The Korean Journal of Pain
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    • 제12권2호
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    • pp.268-271
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    • 1999
  • Intrathecal phenol-glycerin block is a potent tool in stepwise approach to intractable perineal pain. At outpatient clinic, intrathecal phenol-glycerin block have been frequently used to control the cancer pain, as this procedure does not require special equipment. However, undesirable effects may occur with any given intrathecal injection. Although most side effects do not last long, they deserve well to prevent. Recently, we have been controlled the perineal and perianal cancer pain with intrathecal phenol-glycerin block without any specific complications. However, one patient we managed experienced that one patient, with this procedure for chronic non-malignant perineal pain control experience gait disturbance and one-week of voiding and defication difficulties. This research reports these practices, including the review of literature.

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치환된 나프탈이미드기를 가지는 비닐고분자의 합성과 형광특성(I) (Synthesis and Fluorescence Behavior of Vinyl Polymers with Substituted Naphthalimide Group(I))

  • 오대희
    • 한국인쇄학회지
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    • 제15권2호
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    • pp.77-90
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    • 1997
  • Positive type presensitized offset plate developer were blended by quantitative analysis method. The test had been proceeeded to check variation of developability, shelf life and tone reproduction by SiO2/Na2O ratio to PS plate developer, added glycerin, and sodium phosphate with glycerin. This study of tone reproduction had been tested 5 times to get accuracy by PS platesusing kodak CCG C-3, KMS. The test result of tone reproduction of presensitized offset plates can be summarized as follows ; major compositions in positive type plate developer were Na, Si, K and P, developability were increased by Sio2/NaO2 ratio in positive type plate developer. Shelf life can be kept by add glycerin to positive type plate developer. Tone reproduction were improved by sodium phosphate due to buffer action while shelf life can be kept by add glycerin in positive type plate developer.

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The physicochemical properties of rice extrudate by addition of emulsifier(Glycerin fatty acid ester)

  • 고광진
    • 동아시아식생활학회지
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    • 제2권2호
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    • pp.277-282
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    • 1992
  • This study was designedto investigate changes in phsicochemical properties of rice extrudate with added glycerin fatty acid ester extruded by single screw extruder. According to emulsifier content, expansion ratio and water solubility index were represented minimum in rice extrudate with added 2.0% and 2.5% glycerin fatty acid ester. Extrudate with added 1.5% emulsifier revealed lowest break strength and bulk density, so got a tender and light texture. Meanwhile water absorption index was showed maximum at 1.5% emulsifier content. As emulsifier content increased, lightness raised. By the microstructure obsorved with image analyzer, addition of emulsifier had decreased area and fractarea of air cells of cross section of extrudates. On the results of this research, quality of extrudate with added 1.5% glycerin fatty acid ester was considered very well than 100% rice extrudate, because of tender and light texture, highest water absorption indexand fine structure with higher lightness.

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Biodiesel Refining and Glycerin Recovering Process of Transesterification from Tra Catfish Fat

  • Huong, Le Thi Thanh;Tan, Phan Minh;Hoa, Tran Thi Viet;Lee, Soo
    • 한국응용과학기술학회지
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    • 제26권1호
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    • pp.1-9
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    • 2009
  • Nowadays, Tra catfish fat is given attention as an appropriate material for biodiesel production in Vietnam. The aim of this work is to investigate the optimal conditions of refining biodiesel and recovering glycerin by the transesterification from Tra catfish fat using KOH catalyst. As our results, the yield of transesterification was achieved to 94.17% at $50^{\circ}C$ for 45 min with 6:1 molar ratio of methanol to fat in the presence of 0.8% KOH catalyst, and wherein the biodiesel was refined by washing with distilled water at $70^{\circ}C$ and dried in a microwave oven. The yield of raw glycerin recoveries from the transesterification process was 78.58%. The purity of raw glycerin was 84.14% by the conditions of neutralization state with $H_{3}PO_{4}$ solution (pH = 5), $70^{\circ}C$, and 60 min. Activated carbon (3.0 wt.%) was used for the bleaching process at $80^{\circ}C$ for 20 min. The biodiesel was obtained in accordance with for ASTM D 6751 (biodiesel standard). The ash and water of raw glycerins were 7.32 and 8.01%, respectively, and implied that the raw glycerin is very promising candidate to be used as a raw material for textile and cosmetic industries.

