• Title/Summary/Keyword: gamma spectra

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Effect of Gamma Irradiation on the Mechanical and Thermal Properties of Biodegradable Packaging Materials

  • Lim, DaeGyu;Kim, Youngsan;Kwon, Sangwoo;Jang, Hyunho;Park, Su-il
    • KOREAN JOURNAL OF PACKAGING SCIENCE & TECHNOLOGY
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    • v.27 no.2
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    • pp.85-90
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    • 2021
  • The gamma irradiation was on to Poly(butylene sebacate-co-terephthalate) (PBSeT), Poly(butylene adipate-co-terephthalate) (PBAT), Poly(lactic acid) (PLA) and casting polypropylene (CPP) at dose levels from 0 to 50 kGy. The properties of gamma irradiated samples were analyzed using DSC, TGA, UTM and FT-IR spectra. The mechanical and thermal properties of PBSeT and PBAT after gamma irradiation were less affected than CPP. The tensile strength and elongation of PBSeT was not affected by gamma irradiation, while these of PBAT, PLA and CPP were significantly decreased at 50 kGy gamma-ray dose. The thermal stability of PBSeT, PBAT, PLA and CPP showed a similar tendency to tensile strength. The glass transition temperature(Tg) and melting temperature(Tm) of PBSeT and PBAT were not altered by increasing gamma-ray dose, while these of PLA and CPP decreased. The chemical composition of all samples was not modified by gamma irradiation, and it was confirmed by FT-IR spectra. Based on mechanical and thermal stability studies of gamma irradiation on bioplastics, tested biodegradable packaging materials showed a potential to be used in sterilization process up to 35 kGy.

Beam Characteristics of Polychromatic Diffracted Neutrons Used for Prompt Gamma Activation Analysis

  • S. H. Byun;G. M. Sun;Park, H. D.
    • Nuclear Engineering and Technology
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    • v.34 no.1
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    • pp.30-41
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    • 2002
  • The neutron beam is fully characterized for the prompt gamma activation analysis facility at Hanaro in the Korea Atomic Energy Research Institute(KAERI). The facility uses thermal neutrons which are diffracted vertically from a horizontal beam port by a set of pyrolytic graphite(PG) crystals positioned at the Bragg angle of 45" Neutron spectra, neutron flux and Cd-ratio are determined for the three extraction modes of diffracted beam by means of the theoretical and experimental efforts. To obtain theoretical result, the reflectivity of pyrolytic graphite is calculated in the diffraction model for mosaic crystal and the angular divergence after diffraction by mosaic crystal is estimated from Monte Carlo simulation. The time-of-flight spectrometer and gold activation wire are used for measuring the neutron spectra. Both the calculated and measured spectra have proven that the unique feature of polychromatic beam obtained by PG crystals are useful for PGAA. The thermal neutron flux of 7.9$\times$107 n/cm$^2$s and the Cd-ratio of 266 for gold have been achieved at the sample position while the reactor operates at 24 MW The uniformity of beam flux is 12% in the central 1$\times$1 cm$^2$ area. Finally, the beam is briefly characterized by the effective velocity and temperature which are determined by measuring the prompt Y-ray spectra for thin and thick boron samples.ples.

A comparative study of machine learning methods for automated identification of radioisotopes using NaI gamma-ray spectra

  • Galib, S.M.;Bhowmik, P.K.;Avachat, A.V.;Lee, H.K.
    • Nuclear Engineering and Technology
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    • v.53 no.12
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    • pp.4072-4079
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    • 2021
  • This article presents a study on the state-of-the-art methods for automated radioactive material detection and identification, using gamma-ray spectra and modern machine learning methods. The recent developments inspired this in deep learning algorithms, and the proposed method provided better performance than the current state-of-the-art models. Machine learning models such as: fully connected, recurrent, convolutional, and gradient boosted decision trees, are applied under a wide variety of testing conditions, and their advantage and disadvantage are discussed. Furthermore, a hybrid model is developed by combining the fully-connected and convolutional neural network, which shows the best performance among the different machine learning models. These improvements are represented by the model's test performance metric (i.e., F1 score) of 93.33% with an improvement of 2%-12% than the state-of-the-art model at various conditions. The experimental results show that fusion of classical neural networks and modern deep learning architecture is a suitable choice for interpreting gamma spectra data where real-time and remote detection is necessary.

