• Title/Summary/Keyword: finer grain size

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The Effect of Y Addition on the Microstructure and Mechanical Property of Rapidly Solidified AZ91 Alloy (급속응고한 AZ91합금의 미세조직 및 기계적 특성에 미치는 Y첨가의 영향)

  • Choi, Jae-Young;Park, Hoon-Mo;Nam, Tae-Woon
    • Journal of Korea Foundry Society
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    • v.20 no.6
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    • pp.386-394
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    • 2000
  • In the present study, the effect of yttrium addition on the microstructure and mechanical property of rapidly solidified AZ91 alloy by melt spinning process is estimated. As yttrium was added, the microstructure of RS ribbons and extrudates became finer than those of AZ91, and RE related phases $(Al_2RE)$ were formed. In the case of the addition of 3wt%Y, the microstructure of extrude showed the finest grain size. At room temperature, the AZ91 + 3wt%Y alloy showed the highest tensile strength, 352 MPA due to precipitation of ${\beta}(Mg_{17}Al_{12})$ phase and $Al_2RE$ phase. At the elevated temperature, the mechanical property of AZ91 + 3wt%Y alloy was higher than those of other Mg alloys. The reasons were that $Al_2Y$ compound was thermally stable and suppressed the grain growth. In contrast with $Al_2Y$ compounds, ${\beta}$ phase was thermally unstable and could not suppress the grain growth at the elevated temperature. Therefore, $Al_2Y$ phase contributed to improve the thermal stability of RS AZ91 alloy.

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Fatigue Behavior of Fine Grained AM60 Magnesium Alloy Produced by Severe Plastic Deformation (강소성변형된 미세립 AM60 마그네슘 합금의 피로거동)

  • You, In-Dong;Lee, Man-Suk;Kim, Ho-Kyung
    • Journal of the Korean Society of Safety
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    • v.27 no.3
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    • pp.15-19
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    • 2012
  • The fatigue behavior of AM60 magnesium alloy produced by equal channel angular pressing(ECAP) process was investigated through fatigue lifetime and fatigue crack propagation rate tests. The grain structure of the material was refined from 19.2 ${\mu}m$ to 2.3 ${\mu}m$ after 6 passes of ECAP at 493 K. The yield strength(YS) and ultimate tensile strength (UTS) increase after two passes but decrease with further pressing, although the grain size becomes finer with increasing pass number. The softening effect due to texture anisotropy overwhelmed the strengthening effect due to grain refinement after 2 passes. A large enhancement in fatigue strength was achieved after two ECAP passes. The current finding suggests that two passed material is better than the multi-passed material in view of the static strength and fatigue performance.

Effect of Grain Size Control and Binder Additions on the Soft Magnetic Properties of Fe-based Nanocrystalline Powder Cores (Fe계 나노결정 분말코아의 연자성특성에 미치는 입도제어 및 바인더 첨가의 영향)

  • Cho E.K.;Cho H.J.;Kwon H.T.;Cho E.M.;Ryu H.H.;Sohn K.Y.;Park W.W.
    • Journal of Powder Materials
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    • v.13 no.4 s.57
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    • pp.256-262
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    • 2006
  • The amorphous $Fe_{73}Si_{16}B_7Nb_3Cu_1$ alloy strip was pulverized to get a flake-shaped powder after annealing at $425^{\circ}C$ for 90 min and subsequently ground to obtain finer flake-shaped powder by using a ball mill. The powder was mixed with polyimide-based binder of $0.5{\sim}3wt%$, and then the mixture was cold compacted to make a toroidal powder core. After crystallization treatment for 1 hour at $380{\sim}600^{\circ}C$, the powder was transformed from amorphous to nanocrystalline with the grain size of $10{\sim}15nm$. Soft magnetic characteristics of the powder core was optimized at $550{\sim}600^{\circ}C$ with the insulating binder of 3wt%. As a result, the powder core showed the outstanding magnetic properties in terms of core loss and permeability, which were originated from the optimization of the grain size and distribution of the insulating binder.

