• Journal of the Korean Ceramic Society
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• v.53 no.5
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• pp.568-573
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• 2016

We explore the crystalline structure and phase transition of lithium thiophosphate ($Li_7P_3S_{11}$) solid electrolyte using electron microscopy and X-ray diffraction. The glass-like $Li_7P_3S_{11}$ powder is prepared by the high-energy mechanical milling process. According to the energy dispersive X-ray spectroscopy (EDS) and selected area diffraction (SAD) analysis, the glass powder shows chemical homogeneity without noticeable contrast variation at any specific spot in the specimen and amorphous SAD ring patterns. Upon heating up to $260^{\circ}C$ the glass $Li_7P_3S_{11}$ powder becomes crystallized, clearly representing crystal plane diffraction contrast in the high-resolution transmission electron microscopy image. We further confirm that each diffraction spot precisely corresponds to the diffraction from a particular $Li_7P_3S_{11}$ crystallographic structure, which is also in good agreement with the previous X-ray diffraction results. We expect that the microscopic analysis with EDS and SAD patterns would permit a new approach to study in the atomic scale of other lithium ion conducting sulfides.

• Journal of the Korean institute of surface engineering
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• v.55 no.6
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• pp.353-362
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• 2022

Recently, transmittance of photomasks for ultra-violet (UV) region is getting more important, as the light source wavelength of an exposure process is shortened due to the demand for technologies about high integration and miniaturization of devices. Meanwhile, such problems can occur as damages or the reduction of yield of photomask as electrostatic damage (ESD) occurs in the weak parts due to the accumulation of static electricity and the electric charge on chromium metal layers which are light shielding layers, caused by the repeated contacts and the peeling off between the photomask and the substrate during the exposure process. Accordingly, there have been studies to improve transmittance and antistatic performance through various functional coatings on the photomask surface. In the present study, we manufactured antireflection films of Nb₂O₅, | SiO₂ structure and antistatic films of ITO designed on 100 × 100 × 3 mmt sodalime glass by DC magnetron sputtering system so that photomask can maintain high transmittance at I-line (365 nm). ITO thin film deposited using In/Sn (10 wt.%) on sodalime glass was optimized to be 10 nm-thick, 3.0 × 103 𝛺/☐ sheet resistance, and about 80% transmittance, which was relatively low transmittance because of the absorption properties of ITO thin film. High average transmittance of 91.45% was obtained from a double side antireflection and antistatic thin films structure of Nb₂O₅ 64 nm | SiO₂ 41 nm | sodalime glass | ITO 10 nm | Nb₂O₅ 64 nm | SiO₂ 41 nm.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2007.05a
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• pp.123-126
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• 2007

Deformation behavior of $Zr_{55}Cu_{30}Al_{10}Ni_5$ (at. %) bulk metallic glass (BMG) fabricated by suction casting method has been investigated at elevated temperatures in this study. The BMG was first verified to have an amorphous structure thru X-ray diffraction (XRD) and differential scanning calorimetry (DSC). A series of compression tests has consequently been performed in supercooled liquid temperature region to investigate the high temperature deformation behavior. A transition from Newtonian to non-Newtonian flow appeared to take place depending upon both the strain rate and test temperature. A processing map based on a dynamic materials model has been constructed to estimate a feasible forming condition for this BMG alloy.

• Proceedings of the Korean Vacuum Society Conference
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• 2016.02a
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• pp.354.1-354.1
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• 2016

Nanoporous gold (NPG) is a very promising material in various fields such as sensor, actuator, and catalysis because of its high surface to volume ratio and conducting nature. In this study, we fabricated a NPG based amperometric sensor on a glass substrate by means of co-sputtering of Au and Si. During the sputtering process, we found the optimum conditions for heat treatment to reduce the residual stress and to improve adhesion between NPG films and the glass substrate. Subsequently, Si was selectively etched from Au-Si alloy by KOH solution, which forms nanoporous structures. Scanning electron microscopy (SEM) and auger electron spectroscopy (AES) were used to estimate the structure of NPG films and their composition. By employing appropriate heat treatments, we could make very stable NPG films. We tested the performance of NPG sensor with aniline molecules, which shows high sensitivity for sensing low concentration of aniline.

