• Title/Summary/Keyword: gas measurement method

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A study on the characteristics of MEM structure of $SrBi_2Ta_2O_9$ thin films by RE magnetron sputtering (RF 마그네트론 스퍼터링법에 의한 MFM 구조의 $SrBi_2Ta_2O_9$ 박막 특성에 관한 연구)

  • 이후용;최훈상;최인훈
    • Journal of the Korean Vacuum Society
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    • v.9 no.2
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    • pp.136-143
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    • 2000
  • $SrBi_2Ta_2O_9;(SBT)$ films were deposited on p-type Si(100) at room temperature by rf magnetron sputtering method to confirm the possibility of application of $Pt/SBT/Pt/Ti/SiO_2/Si$ structure (MFM) for destructive read out ferroelectric RAM (random access memory). Their structural characteristics with the various annealing times and Ar/$O_2$ gas flow ratios in sputtering were observed by XRD (X-ray diffractometer) and the surface morphologies were observed by FE-SEM (field emission scanning electron microscopy), and their electrical properties were observed by P-V (polarization-voltage measurement) and I-V (current-voltage measurement). The Ar/$O_2$ gas flow ratios of sputtering gas were changed from 1 : 4 to 4 : 1 and SBT thin films were deposited at room temperature. The films show (105), (110) peaks of SBT by XRD measurement. SBT thin films deposited at room temperature were crystallized by furnace annealing at 80$0^{\circ}C$ in oxygen atmosphere during either one hour or two hours. Among their electrical properties, P-V curves showed shaped hysteresis curves, but the SBT thin films showed the asymmetric ferroelectric properties in P-V curves. When Ar/$O_2$ gas flow ratios are 1 : 1, 2: 1, the leakage current density values of SBT thin films are good, those values of 3 V, 5 V, and 7 V are respectively $3.11\times10^{-8} \textrm{A/cm}^2$, $5\times10^{-8}\textrm{A/cm}^2$, $7\times10^{-8}\textrm{A/cm}^2$.After two hours of annealing time, their electrical properties and crystallization are improved.

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A Comparative Study on the Measurement of Smoke from Diesel Vehicle on Chassis-dynamometer using Reflection Photo and Light Extinction Method (차대 동력계에서의 디젤 차량의 매연 측정을 위한 여지 반사식 및 광투과식 측정법의 비교 연구)

  • Kim, Ju-Chul;Lee, Choong-Hoon
    • Journal of the Korean Society of Safety
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    • v.22 no.6
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    • pp.13-19
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    • 2007
  • Diesel car's smoke measurement equipment and method were investigated based on the exhaust gas regulations. Reflection photo method and light extinction method for measuring smoke were compared under conditions of both no load mode and Lug-down 3 mode. Free acceleration mode at no load condition was used for regular inspection of diesel car, and Lug-down 3 mode was used for fine inspection of the diesel car. A correlation between no load mode and Lug-down 3 mode was investigated in this research. The smoke measured with reflection photo method was 1.5${\sim}$2 times higher than that of light extinction method The correlation coefficient between reflection photo method and light extinction method for measuring smoke was 0.83, which shows comparatively high correlation between the two methods for measuring smoke in diesel engines.

Determination of Airborne Formaldehyde Using the Gas Chromatograph-Pulsed Discharge Electron Capture Detector (GC-PDECD를 이용한 공기 중 포름알데하이드의 분석)

  • 김희갑;박미진;김만구
    • Environmental Analysis Health and Toxicology
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    • v.17 no.2
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    • pp.117-123
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    • 2002
  • A gas chromatographic method for the determination of airborne formaldehyde was established. In order to be highly detectable with the electron capture detector, formaldehyde was derivatized to its pentafluorobenzyl oxime form by reacting with O- (2,3,4,5,6- pentafluorobenzyl)hydroxylamine hydrochloride (PFBHA) at pH of 4.6 and temperature of 50$^{\circ}C$ for 1 hour. Air samples were collected into a Tedlar$\^$(R)/ bag followed by transferring into water contained in two impingers in series. Collection efficiency in the front trap was higher than 90%. Measurement of selected indoor and outdoor air samples showed higher formaldehyde concentrations in indoor air environments and the importance of ventilation for reducing indoor pollution.