Distributions of Organic Matter and Trace Metals in Intertidal Surface Sediment from the Mokpo-Haenam Coast (목포-해남 연안 조간대 퇴적물중 유기물 및 미량금속 분포 특성)

  • Hwang, Dong-Woon;Kim, Pyoung-Joong;Jung, Rae-Hong;Yoon, Sang-Pil
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.46 no.4
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    • pp.454-466
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    • 2013
  • To evaluate the organic matter and trace metal pollution in intertidal sediment of the coastal zone, various geochemical parameters (grain size, ignition loss [IL], chemical oxygen demand [COD], acid volatile sulfide [AVS], and metals [Al, Fe, Cu, Pb, Zn, Cd, Cr, Mn, Hg, and As]) were measured for the intertidal surface sediment of the mainland and islands between Mokpo and Haenam in the southwestern coast of Korea. The surface sediments consist mainly of finer sediments, such as mud and silt. The concentrations of IL, COD, and trace metals in intertidal sediment were relatively high in the shoreline of the mainland than in that of islands and those in some stations exceeded the sediment quality guidelines (SQGs). Moreover, the concentrations of IL, COD, and trace metals (except As) in sediment showed relatively good positive correlations with mean grain size, indicating that the concentrations of organic matter and trace metals in intertidal sediment of the study region are dependent on grain size of sediment. Pollution evaluation for trace metals using geochemical assessment techniques, such as enrichment factor, geoaccumulation index, and SQGs, suggested that the intertidal sediments in the study region show light pollution with Cr and moderate pollution with As. More extensive interdisciplinary studies are required to determine the potential causes of As pollution in intertidal sediment.

Analysis of Microstructural Refinement for Inconel 706 during Hot Forging Process through Reheating and Strain (Inconel 706의 열간단조 공정 중 재가열과 변형양에 따른 결정립 미세화에 대한 분석)

  • S. G. Seong;H. J. Kang;Y. S. Lee;S. Y. Lee;U. J. Lee;H. I. Jae;J. H. Shin;E. Y. Yoon
    • Transactions of Materials Processing
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    • v.32 no.5
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    • pp.239-246
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    • 2023
  • To reduce the forming load due to the temperature drop, during the hot forging process, a reheating hot forging process design is required that to repeat heating and forging. However, if the critical strain required for recrystallization is not induced during forging and grain growth becomes dominant due to the reduction in dislocation density due to repeated heating, the mechanical properties may deteriorate. Therefore, in this study, Inconel 706 alloy was applied, and the grain refinement behavior was comparatively analyzed according to the number of reheating times and effective strain during reheating hot forging process. Reheating was carried out with a total compression rate of 40% up to 4 times. The Inconel 706 compression test specimens heated once showed finer grains as the effective strain increased due to the dynamic recrystallization phenomenon. However, as the number of heating increases, grain refinement was observed even in a low effective strain distribution of 0.43 due to static recrystallization during reheating. Moreover, grain growth occurs at a relatively low effective strain of 0.43 when the number of reheating is four or more. Therefore, it was effective to apply an effective strain of 0.43 or more during hot forging to Inconel 706 in order to induce crystallization through grain refinement and improve the properties of forged products. In addition, we could notice that up to three reheating times condition was appropriate to prevent grain growth and maintain fine grain size.

