• Title/Summary/Keyword: gas measurement method

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The preparation of ${SiO_x}{N_y}$ thin films by reactive RF sputtering method (고주파 반응성 스퍼터링법에 의한 ${SiO_x}{N_y}$ 박막의 제작)

  • 조승현;최영복;김덕현;정성훈;문동찬;김선태
    • Korean Journal of Optics and Photonics
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    • v.11 no.1
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    • pp.13-18
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    • 2000
  • The SiOxNy thin films were prepared on Si(lOO) by reactive RF sputtering method. The reactive gas ratio and the power were used as parameters for depositing SiOxNy thin fims. The properties of ${SiO_x}{N_y}$ thin tilms were investigated by XRD, XPS, refractive index and extinction coefficient analyzer (n'||'&'||'k analyzer), and FfIR. It was found by the results of the x-ray diffraction measurement that SiOxNy thin films were grown to an amorphous structure. From the results of the XPS, and the n'||'&'||'k analyzer, it was found that refractive index was intended to increase with the increasement of the relative nitrogen contents of the ${SiO_x}{N_y}$ thin films.

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Efficiency Estimation of Toxicity Free Eire Resistance Cable

  • Yoon, Hun-Ju;Hon, Jin-Woong
    • Transactions on Electrical and Electronic Materials
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    • v.3 no.3
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    • pp.34-38
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    • 2002
  • In this paper, efficiency estimation of toxicity fee fire resistance cable experiments was measured smoke density of toxicity free fire resistance polyolefin insulation material and electric field dependence of tree shape in low density polyethylene (LDPE). One of the most serious causes of failure in high-voltage cables, can be an electrical discharge across an internal gab or void in the insulating material. Treeing due to partial discharge is one of the main causes of breakdown in the insulating materials and reduction of the insulation life. Therefore the necessity for establishing a method to diagnose the aging of insulation materials and to predict the breakdown of insulation and research of the fire resistance character has become important. First, we have studied on electric field dependence of tree shape in LDPE about treeing phenomena occurring on the high electrical field. Second, the measurement method is the attenuation quantity of irradiation by smoke accumulating with in a closed chamber due to non-flaming heat decomposition and flaming combustion. A main cause of fire-growth and generating toxic gas when, it bums, should be dealt with great care in life. safety design. The fire gases were occurred carbon monoxide and decomposition than in polyolefin due to incomplete combustion of PVC, which has high content of carbon in chemical compound.

Performance Verification of the Gas Insulated Switchgear using UHF Partial Discharge Diagnosis Method (UHF 부분방전 진단법에 의한 가스절연 개폐장치의 성능검증)

  • Kim, J.B.;Jung, J.R.;Kim, M.S.;Song, W.P.;Kim, M.H.;Ko, H.S.;Choi, I.H.
    • Proceedings of the KIEE Conference
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    • 2004.05b
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    • pp.132-135
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    • 2004
  • In generally, compared with VHF band, electromagnetic waves of UHF band have a low influence for external noise. We can detect the real abnormality with several pC in GIS using UHF method. Recently, it has applied to use the external UHF sensor attached on spacer to GIS of existing substation. In this paper, we firstly described the technique of the partial discharge measurement using frequency analysis and phase analysis in UHF band. Secondly, we presented the results of sensitivity, the relationship of dBm-pC and diagnosis of the reason of PD source by phase analysis. And then, we report the diagnosis result of partial discharge on 800kV GIS in domestic substation. rge diagnosis of GIS.

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Detecting Characteristics of Ultrasonics Generated by Partial Discharge in Insulating Oil Using the Optical Fiber Mach-Zehnder Interferometer (광섬유 Mach-Zehnder 간섭계를 이용한 부분방전 초음파 검출특성)

  • 이상훈;심승환;이광식;김달우
    • Journal of the Korean Institute of Illuminating and Electrical Installation Engineers
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    • v.17 no.4
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    • pp.50-56
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    • 2003
  • It is well known that a partial-discharge(PD) in insulation oil is the source of various physical and chemical phenomena, such as heat, light, gas, chemical transformation, electric current, electromagnetic radiation and ultrasonics. The PD can be detected by measuring one of these changes. Although some techniques are employed in this purpose, several obstacles interfere with an on-line measurement. Ultrasonic-wave detection is a useful method for the diagnosis of the transformer-insulation condition. Conventionally, ulyrasonic waves are detected by Piezo-electric transducer, but we use optical method that has many advantages. In this paper, we constructed a Mach-Zehnder interferometer with optical fiber and investigated the principle of operation. Test arrangement is based on the needle-plane electrode system in oil and applied AC high voltage. Ultrasonic waves were detected and analyzed with wavelet transform.

