• Title/Summary/Keyword: fusion material

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Characterization of Atmospheric H2-Plasma-Treated LiNi1/3Co1/3Mn1/3O2 as Cathode Materials in Lithium Rechargeable Batteries (리튬이차전지에서 대기압 수소플라즈마 처리된 LiNi1/3Co1/3Mn1/3O2 양극 활물질의 특성분석)

  • Sun, Ho-Jung;Lee, Jae-Ho;Jeong, Hyun-Young;Seok, Dong-Chan;Jung, Yongho;Park, Gyungse;Shim, Joongpyo
    • Transactions of the Korean hydrogen and new energy society
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    • v.24 no.2
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    • pp.160-171
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    • 2013
  • $LiNi_{1/3}Co_{1/3}Mn_{1/3}O_2$ powder for cathode materials in lithium rechargeable batteries was treated by atmospheric plasma containing hydrogen to investigate the relationship between charge/discharge performance and physical/chemical changes of materials. Hydrogen plasma at atmosphere pressure was irradiated on the surface of active materials, and the change for their crystal structure, surface morphology, and chemical composition were observed by XRD, SEM-EDS and titration method, respectively. The crystal structure and surface morphology of $H_2$ plasma-treated powders were not changed but their chemical compositions were slightly varied. For charge/discharge test, $H_2$ plasma affected initial capacity and rate capability of active materials but continuous cycling was not subject to plasma treatment. Therefore, it was observed that $H_2$ plasma treatment affected the surface of materials and caused the change of chemical composition.

Expression and Purification of a Functional Recombinant Aspartate Aminotransferase (AST) from Escherichia coli

  • Zou, Lihui;Zhao, Haijian;Wang, Daguang;Wang, Meng;Zhang, Chuanbao;Xiao, Fei
    • Journal of Microbiology and Biotechnology
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    • v.24 no.7
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    • pp.998-1003
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    • 2014
  • Aspartate aminotransferase (AST; E.C. 2.6.1.1), a vitamin B6-dependent enzyme, preferentially promotes the mutual transformation of aspartate and ${\alpha}$-ketoglutarate to oxaloacetate and glutamate. It plays a key role in amino acid metabolism and has been widely recommended as a biomarker of liver and heart damage. Our study aimed to evaluate the extensive preparation of AST and its application in quality control in clinical laboratories. We describe a scheme to express and purify the 6His-AST fusion protein. An optimized sequence coding AST was synthesized and transformed into Escherichia coli BL21 (DE3) strain for protein expression. Ideally, the fusion protein has a volumetric productivity achieving 900 mg/l cultures. After affinity chromatography, the enzyme activity of purified AST reached 150,000 U/L. Commutability assessment between the engineered AST and standard AST from Roche suggested that the engineered AST was the better candidate for the reference material. Moreover, the AST showed high stability during long-term storage at $-20^{\circ}C$. In conclusion, the highly soluble 6His-tagged AST can become a convenient tool for supplying a much better and cheaper standard or reference material for the clinical laboratory.

Evaluation on Resistance Spot Weldability and Nugget Formation of Surface Roughness Treated Steel Sheet (표면조도 특성에 따른 저항 점 용접성 평가 및 너깃 형성 고찰)

  • Kim, Ki-Hong;Choi, Yung-Min;Kim, Young-Seok;Rhym, Young-Mok;Yu, Ji-Hun;Kang, Nam-Hyun;Park, Yeong-Do
    • Journal of Welding and Joining
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    • v.26 no.5
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    • pp.79-89
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    • 2008
  • With the increased use of surface textured steel sheet in body-in-white assembly, resistance spot weldability of these steels is considered to be an important subject. This study evaluated nugget formation and weldability by measuring dynamic resistance with various weld pressure, current, and weld time for steel sheet with two different surface roughnesses. The surface roughness for T-H steel ($R_{a}=1.70\;{\mu}m$) was higher than that for T-L steel ($R_{a}=1.33\;{\mu}m$), and resulted in increased contact resistance and heating for T-H steel spot welding. Therefore, at low weld current and weld cycle ranges, the T-H steel showed better weldability over the T-L steel. The evaluations of weld interface showed that the fusion zone in the T-H steel sheet was continuous in contrast to discontinuous fusion zone for T-L steel sheet at the same welding conditions. A comparison of dynamic resistance and tensile-shear strength (TSS) between T-H and T-L steel sheet suggested that high surface roughness provided larger heating at early cycle of welding and larger TSS.