The measurement of electron drift velocity and analysis of transport coefficients in SF$_6$+$N_2$ gas (SF$_6$+$N_2$혼합기체의 전자 이동속도 측정 및 수송계수 해석)

  • 하성철;하영선
    • Electrical & Electronic Materials
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    • v.7 no.6
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    • pp.462-472
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    • 1994
  • In this paper, electron drift velocity is experimentally measured in SF$_{6}$+N$_{2}$ Gas by induced cur-rent method and quantitaive production of electron transport coefficient is calculated by backward-prolongation of Boltzmann equation. Then electron energy distribution function and attachment coefficients are calculated. This paper can use the electron drift velocity by experimentally and the electron transport coefficient by calculated as a basic data of mixed Gas by comparing and investigating.g.

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The Study on Characteristics of N-Doped Ethylcyclohexane Plasma-Polymer Thin Films

  • Seo, Hyeon-Jin;Jo, Sang-Jin;Lee, Jin-U;Jeon, So-Hyeon;Bu, Jin-Hyo
    • Proceedings of the Korean Vacuum Society Conference
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    • 2013.02a
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    • pp.540-540
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    • 2013
  • In this studying, we investigated the basic properties of N-doped plasma polymer. The N-doped ethylcyclohexane plasma polymer thin films were deposited by radio frequency (13.56 MHz) plasma-enhanced chemical vapor deposition method. Ethylcyclohexenewas used as organic precursor (carbon source) with hydrogen gas as the precursor bubbler gas. Additionally, ammonia gas [NH3] was used as nitrogen dopant. The as-grown polymerized thin films were analyzed using ellipsometry, Fourier-transform infrared [FT-IR] spectroscopy, Raman spectroscopy, FE-SEM, and water contact angle measurement. The ellipsometry results showed the refractive index change of the N-doped ethylcyclohexene plasma polymer film. The FT-IR spectrashowed that the N-doped ethylcyclohexene plasma polymer films were completely fragmented and polymerized from ethylcyclohexane.

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Electron Density Measurement of Inductively Coupled Plasma by Ar Gas Pressure (Ar 가스 압력에 따른 유도결합형 플라즈마의 전자 밀도 측정)

  • 이영환;김광수;조주웅;박대희
    • The Transactions of the Korean Institute of Electrical Engineers C
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    • v.52 no.11
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    • pp.508-511
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    • 2003
  • In this paper, electrical characteristics of inductively coupled plasma in an electrodeless fluorescent lamp were investigated using a Langmuir probe with a variation of argon gas pressure. The RF output was applied in the range of 5 ∼ 50 (W) at 13.56 (MHz). The internal plasma voltage of the chamber and the probe current were measured while varying the supply voltage to the Langmuir probe in the range of -100 (V) ∼+100 (V). When the pressure of argon gas was increased, electric current was decreased. There was a significant electric current increase from l0W to 30 〔W〕. Also, when the RF power was increased, electron density was increase. This implies that this method can be used to find an optimal RF rower for efficient light illumination in an electrodeless fluorescent lamp.

Visualization of Gas/liquid Ejector Flow and Void Fraction Measurement using Fiber Optic Probe (기체-액체 이젝터 유동의 가시화와 광섬유 탐침에 의한 기포분율 측정)

  • Choi, Sung Hwan;Ji, Ho Seong;Kim, Kyung Chun
    • Journal of the Korean Society of Visualization
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    • v.11 no.1
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    • pp.34-40
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    • 2013
  • Gas/liquid two-phase ejector is a device without moving parts, in which liquid is used to drive gas of a low-pressure source. In this paper, the hydrodynamic characteristics of a vertical down type two-phase ejector were studied using an air-water loop system. Entrained air flow rates were measured with inlet and outlet pressures of the ejector with varying water flow rate. Homogeneous bubbly flows in the discharge pipe were confirmed by the high speed flow visualization method. Quantitative measurements of void fraction were made using a newly developed fiber optic probe system.