A Survey on Improvements of Range Hood in Apartment

  • Kang, Kyungmo;Kim, Taeyeon;Lee, Yun-gyu
    • KIEAE Journal
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    • v.17 no.5
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    • pp.43-50
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    • 2017
  • Purpose: Residential cooking(gas or electricity) emits many air pollutants. For Removal of these contaminants, range hood is play an important role in the cooking activities. However, deterioration about performance of range hood can be occur in used range hood which is not verified on performance by testing balancing and adjusting in apartment. So, purpose of this study is to improve the range hood against cooking-generated contaminations. Method: To improve hood, survey of range hood which mounted in apartment have to conduct at first. In this study, the survey was conducted for 3 steps. First, Visual inspection for conditions of range hood. Second, questionnaire of operating and maintenance method. Third, interview with user about need for improvement, complainant. Finally, we integrated the survey for range hood and introduced the probable cause of deterioration through this comprehensive survey. Result: Result of measurement for air volume for range hood, A measured air volume has reduced by 41.4, 38.0, 32.0% each step from rated air volume. There are lots of reasons of this phenomenon including to maintenance, air path of duct, lower-cost devices, exhaust ports. For solve this problem, guideline about operating hood, user in apartment will have to supply with maintenance information at first.

Numerical simulation of a regenerative thermal oxidizer for volatile organic compounds treatment

  • Hao, Xiaowen;Li, Ruixin;Wang, Jiao;Yang, Xinfei
    • Environmental Engineering Research
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    • v.23 no.4
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    • pp.397-405
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    • 2018
  • As regulations governing the control of volatile organic compounds (VOCs) have become increasingly stringent in China, regenerative thermal oxidizers (RTOs) have been more frequently applied in medium- and high-concentration VOCs treatments. However, due to the lack of existing RTO-related research, experience remains a dominant factor for industrial application. This paper thus aimed to establish a model for industrial RTOs, using a transient simulation method and thermal equilibrium model to simulate the internal velocities and temperature distributions of an RTO across multiple cycles. A comparison showed an error of less than 5% between most correlating simulated and experimental measurement points, verifying that the simulation method was accurate. After verification, the velocity and temperature fields inside the RTO were simulated to study the uniformity of temperature and velocity within the packed beds: both fields displayed high uniformity after gas flowed through the honeycomb regenerator. The effects of air volume, VOCs concentrations, and valve switching times on the oxidation chamber temperature, RTO outlet temperature, and thermal efficiency (as well as their averages) were studied. The VOCs removal rate in this study was constantly above 98%, and the average thermal efficiency reached 90%.

Purity assignment of 17β-estradiol by mass balance method

  • Lee, Hwa-Shim;Oh, Kwang-Hoon
    • Analytical Science and Technology
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    • v.30 no.5
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    • pp.226-233
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    • 2017
  • In general, quantitative chemical analysis in various areas including food, the environment, in vitro diagnostics, etc., requires traceability in order to increase the reliability of the measurements. Measurement traceability is a property of an unbroken chain of comparisons relating an instrument's measurements to SI units. Purity analysis is the first process for establishing traceability to SI units in chemical measurements. The purpose of this study is to develop and validate a method of purity assignment for establishing the traceability of $17{\beta}$-estradiol measurements in an in vitro diagnostics field. The establishment of this method is very important as it can be applied to the development of CRM and to the analysis of the purity of other hormones. The method of assignment of the purity of $17{\beta}$-estradiol was developed using the mass balance method and was validated through participation in an International comparison. In the mass balance method, impurities are categorized into four classes as follows: total related structure impurities, water, residual organic solvents, and nonvolatiles/inorganics. In this study, total related structure impurities were characterized by a gas chromatography-flame ionization detector (GC-FID) and a high-performance liquid chromatography-ultraviolet (HPLC-UV) detector, water content was determined by a Karl-Fisher coulometer, and total residual solvents and nonvolatiles/inorganics were checked simultaneously by thermogravimetric analysis (TGA). The purity of the $17{\beta}$-estradiol was 985.6 mg/g and the expanded uncertainty was 2.1 mg/g at 95% confidence. The developed method can be applied to the development of certified reference materials, which play a critical role in traceability.