Broad Beam Gamma-Ray Spectrometric Studies with Environmental Materials

  • El-Kateb, Abdul-Hamid Hussein
    • Journal of Radiation Protection and Research
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    • v.43 no.2
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    • pp.75-84
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    • 2018
  • Background: Gamma-ray spectrometry helps in radiation shielding problems and different applications of radioisotopes. Experimental arrangements including broad beam geometries are widely used. The aim is to investigate and evaluate the ${\gamma}-ray$ spectra via attenuation by environmental materials. Materials and Methods: The photo peak to nominated parts in the ${\gamma}-ray$ spectra and the attenuation coefficients ${\mu}_b/{\rho}$ from broad beam geometries are measured for the materials water, soil, sand and cement at the energies 0.662, 1.25, and 1.332 MeV with a $3{^{\prime}^{\prime}}{\times}3{^{\prime}^{\prime}}$ NaI(Tl) detector. Results and Discussion: The ${\gamma}-ray$ spectra vary according to changes in the effective atomic number $Z_{eff}$ of the attenuator, the photon energy and the solid angle. The peak to total ratios are the most sensitive parts to variations in the experimental conditions and overturn in the region 0.663 MeV to 1.332 MeV. This is indicated as inversion trend. The results are discussed in view of $Z_{eff}$ and the experimental conditions. The intensity build-up is larger at the lower energy and larger scattering angles in agreement with Klein-Nishina formula and other results. The build-up factor B is$${\sim_=}$$1 at high ${\gamma}-energies$ and small scattering angles. Conclusion: The sensitivity to material characteristics decrease gradually from peak: to total, to Compton valley, to Compton plateau ratios. Rigorous collimation is necessary at small energies. Cement, of the largest $Z_{eff}$, is characterized by the maximum broad beam mass attenuation coefficients ${\mu}_b/{\rho}$. The obtained results provide information to decide for the suitable experimental set-up based on aim of the work.

Full spectrum estimation of helicopter background and cosmic gamma-ray contribution for airborne measurements

  • Lukas Kotik;Marcel Ohera
    • Nuclear Engineering and Technology
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    • v.55 no.3
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    • pp.1052-1060
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    • 2023
  • The airborne radiation monitoring has been used in geophysics for more than forty years and now it also has its important role in emergency monitoring. The aircraft background and the cosmic gamma-rays contribute to the measured gamma spectrum on the aircraft board. This adverse effect should be eliminated before the data processing. The paper describes two semiparametric methods to estimate the full spectrum aircraft background and cosmic gamma-ray contribution from spectra measured at altitudes where terrestrial contribution is negligible. The methods only assume to know possible peak positions in spectra and their full width at half maximum, that can be easily obtained e.g. from terrestrial measurement. The methods were applied to real experimental data acquired on Mi-17 and Bell 412 helicopter boards. The IRIS airborne gamma-ray spectrometer, with 4×4 L NaI(Tl) crystals, produced by Pico Envirotec Inc., Canada, was used on helicopters' boards. To obtain valid estimate of the aircraft background and the cosmic contribution, the measurements over sea and large water areas were carried out. However, the satisfactory results over inland were also achieved comparing with those acquired over large water areas.

Ambient dose equivalent measurement with a CsI(Tl) based electronic personal dosimeter

  • Park, Kyeongjin;Kim, Jinhwan;Lim, Kyung Taek;Kim, Junhyeok;Chang, Hojong;Kim, Hyunduk;Sharma, Manish;Cho, Gyuseong
    • Nuclear Engineering and Technology
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    • v.51 no.8
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    • pp.1991-1997
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    • 2019
  • In this manuscript, we present a method for the direct calculation of an ambient dose equivalent (H* (10)) for the external gamma-ray exposure with an energy range of 40 keV to 2 MeV in an electronic personal dosimeter (EPD). The designed EPD consists of a 3 × 3 ㎟ PIN diode coupled to a 3 × 3 × 3 ㎣ CsI (Tl) scintillator block. The spectrum-to-dose conversion function (G(E)) for estimating H* (10) was calculated by applying the gradient-descent method based on the Monte-Carlo simulation. The optimal parameters for the G(E) were found and this conversion of the H* (10) from the gamma spectra was verified by using 241Am, 137Cs, 22Na, 54Mn, and 60Co radioisotopes. Furthermore, gamma spectra and H* (10) were obtained for an arbitrarily mixed multiple isotope case through Monte-Carlo simulation in order to expand the verification to more general cases. The H* (10) based on the G(E) function for the gamma spectra was then compared with H* (10) calculated by simulation. The relative difference of H* (10) from various single-source spectra was in the range of ±2.89%, and the relative difference of H* (10) for a multiple isotope case was in the range of ±5.56%.