A Study on the Computational Technique of Cold Gas Flow in Puffer Interrupter (파퍼식 차단부의 냉가스 유동해석기법에 관한 연구)

  • Choi, Y.K.;Song, K.D.;Shin, Y.J.;Park, K.Y.
    • Proceedings of the KIEE Conference
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    • 1997.07a
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    • pp.104-108
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    • 1997
  • The puffer type GCB(gas circuit breaker) has been widely used in modern transmission power system. Understanding the motion of cold $SF_6$ gas flow is essential for the better design of those GCB's. For this purpose, a program using the so-called FLIC(Fluid-In-Cell) method has been developed and applied to a puffer type GCB. The calculated results are compared with those from the measurement and the computation by commercial CFD (Computational Fluid Dynamics) package 'RAMPANT' and show fairly good agreement.

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Standardized Protocols for Measuring Volatile Sulfur Compounds: Scientific Foundations and Methodologies

  • Ji-Youn Kim;Ji-Rak Kim;Jin-Seok Byun;Jae-Kwang Jung
    • Journal of Oral Medicine and Pain
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    • v.49 no.1
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    • pp.5-11
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    • 2024
  • Halitosis is defined as a nasty odor emanating through the mouth and is primarily related to the enhanced concentration of volatile sulfur compounds (VSCs). VSC measurements have been commonly used for experimental comparison and clinical diagnosis. As quantitative methods for comparative analyses of oral malodor, gas chromatography devices have been most commonly used to quickly and easily determine the concentration of several gas components of VSCs, which are agents primarily responsible for halitosis. The concentrations of VSCs fluctuate dynamically depending on contributing factors, including various oral/systemic conditions, intake of medicine and food/drink, oral hygiene, and even routine daily activities. Therefore, the exact analysis of VSCs requires the appropriate standardization of not only exact measurement techniques but also participant conditioning with scientific considerations. Thus, this paper describes the experimental standardizations commonly recommended in previous literature and their scientific background.

Three-dimensional accuracy of different correction methods for cast implant bars

  • Kwon, Ji-Yung;Kim, Chang-Whe;Lim, Young-Jun;Kwon, Ho-Beom;Kim, Myung-Joo
    • The Journal of Advanced Prosthodontics
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    • v.6 no.1
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    • pp.39-45
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    • 2014
  • PURPOSE. The aim of the present study was to evaluate the accuracy of three techniques for correction of cast implant bars. MATERIALS AND METHODS. Thirty cast implant bars were fabricated on a metal master model. All cast implant bars were sectioned at 5 mm from the left gold cylinder using a disk of 0.3 mm thickness, and then each group of ten specimens was corrected by gas-air torch soldering, laser welding, and additional casting technique. Three dimensional evaluation including horizontal, vertical, and twisting measurements was based on measurement and comparison of (1) gap distances of the right abutment replica-gold cylinder interface at buccal, distal, lingual side, (2) changes of bar length, and (3) axis angle changes of the right gold cylinders at the step of the post-correction measurements on the three groups with a contact and non-contact coordinate measuring machine. One-way analysis of variance (ANOVA) and paired t-test were performed at the significance level of 5%. RESULTS. Gap distances of the cast implant bars after correction procedure showed no statistically significant difference among groups. Changes in bar length between pre-casting and post-correction measurement were statistically significance among groups. Axis angle changes of the right gold cylinders were not statistically significance among groups. CONCLUSION. There was no statistical significance among three techniques in horizontal, vertical and axial errors. But, gas-air torch soldering technique showed the most consistent and accurate trend in the correction of implant bar error. However, Laser welding technique, showed a large mean and standard deviation in vertical and twisting measurement and might be technique-sensitive method.