• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2009년도 추계학술대회 논문집
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• pp.459-461
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• 2009

In this research, a new method for consolidation of Al-20wr%Si powders using a magnetic pulsed compaction (MPC) was introduced. A wide Range of experimental studies were carried out to characterize the mechanical properties and microstructure of the MPCed materials by means of SEM, TEM and tensile test. It was found that the effective properties like higher strength and full density were achieved while maintaining a fine microstructure. Consolidated bulk by MPC showed higher density without any crack than that of the general process. With increasing the number of MPC compaction, the density and mechanical properties were also greatly improved.

• 한국콘크리트학회:학술대회논문집
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• 한국콘크리트학회 2002년도 가을 학술발표회 논문집
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• pp.549-554
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• 2002

In Powder System, SCC demands high dosage of superplasticizer and a lage amout of powder for suitable fluidity and viscosity. Okamura's method of most representative mixing design method in SCC of Powder-System is unfavorable economically because of using a large amount of powder. In addition, many ready-mixed concrete plants do not use his mix design method and procedure due to complexity for practical application. Therefore, Nan Su proposed more simple mix design method than Okamura's. It had an advantage in simplicity in practical application and required a smaller amount of powders compared with Okamura's method. This paper proposed an optimal mixture proportion of SCC with consideration of Nan Su's method. The new and modified mix design method required a smaller amount of powder than that of Nan Su's. To check the properties of SCC, considered with the requirements specified by the Japanese Society of Civil Engineering.(JSCE)

• E2M - 전기 전자와 첨단 소재
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• 제7권6호
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• pp.496-503
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• 1994

In recent years Sol-Gel processing provides an interesting alternative method for the fabrication of ferroelectric thin layers and powder. PZT powder was prepared from an alkoxide-based solution by a Sol-Gel method. Gelation of synthesized complex solutions, microstructure, thermal analysis and crystallization behaviors of the calcined powder were studied in accordance with a water content and a catalyst. Especially gelation and crystallization behavior were analysed with the change of pH. The gelation time decreased as the pH of the mixed solution increased. For PZT powder with 650.deg. C heat treatment, 100% perovskite phase was formed by using either acidic or basic catalyst. By using either acidic or basic catalyst, we were able to get very fine powders of uniform shape with an average particle size of 0.8-1.mu.m.

• 한국표면공학회지
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• 제28권2호
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• pp.83-91
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• 1995

A new method for preparation of thin nickel foam for Ni-MH battery was investigated. In this method, fine graphite powders of $1\mu\textrm{m}$～$2\mu\textrm{m}$ diameter were pasted into pores of thin polyurethane foam film in order to supply electric conducting seeds for nickel deposition by electroless plating reaction. After electroless plating, remaining polyurethane foam was removed chemically by organic solvent treatment and graphite particles also removed by ultrasonic cleaning. Porosity of formed nickel foam was about 85% During electroplating, porosity of the nickel foam decreased less than 5% up to $30\mu\textrm{m}$ coating thickness. And then it was electroplated and heat-treated to improve mechanical strength and ductility. Finally, thin nickel foam for Ni electrode of Ni-MH battery with 80% porosity and $350\mu\textrm{m}$～X$400\mu\textrm{m}$ thickness was obtained.

• The Korean Journal of Ceramics
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• 제2권4호
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• pp.251-256
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• 1996

Effect of mixed grinding with a planetary ball mill of starting materials before heat treatment on the crystal structure and superconduction properties in the YBaCu composite oxide was studied. The size reduction of powders too place in the early stage of grinding, followed by aggregation of the resultant fine particles. The uniformity of the composition in the mixture was improved with grinding, which later decreased in the crystal grain size and well distribution of twin phase in the sintered bodies. The critical current density of the sintered bodies obtained from the mixture ground for 60 minutes showed the maximum value about 150 A/$\textrm{cm}^2$, while critical temperatures were around 90K and were independent of the grinding time.