Vapor Recognition Using Image Matching of Micro-Array Sensor Response from Portable Electronic Nose (휴대용 전자 후각 장치에서 다채널 마이크로 센서 신호의 영상 정합을 이용한 가스 인식)

  • Yang, Yoon-Seok
    • Journal of the Institute of Electronics Engineers of Korea SC
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    • v.48 no.2
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    • pp.64-70
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    • 2011
  • Portable artificial electronic nose (E-nose) system suffers from noisy fluctuation in surroundings such as temperature, vapor concentration, and gas flow, because its measuring condition is not controled precisely as in the laboratory. It is important to develop a simple and robust vapor recognition technique applicable to this uncontrolled measurement, especially for the portable measuring and diagnostic system which are expanding its area with the improvements in micro bio sensor technology. This study used a PDA-based portable E-nose to collect the uncontrolled vapor measurement signals, and applied the image matching algorithm developed in the previous study on the measured signal to verify its robustness and improved accuracy in portable vapor recognition. The results showed not only its consistent performance under noisy fluctuation in the portable measurement signal, but also an advanced recognition accuracy for 2 similar vapor species which have been hard to discriminate with the conventional maximum sensitivity feature extraction method. The proposed method can be easily applied to the data processing of the ubiquitous sensor network (USN) which are usually exposed to various operating conditions. Furthermore, it will greatly help to realize portable medical diagnostic and environment monitoring system with its robust performance and high accuracy.

A Study on the Measurement of Axial Cracks in the Magnetic Flux Leakage NDT System (자기누설 비파괴 검사 시스템에서 축방향 미소결함 측정에 관한 연구)

  • Kim, Hui-Min;Park, Gwan-Soo;Rho, Yong-Woo;Yoo, Hui-Ryong;Cho, Sung-Ho;Kim, Dong-Kyu;Koo, Sung-Ja
    • Journal of the Korean Magnetics Society
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    • v.22 no.2
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    • pp.49-57
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    • 2012
  • From among the NDT (Non-Destructive Testing) methods, the MFL (Magnetic Flux Leakage) PIG (Pipeline Inspection Gauge) is especially suitable for testing pipelines because the pipeline has high magnetic permeability. MFL PIG showed high performance in detecting the metal loss and corrosions. However, MFL PIG is difficult to detect the crack which occured by exterior-interior pressure difference in pipelines and the shape of crack is very long and narrow. Therefore, the new PIG is needed to be researched and developed for detecting the cracks. The CMFL (Circumferential MF) PIG performs magnetic fields circumferentially and can maximize the magnetic flux leakage at the cracks. In this paper, CMFL PIG is designed and the distribution of the magnetic fields is analyzed by using 3 dimensional nonlinear finite element method (FEM). By Simulating and Measuring the magnetic leakage field, it is possible to detect of axial cracks in the pipeline.

Quantitative Elemental Analysis in Soils by using Laser Induced Breakdown Spectroscopy(LIBS) (레이저유도붕괴분광법을 활용한 토양의 정량분석)

  • Zhang, Yong-Seon;Lee, Gye-Jun;Lee, Jeong-Tae;Hwang, Seon-Woong;Jin, Yong-Ik;Park, Chan-Won;Moon, Yong-Hee
    • Korean Journal of Soil Science and Fertilizer
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    • v.42 no.5
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    • pp.399-407
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    • 2009
  • Laser induced breakdown spectroscopy(LIBS) is an simple analysis method for directly quantifying many kinds of soil micro-elements on site using a small size of laser without pre-treatment at any property of materials(solid, liquid and gas). The purpose of this study were to find an optimum condition of the LIBS measurement including wavelengths for quantifying soil elements, to relate spectral properties to the concentration of soil elements using LIBS as a simultaneous un-breakdown quantitative analysis technology, which can be applied for the safety assessment of agricultural products and precision agriculture, and to compare the results with a standardized chemical analysis method. Soil samples classified as fine-silty, mixed, thermic Typic Hapludalf(Memphis series) from grassland and uplands in Tennessee, USA were collected, crushed, and prepared for further analysis or LIBS measurement. The samples were measured using LIBS ranged from 200 to 600 nm(0.03 nm interval) with a Nd:YAG laser at 532 nm, with a beam energy of 25 mJ per pulse, a pulse width of 5 ns, and a repetition rate of 10 Hz. The optimum wavelength(${\lambda}nm$) of LIBS for estimating soil and plant elements were 308.2 nm for Al, 428.3 nm for Ca, 247.8 nm for T-C, 438.3 nm for Fe, 766.5 nm for K, 85.2 nm for Mg, 330.2 nm for Na, 213.6 nm for P, 180.7 nm for S, 288.2 nm for Si, and 351.9 nm for Ti, respectively. Coefficients of determination($r^2$) of calibration curve using standard reference soil samples for each element from LIBS measurement were ranged from 0.863 to 0.977. In comparison with ICP-AES(Inductively coupled plasma atomic emission spectroscopy) measurement, measurement error in terms of relative standard error were calculated. Silicon dioxide(SiO2) concentration estimated from two methods showed good agreement with -3.5% of relative standard error. The relative standard errors for the other elements were high. It implies that the prediction accuracy is low which might be caused by matrix effect such as particle size and constituent of soils. It is necessary to enhance the measurement and prediction accuracy of LIBS by improving pretreatment process, standard reference soil samples, and measurement method for a reliable quantification method.