유화조건이 홍화적색소의 물성에 미치는 영향 (Effect of Emulsion State on the Physical Properties of Carthamus Red Pigment)

  • 이승룡;장규섭;이석건;윤혜현;한태룡
    • 농업과학연구
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    • 제27권1호
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    • pp.54-62
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    • 2000
  • 상기 실험으로부터 얻어진 결과를 요약하면 다음과 같다. 1. Hunter-value를 측정한 결과 hunter L-value 즉, 백색도에 있어서는 glycerin+carthamin+lecithin의 경우가 실온저장 및, 열악조건 그리고 광조사시에 있어서 모두 8 시간이 경과하면서부터는 급격하게 상승하는 모습을 보였다. 2. 실온하에서 hunter a-value 즉, 적색도에 있어서는 carthamin 첨가구가, b-value 즉, 황색도에 있어서는 paprika 첨가구가 더 강하게 나타났다. 열악조건에서는 실온저장의 경우와 다소 다른 양상을 보여주었는데, D.W+carthamin+lecithin의 경우에 있어서도 hunter L-value가 낮은 값을 나타냈으며, hunter avalue의 경우 soybean oil+paprika에서도 높은 값을 보여주었다. 3. 유변학적 특성에 대한 실험에서 비교적 고점도를 가지고 있는 glycerin을 base material로 하였을 때는 이에 비해 저점도라고 할 수 있는 soybean oil이나 증류수가 쓰여졌을 때보다 spindle의 rpm에 따른 viscosity나 shear rate, shear stress등의 값이 월등히 높은 값을 나타냈다. 그리고, 일반적으로 spindle의 rpm에 대한 shear rate 및 shear stress의 값은 비례적으로 증가하는 경향을 나타냈다. 유화제의 사용여부에 있어서는 lecithin을 사용했을 경우, 사용하지 않았을 때보다 높은 점도를 나타냈고, 통일한 조건에서 carthamin보다는 paprika가 두 배 정도 더 높은 점도를 나타냈다. 4. soybean oil을 사용한 실험구에 있어서는 lecithin의 첨가유무가 점도에 아무런 영향을 미치지 않는 것으로 나타났으나, glycerin을 사용한 실험구에 있어서는 유화제인 lecithin을 병행했을 경우, 특이하게도 오히려 paprika에서보다 carthamin에서 더 높은 점도를 나타냈다. 5. Shear stress 의 경우 soybean oil 첨가구와 glycerin 첨가구가 현저한 차이를 보이며 증가한 반면, shear rate에 있어서는 두 가지 경우 모두 거의 같은 경향을 나타낸 점이 특이했다.

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마그네슘과 글리세린 처리한 붕소 분말로 합성한 Mg(B1-xCx)2의 초전도 특성 (Superconducting Properties of Mg(B1-xCx)2 Bulk Synthesized Using Magnesium and Glycerin-treated Boron Powder)

  • 김이정;전병혁;박순동;탄카이신;김봉구;손재민;김찬중
    • 한국분말재료학회지
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    • 제15권3호
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    • pp.182-187
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    • 2008
  • Carbon was known to be one of effective additives which can improve the flux pinning of $MgB_2$ at high magnetic fields. In this study, glycerin $(C_3H_8O_3)$ was selected as a chemical carbon source for the improvement of critical current density of $MgB_2$. In order to replace some of boron atoms by carbon atoms, the boron powder was heat-treated with liquid glycerin. The glycerin-treated boron powder was mixed with an appropriate amount of magnesium powder to $MgB_2$ composition and the powder pallets were heat treated at $650^{\circ}C\;and\;900^{\circ}C$ for 30 min in a flowing argon gas. It was found that the superconducting transition temperature $(T_c)$ of $Mg(B_{1-x}C_x)_2$ prepared using glycerin-treated boron powder was 36.6 K, which is slightly smaller than $T_c$(37.1 K) of undoped $MgB_2$. The critical current density $(J_c)$ of $Mg(B_{1-x}C_x)_2$ was higher than that of undoped $MgB_2$ and the $T_c$ improvement effect was more remarkable at higher magnetic fields. The $T_c$, decrease and $J_c$ increase associated with the glycerin treatment for boron powder was explained in terms of the carbon substitution to boron site.

배대승기탕(倍大承氣湯) 보류관장(保留灌腸)을 시행(施行)한 중풍변폐(中風便閉) 환자(患者) 45례(例)에 대(對)한 임상적(臨床的) 고찰(考察) (The Clinical Study on 45 Cases of Patients of constipation caused by C.V.A. who were treated with Bo-Riu Enema(保留灌腸))

  • 강영록;김연진;황치원
    • 대한한방내과학회지
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    • 제21권2호
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    • pp.329-336
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    • 2000
  • During 9 months the clinical study on the 45 cases constipation patients caused by C.V.A, who were treated with Bo-Riu Enema, was done in the Department of Oriental Internal Medicine II, Oriental Medicine Hospital, Taejon University. The result of this study is compared with glycerin-enema treated group. The results were as follows ; 1. The incidence rate of constipation caused by C.V.A is higher in old aged group. 2. The incidence rate of constipation caused by C.V.A is higher in Tae-Um-In(太陰人). 3. The improvement rate of constipation caused by C.V.A is higher in Bo-Riu Enema treated group than in glycerin-enema. 4. The admission period is shorter in Bo-Riu Enema treated group than in glycerin-enema. 5. In case of paralytic ileus, the improvement rate of constipation caused by C.V.A is higher in Bo-Riu Enema treated group than in glycerin-enema.

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