• Journal of the Korean Society of Manufacturing Process Engineers
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• v.6 no.2
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• pp.47-51
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• 2007

Special quality of automobile clutch master cylinder(CMC) and analyzed aluminum, plastic material comparison. Efficiency of plastic master cylinder can modularize higher, light weight anger of parts, several piece parts by single parts, prove NVH(Noise, Vibration, Harshness) than aluminum master cylinder as analysis result. Also, structure is easy simplicity, exchange, maintenance costs can be reduced and decrease environmental pollution because recycling is superior. According as content of glass fiber increases, mechanical properties of matter of material increase equally and glass fiber changed variously by condition on manufacturing process. Through comparison analysis with Plastic Body development connection site, did verification.

• Journal of the Korean Society for Precision Engineering
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• v.29 no.1
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• pp.109-113
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• 2012

The LED failure rate greatly depends on the physical properties of packaging materials (epoxy). The glass transitions temperature (Tg) of the epoxy is one of the most important physical properties. Therefore, in the present study, various epoxies with high Tg were prepared and their failure shapes were analyzed. In addition, the failure shapes depending on the amount of epoxy and the wire bonding structure were measured. As a consequence, the lower failure rate was obtained with the smaller amount of epoxy. The safety of LED was improved with increasing the Tg of the epoxy.

• Fibers and Polymers
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• v.5 no.1
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• pp.25-30
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• 2004

The present paper reports the impact of thermal treatment on the characteristics of core-sheath type hybrid technical yarns. The core-sheath type hybrid yams are prepared using DREF-III technology. Polyester and glass multifilaments are used as core components whereas the cotton and polyester staple fibers are the sheath components wrapped around the core filament with different proportions to form a hybrid structure. The thermal treatment is carried out both in dry and in wet state under relaxed condition and the thermal shrinkage, sheath-slipping resistance and tensile and bending properties of hybrid yarns have been studied. Thermal treatment markedly increases the thermal shrinkage and sheath-slipping resistance of hybrid yarns with polyester multifilament in core, but insignificant effect for yarns with glass multifilament in core. Breaking elongation of hybrid yams with polyester multifilament in core increases with treatment temperature. The hybrid yarns with glass multifilament in core are least affected by thermal treatment.

• 한국정보디스플레이학회:학술대회논문집
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• 2008.10a
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• pp.359-361
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• 2008

Glasses in the $SnO_2-(50-x)P_2O_5-xB_2O_3$ system were examined as potential replacement for the PbO glass frits with low firing temperature for component materials of a plasma display panel. The glasses were evaluated for their structural and the thermal expansion coefficient, glass transition and glass softening temperatures and Vickers hardness as a function of the $B_2O_3$ content.

• Proceedings of the Korean Society For Composite Materials Conference
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• 2002.10a
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• pp.52-55
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• 2002

This paper examines the effective thermal conductivity of 3-D braided glass/epoxy composites. 3-D braided composites have a number of advantage over conventional laminate composites, including through-thickness reinforcement, and high damage tolerance and processability. The thermal properties of composites depend primarily on the microstructure of the braided preform and properties of constituent materials. A thermal resistance network model based on structure of the braided preform is proposed by using thermal-electrical analogy. In order to affirm the applicability theses solutions, thermal conductivities of 3-D braided glass/epoxy composites are measured

• Journal of the Korean Society of Manufacturing Process Engineers
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• v.6 no.1
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• pp.57-61
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• 2007

Special quality of automobile clutch master cylinder(CMC) and analyzed aluminum, plastic material comparison. Efficiency of plastic master cylinder can modularize higher, light weight anger of parts, several piece parts by single parts, prove NVH(Noise, Vibration, Harshness) than aluminum master cylinder as analysis result. Also, structure is easy simplicity, exchange, maintenance costs can be reduced and decrease environmental pollution because recycling is superior. According as content of glass fiber increases, mechanical properties of matter of material increase equally and glass fiber changed variously by condition on manufacturing process. Through comparison analysis with Plastic body development connection site, did verification.