Prediction of Shielding Performance by Thickness by Comparing the Single and Laminated Structures of Lead-free Radiation Fusion Shielding Sheets (무연 방사선 융합 차폐시트 단일 구조와 적층 구조의 비교를 통한 두께별 차폐성능 예측)

  • Kim, Seon-Chil
    • Journal of the Korea Convergence Society
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    • v.12 no.1
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    • pp.105-110
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    • 2021
  • Radiation shielding of affinity material, which is widely used in medical institutions, is made in sheet form and is mainly applied to apron. Shielding performance is presented based on lead equivalent, and is presented as 0.25-0.50mmPb. In the case of shielding materials where lead is used as the main material, the shielding performance can be adjusted by thickness due to the excellent machinability of lead. However, eco-friendly shielding sheets are difficult to control shielding performance based on thickness criteria as shielding performance varies depending on the content of shielding materials, the properties of polymeric materials that are base materials, and the technical differences in the process. In this study, shielding sheets were manufactured based on thickness to solve these problems and the shielding performance was compared in this study. As a result, it was shown that the laminated structure shielding sheet was more effective.

Analysis of Radiation Fusion Shielding Performance of Ytterbium Oxide, a Radiation Impermeable Substance (방사선 불투과성 물질 산화이테르븀(Ytterbium oxide)의 방사선 융합 차폐성능 분석)

  • Kim, Seon-Chil
    • Journal of the Korea Convergence Society
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    • v.12 no.4
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    • pp.87-94
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    • 2021
  • While the shielding substances of radiation shields in medical institutions are beginning to be replaced by environmentally friendly materials, radiation protection according to the shielding properties of environmentally friendly substances is becoming an important factor rather than the existing lead shielding properties. Tungsten and barium sulfate are representative shielding materials similar to lead, and are made in sheets or fiber form with eco-friendly materials. Ytterbium is an impermeable material used as a fluorine compound in the dental radiation field. This study aims to evaluate the shielding performance in the x-ray shielding area by comparing the shielding properties of ytterbium by energy band and that of existing eco-friendly materials. When three types of shielding sheets were fabricated and tested under the same process conditions, the shielding performance of the medical radiation area was about 5 % difference from tungsten. Furthermore, shielding performance was superior to barium sulfate. In the cross-sectional structure of the shielding sheet, there was a disadvantage that the arrangement of particles was not uniform. Ytterbium oxide showed sufficient potential as a medical radiation shielding material, and it is thought that it can improve the shielding performance by controlling the particle arrangement structure and particle size.

Fabrication and analysis of flexible and transparent antenna on polyamide substrate for laptop computer (폴리아미드 기판에 제작된 노트북용 플렉서블 투명 전극 안테나의 제작 및 분석)

  • Lee, Changmin;Kim, Ilkwon;Kim, Youngsung;Kim, Yongjin;Jung, Changwon
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.15 no.7
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    • pp.4457-4462
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    • 2014
  • This paper presents an antenna design that can be applied to flexible transparent conducting film. The antennas shaping PIFA (Planar Inverted F-shpae Antenna) were produced on polyamide substrates, which are flexible. The IZTO/Ag/IZTO multilayer films were used for the antennas and exhibited superior electrical, optical and flexible characteristics. This study compared the transparency and performance of two antennas (IZTO/Ag/IZTO multilayer film, and Ag monolayer film). The operation frequencies were set to 5.18~5.32 GHz of WLAN (802.11a). The performance showed a maximum efficiency and peak gain of 89 % and 5.86 dBi, respectively.

Friction Behavior of Oil-enriched Nanoporous Anodic Aluminum Oxide Film (오일 함침된 나노 기공 산화알루미늄 필름의 마찰 거동)

  • Kim, Hyo-Sang;Kim, Dae-Hyun;Hahn, Jun-Hee;Ahn, Hyo-Sok
    • Tribology and Lubricants
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    • v.27 no.4
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    • pp.193-197
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    • 2011
  • Friction behavior of nanoporous anodic aluminum oxide(AAO) film was investigated. A 60 ${\mu}m$ thick AAO film having nanopores of 45 nm diameter with 105 nm interpore-diatance was fabricated by mild anodization process. The AAO film was then saturated with paraffinic oil. Reciprocating ball-on-flat sliding friction tests using 1 mm diameter steel ball as the counterpart were carried out with normal load ranging from 0.1 N to 1 N in an ambient environment. The morphology of worn surfaces were analyzed using scanning electron microscopy. The friction coefficient significantly increased with the increase of load. The boundary lubrication layer of paraffinic oil contributed to the lower friction at relatively low load (0.1 N), but it is less effective at high load (1 N). Plastic deformed layer patches were formed on the worn surface of oil-enriched AAO at relatively low load (0.1 N) without evidence of tribochemical reaction. On the other hand, thick tribolayers were formed on the worn surface of both oil-enriched and as-prepared AAO at relatively high load (1 N) due to tribochemical reaction and material transfer.