Pin Power Distribution Determined by Analyzing the Rotational Gamma Scanning Data of HANARO Fuel Bundle

  • Lee, Jae-Yun;Park, Hee-Dong
    • Nuclear Engineering and Technology
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    • v.30 no.5
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    • pp.452-461
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    • 1998
  • The pin power distribution is determined by analyzing the rotational gamma scanning data for 36 element fuel bundle of HANARO. A fission monitor of Nb$^{95}$ is chosen by considering the criteria of the half-life, fission yield, emitting ${\gamma}$-ray energy and probability. The ${\gamma}$-ray spectra were measured in Korea Atomic Energy Research Institute(KAERI) by using a HPGe detector and by rotating the fuel bundle at steps of 10$^{\circ}$. The counting rates of Nb$^{95}$ 766 keV ${\gamma}$-rays are determined by analyzing the full absorption peak in the spectra. A 36$\times$36 response matrix is obtained from calculating the contribution of each rod at every scanning angle by assuming 2-dimensional and parallel beam approximations for the measuring geometry. In terms of the measured counting rates and the calculated response matrix, an inverse problem is set up for the unknown distribution of activity concentrations of pins. To select a suitable solving method, the performances of three direct methods and the iterative least-square method are tested by solving simulation examples. The final solution is obtained by using the iterative least-square method that shows a good stability. The influences of detection error, step size of rotation and the collimator width are discussed on the accuracy of the numerical solution. Hence an improvement in the accuracy of the solution is proposed by reducing the collimator width of the scanning arrangement.

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Application Study of Chemoinfometrical Near-Infrared Spectroscopic Method to Evaluate for Polymorphic Content of Pharmaceutical Powders (일본의 근적외선분광법에 대한 제약회사 응용 및 현황)

  • Otsuka, Makoto
    • Proceedings of the Korean Society of Near Infrared Spectroscopy Conference
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    • 2002.11a
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    • pp.97-117
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    • 2002
  • A chemoinfometrical method for quantitative determination of crystal content of indomethacin (IMC) polymorphs based on fourie-transformed near-infrared (FT-NIR) spectroscopy was established. A direct comparison of the data with the ones collected from using the conventional powder X-ray diffraction method was performed. Pure $\alpha$ and ${\gamma}$ forms of IMC were prepared using published methods. Powder X-ray diffraction profiles and NIR spectra were recorded for six kinds of standard materials with various content of ${\gamma}$ form IMC. The principal component regression (PCR) analyses were performed based on normalized NIR spectra sets of standard samples of known content of IMC ${\gamma}$ form. A calibration equation was determined to minimize the root mean square error of the prediction. The predicted ${\gamma}$ form content values were reproducible and had a relatively small standard deviation. The values of ${\gamma}$ form content predicted by two methods were in close agreement. The results were indicated that NIR spectroscopy provides for an accurate quantitative analysis of crystallinity in polymorphs compared with the results obtained by conventional powder X-ray diffractometry.

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Measurement of Gamma-ray Yield from Thick Carbon Target Irradiated by 5 and 9 MeV Deuterons

  • Araki, Shouhei;Kondo, Kazuhiro;Kin, Tadahiro;Watanabe, Yukinobu;Shigyo, Nobuhiro;Sagara, Kenshi
    • Journal of Radiation Protection and Research
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    • v.42 no.1
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    • pp.16-20
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    • 2017
  • Background: The design of deuteron accelerator neutron source facilities requires reliable yield estimation of gamma-rays as well as neutrons from deuteron-induced reactions. We have so foar measured systematically double-differential thick target neutron yields (DDTTNYs) for carbon, aluminum, titanium, copper, niobium, and SUS304 targets. In the neutron data analysis, the events of gamma-rays taken simultaneously were treated as backgrounds. In the present work, we have re-analyzed the experimental data for a thick carbon target with particular attention to gamma-ray events. Materials and Methods: Double-differential thick target gamma-ray yields from carbon irradiated by 5 and 9 MeV deuterons were measured using an NE213 liquid organic scintillator at the Kyushu University Tandem accelerator Laboratory. The gamma-ray energy spectra were obtained by an unfolding method using FORIST code. The response functions of the NE213 detector were calculated by EGS5 incorporated in PHITS code. Results and Discussion: The measured gamma-ray spectra show some pronounced peaks corresponding to gamma-ray transitions between discrete levels in residual nuclei, and the measured angular distributions are almost isotropic for both the incident energies. Conclusion: PHITS calculations using INCL, GEM, and EBITEM models reproduce the spectral shapes and the angular distributions generally well, although they underestimate the absolute gamma-ray yields by about 20%.

F-GAMMA with KVN

  • Park, Songyoun;Sohn, Bong Won
    • The Bulletin of The Korean Astronomical Society
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    • v.38 no.1
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    • pp.42.2-42.2
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    • 2013
  • The F-GAMMA (FERMI-GST AGN Multi-frequency Monitoring Alliance) project is a program for the monthly monitoring of the broad-band spectra of currently about 90 selected Fermi-GST AGNs. F-GAMMA utilizes several facilities in cm, mm, sub-mm, infrared and optical bands, achieving an unprecedented coverage for the study of the spectral evolution of powerful relativistic jets in AGNs. The KVN joined the F-GAMMA project in May 2011, aiming to monitor flux density at 22 and 43 GHz. We present the preliminary results of flux density variability, evolution of spectral index, and modulation index.

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