Estimation of Permeability Coefficient Using Fractal Dimension of Particle Size Distribution Curve in Granular Soils (조립토 입도분포곡선의 프랙탈차원을 이용한 투수계수의 예측)

  • Park Jae-Seong;Chang Pyoung-Wuck;Son Young-Hwan;Kim Seong-Pil
    • Journal of The Korean Society of Agricultural Engineers
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    • v.48 no.4
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    • pp.41-49
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    • 2006
  • Since particle size distribution curves are useful to estimate permeability of soil, many formulae for permeability coefficient (k) have been published using the parameter from the curves and factors, such as grain size, particle shape and void ratio of soils. However, the parameters such as $C_c,\;C_u$ and $D_n$ derived from only some discrete points on the curve are insufficient to represent the whole gradation. In this paper fractal dimension which is quite new concept and known to be able to represent the entire curve of particle size distribution is employed for the parameters. An empirical formula of permeability coefficient has been developed with fractal dimension and percent of finer than 0.075 mm. The formula developed from this study has confirmed its effectiveness by a series of laboratory tests and comparison to other published formulae. It is found that permeability coefficient is proportional to fractal dimension and inversely proportional to percent of fines.

Reconstruction of Changes in Eolian Particle Deposition Across the Mid-Pleistocene Transition in the Central Part of the North Pacific (중기 플라이스토세 전이기 전후 북태평양 중앙 해역 퇴적물에 기록된 풍성 퇴적물 입자 퇴적 양상 변화 복원)

  • Lee, Sojung;Seo, Inah;Hyeong, Kiseong
    • Ocean and Polar Research
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    • v.41 no.4
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    • pp.275-288
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    • 2019
  • We investigated flux, grain size distribution, Nd-Sr isotope composition, mineral composition, and trace metal composition (REEs and Sc) of inorganic silicate fraction (ISF, mainly Asian dust with an unrestricted amount of volcanic materials) deposited during 600~1000 ka across the Mid-Pleistocene Transition at core NPGP 1401-2A (32°01'N, 178°59'E, 5205m) taken from the central part of the North Pacific. Our results reveal about a 2-fold increase in ISF flux after 800 ka, which is associated with an increase in La/Sc and a decrease in mean grain size. Asian dusts are finer than volcanic materials and La/Sc increases with the enhanced contribution of Asian dusts. Thus, increased flux after 800 ka can be explained by the increased contribution of Asian dusts relative to volcanic materials, likely due to an intensified Westerly Jet (WJ) and the drying of the Asian continent after the MPT. Mean grain size of ISF varies systematically in relation to glacial-interglacial cycles with a decrease during glacial stages, which is consistent with the previous results in the study area. Such a cyclical pattern is also attributed to the increase in the relative contribution of Asian dusts over volcanic components in glacial stages due to intensified WJ and drying of the Asian continent. Thus, it can be concluded that climate changes that had occurred across the MPT were similar to those of interglacial to glacial transitions at least in terms of the dust budget. Different from the Shatsky Rise, however, compositional changes associated with glacial-interglacial mean grain size fluctuations are not observed in Nd-Sr isotope ratios and trace element composition in our study of the Hess Rise. This may be attributed to the location of the study site far (> 4,000 km) from the volcanic sources. The volcanic component at the study site comprises less than 10% and varies within 3% over glacial-interglacial cycles. Such a small variation was not enough to imprint geochemical signals.

Characteristics Variation of the Sedimentary Environment in Winter Season around the Baramarae Beach of Anmyeondo Using Surface Sediment Analysis (표층퇴적물 분석을 통한 동계 안면도 바람아래해수욕장 주변의 퇴적환경 변화특성)

  • JANG, Dong-Ho;KIM, Jang-Soo;PARK, No-Wook
    • Journal of The Geomorphological Association of Korea
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    • v.17 no.1
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    • pp.15-27
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    • 2010
  • This study investigated the sedimentary environment changes in the Baramarae beach of Anmyeondo through spatio-temporal surface sediment analysis. In the winter season 2009, surface sediments were classified into 7 sedimentary facies such as gravel, sand, gravelly sand, gravelly muddy sand, muddy sand, silty sand, and sandy silt. Time-series analysis of average grain size from 2002 to 2009 revealed that the average grain size of sediments became finer and sorting was much worse. On the contrary, during the same period, the grain size became coarsening-trend and sorting was much better in beach area. These different grain size patterns resulted from the different change characteristics of beach and tidal flats. The southwestern beach area was connected to the open sea and thus fine sediments were removed by the environments with relatively high-energy. The sedimentation of fine sediments in the bay resulted from the tidal current action and the reduction of energy by the topographic effects. Fine sediments in the outer part of southwestern tidal flats could be explained such that the Seomot isle blocked ocean waves and as a result, low-energy environments accelerated sedimentations of fine sediments.