Thermal Strain Measurement of Austin Stainless Steel (SS304) during a Heating-cooling Process

  • Ha, Ngoc San;Le, Vinh Tung;Goo, Nam Seo;Kim, Jae Young
    • International Journal of Aeronautical and Space Sciences
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    • v.18 no.2
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    • pp.206-214
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    • 2017
  • In this study, measurement of thermophysical properties of materials at high temperatures was performed. This experiment employed a heater device to heat the material to a high temperature. The images of the specimen surface due to thermal load at various temperatures were recorded using charge-coupled device (CCD) cameras. Afterwards, the full-field thermal deformation of the specimen was determined using the digital image correlation (DIC) method. The capability and accuracy of the proposed technique are verified by two experiments: (1) thermal deformation and strain measurement of a stainless steel specimen that was heated to $590^{\circ}C$ and (2) thermal expansion and thermal contraction measurements of specimen in the process of heating and cooling. This research focused on two goals: first, obtaining the temperature dependence of the coefficient of thermal expansion, which can be used as data input for finite element simulation; and second, investigating the capability of the DIC method in measuring full-field thermal deformation and strain. The results of the measured coefficient of thermal expansion were close to the values available in the handbook. The measurement results were in good agreement with finite element method simulation results. The results reveal that DIC is an effective and accurate technique for measuring full-field high-temperature thermal strain in engineering fields such as aerospace engineering.

Finite Element Analysis of a Newly Designed Screw Type Fixture for an Artificial Intervertebral Disc (새로운 방식의 나사형 인공디스크 고정체 해석)

  • Lim, Jong-Wan;Yang, Hyun-Ik
    • Journal of Biomedical Engineering Research
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    • v.31 no.1
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    • pp.56-66
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    • 2010
  • The various total replacement artificial discs have developed because spinal fusion has shown a lesser mobility of an operated segment and an accelerated degeneration at adjacent discs. But almost artificial discs have not yet been reached on the substitute surgery of fusion because many problems such as those clinical success rates were not more than them of fusion have not solved. In this paper, vertically inserted assemble-screw fixture in vertebrae was proposed to improve the fixed capability of artificial disc. And also, to evaluate the design suitability of newly designed screw-type, including fixtures of commercial discs such as wedge and plate type, the 1/4 finite element model with a vertebra and various implanted fixtures were generated, and next, 3 bending motions such as flexion, bending and twisting under the moment of 10Nm and compression under the force of 1000N were considered, respectively and finally, FE analyses were performed. Results of three fixture types were compared, such as Range of Motion and maximal stress, and so on. For ROM, the screw type was average 58% less than the wedge type and was average 42% less than the plate type under all loading conditions. For average stress ratio at closer nodes between vertebra and each fixture, the wedge type was the lowest as minimum 0.02 in twisting, screw types were the highest as maximum 0.28 in compression. As the results of using cement material, it was predicted that the instability problem of the wedge type was better solved. The screw type which could be increased by implanting depth according to the number of assembling mid screws, showed that the decreased tendency of ROMs and maximal cancellous bone stresses. In further study, controlling the number of assembling screws that was suitable for a patient's bone quality, development of surgical tools and keeping on design supplementations, which will be able to develop the competitive artificial disc.

Effect of welding condition on microstructures of weld metal and mechanical properties in Plasma-MIG hybrid welding for Al 5083 alloy (알루미늄 5083 합금의 플라즈마 미그 하이브리드 용접시 용접부 미세조직과 기계적 성질 변화에 미치는 용접조건의 영향)

  • Park, Sang-Hyeon;Lee, Hee-Keun;Kim, Jin-Young;Chung, Ha-Taek;Park, Young-Whan;Kang, Chung-Yun
    • Journal of Welding and Joining
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    • v.33 no.1
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    • pp.61-71
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    • 2015
  • The effect of welding condition on microstructure and mechanical property of Plasma-MIG Hybrid Weld between Al 5083 plates(thickness : 10mm) was investigated. 1 pass weld without any defects such as puckering, undercut, and lack of fusion was obtained by 150~200A of plasma current and 5~7mm of welding speed. Gas porosities and shrinkage porosities were existed in the weld near fusion line. As welding speed and plasma current were decreasing, the area fraction of porosity was increasing. The hardness of the weld is increasing as welding speed. On the basis of microstructural analysis, Mg segregated region near dendrite boundaries tends to increase with the welding speed. In the result of hardness test, Distribution of hardness in fusion zone showed little change with the plasma current. However, when the welding speed increased, hardness in weld metal markdly increased. It could be considered that effect of heat input to growth of the dendritic solidification structures. Based on tensile test, tensile properties of weld metal was predominated by area fraction of porosities. Consequently, tensile properties can be controlled by formation site and area fraction of porosity.