Grain-Size Trend Analysis for Identifying Net Sediment Transport Pathways: Potentials and Limitations (퇴적물 이동경로 식별을 위한 입도경향 분석법의 가능성과 한계)

  • Kim, Sung-Hwan;Rhew, Ho-Sahng;Yu, Keun-Bae
    • Journal of the Korean Geographical Society
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    • v.42 no.4
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    • pp.469-487
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    • 2007
  • Grain-Size Trend Analysis is the methodology to identify net sediment transport pathways, based on the assumption that the movement of sediment from the source to deposit leaves the identifiable spatial pattern of mean, sorting, and skewness of grain size. It can easily be implemented with low cost, so it has great potentials to contribute to geomorphological research, whereas it can also be used inadequately without recognition of its limitations. This research aims to compare three established methods of grain-size trend analysis to search for the adequate way of application, and also suggest the research tasks needed in improving this methodology 1D pathway method can corporate the field experience into analyzing the pathway, provide the useful information of depositional environments through X-distribution, and identify the long-term trend effectively. However, it has disadvantage of the dependence on subjective interpretation, and a relatively coarse temporal scale. Gao-Collins's 2D transport vector method has the objective procedure, has the capability to visualize the transport pattern in 2D format, and to identify the pattern at a finer temporal scale, whereas characteristic distance and semiquantitative filtering are controversial. Le Roux's alternative 2D transport vector method has two improvement of Gao-Collins's in that it expands the empirical rules, considers the gradient of each parameters as well as the order, and has the ability to identify the pattern at a finer temporal scale, while the basic concepts are arbitrary and complicated. The application of grain sire trend analysis requires the selection of adequate method and the design of proper sampling scheme, based on the field knowledge of researcher, the temporal scale of sediment transport pattern targeted, and information needed. Besides, the relationship between the depth of sample and representative temporal scale should be systematically investigated in improving this methodology.

Characteristics in Microstructure of Particle Reinforced Al Matrix Composites Fabricated by Spray-Cast Forming Process (분사주조한 입자강화 알루미늄 복합재료의 미세조직 특성)

  • Park, Chong-Sung;Lee, In-Woo;Kim, Myung-Ho
    • Journal of Korea Foundry Society
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    • v.14 no.6
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    • pp.530-540
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    • 1994
  • Aluminium-silicon alloy(JIS AC8A) matrix composites reinforced with SiC particles were fabricated by spray-cast forming process, and the microstructure of powders and preforms produced were studied by using an optical and scanning electron microscopy. SiC particles were co-sprayed by mixed phase injection method during the spray casting process. Most of the composite powders formed by this mixed phase injection method exhibit morphology of particle-embedded type, and some exhibits the morphology of particle attached type due to additional attachment of the SiC particles on the surface of the powders in flight. The preforms deposited were resulted in dispersed type microstructure. The pre-solidified droplets and the deposited preform of SiC-reinforced aluminium alloy exhibit finer equiaxed grain size than that of unreinforced aluminium alloy. Eutectic silicons of granular type are crystallized at the corner of the aluminum grains in the preforms deposited, and some SiC particles seem to act as nucleation sites for primary/eutectic silicon during solidification. Such primary/eutectic silicons seem to retard grain growth during the continued spray casting process. It is envisaged from the microstructural observations for the deposited preform that the resultant distribution of SiC injected particles in the Al-Si microsturcture is affected by the amount of liquid phase in the top part of the preform and by the solidification rate of the preform deposited.

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