• 한국수소및신에너지학회논문집
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• 제4권1호
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• pp.41-50
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• 1993

The hydrogen absorption and desorption characteristics of microencapsulated (CFM)$Ni_{4.7}Al_{0.2}Fe_{0.1}$ and $MmNi_4Fe$ powder with Ni and/or Cu by means of chemical plating method have been investigated. Initial hydrogen absorption rate and activation property were increased remarkably by encapsulation and subsequent compacting. Pellets abtained by compacting of Cu-encapsulated fine powder have fairly good strength even after 30 cycles of hydriding and dehydriding. Encapsulated alloy powder and their compacts show a good resistance to degradation by $O_2$ or CO in hydrogen.

• 대한의생명과학회지
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• 제8권2호
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• pp.101-106
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• 2002

The purpose of this study was to test the capacity of automatic tablet crusher. The Automatic tablet crusher not only saved crushing time, but also removed floating fine powders that was occurred during crushing and caused allergy. The characteristics of powder produced by this crusher were as follows: First, to meet the condition as powder after pulverizing 5∼10 g tablet it took 6 to 12 seconds crushing time. But six seconds would do to get powder f3r oral administration. Second, when the quantity of medicine was measured by HPLC, powder from automatic crusher showed higher than that from pestle. HPLC chromatogram indicated that there was no change of medicine in the process of pulverization.

• 한국재료학회:학술대회논문집
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• 한국재료학회 2003년도 춘계학술발표강연 및 논문개요집
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• pp.95-95
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• 2003

최근, 대면적 평판표시소자 제작을 위한 전기발광 (EL; electroluminescence)소자용 소재로서 GaN 분말을 적용하고자 하는 연구가 진행되고 있다. 이와 같이 GaN 분말을 EL 소재로 사용하기 위해서는 원하는 파장의 빛을 발광할 수 있도록 특정의 불순물을 첨가하여야 할 필요가 있다. Mg이 첨가된 GaN 분말의 합성과 특성에 대한 연구가 있었으며, 희토류 원소가 첨가된 GaN 분말의 특성이 보고된바 있다. 본 논문에서는 GaOOH 분말을 출발물질로 채택하여 Zn가 첨가된 GaN 분말을 합성하고 광학적인 특성을 조사하였다. Zn가 첨가된 GaN 분말을 합성하기 위하여, 우선 CaOOH 분말 1g과 일정량의 ZnO 또는 Zn(NO$_3$)$_3$를 함께 섞어 유발에서 습식 혼합한 후 건조시켰다. Ga에 대한 Zn의 몰 비는 0.1부터 30 까지 변화시켰다. 반응온도는 900~110$0^{\circ}C$의 범위에서 변화시켰고, 반응시간은 1~4시간 범위에서 변화시켰으며, NH$_3$의 유량은 400 sccm으로 하였다. X선 회절분석장치를 사용하여 결정구조를 확인하였고, Zn의 첨가에 따른 광학적 특성은 10 K의 온도에서 광루미네센스(PL; photoluminescence)를 측정하여 평가하였다.

• 한국콘크리트학회:학술대회논문집
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• 한국콘크리트학회 1998년도 가을 학술발표회 논문집(I)
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• pp.191-196
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• 1998

Under concentrational paste and dilute suspension systems, we have been tested the effects in the dosage of two superplasticizers [naphtalenic(NSF) and polycarboxylic(NT-2)] which has been varied from 0 to 2.0 wt%, in both one case of cement Ⅱ-anhydrite and fly ash itself and the other case that cement has been substituted 10wt% to Ⅱ-anhydrite and fly ash. The result of tested zeta potential tells that zeta potential values increase in addition to increasing of the NSF dosage. And it's effect was high in case of fly ash. We has confirmed the 10wt% substitution of Ⅱ -anhydrite and fly ash would be more effective than the cement itself in initial fluidity and stable fluidity. And in case of NT-2 and NSF, addition of 1.0wt% NT-2 improved the fluidity of paste cement more than that for NSF.

• 한국안전학회지
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• 제14권3호
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• pp.48-53
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• 1999

It is widely recognized that Hartmann tube for measuring the minimum ignition energy(MIE) of powder. But It requires long time and operational skills for measuring. As a variety of new fine powders are being produced day by day in industry, Japen has been developing a measurement system which employs a new method to create a dust/air mixture in a miniature combustion box. In this system, by vibration, the powder is successively fed downward through a hopper made up of metal mesh, and then it is formed into a thin, certain-like, dust/air mixture. With this new apparatus, three types of powder-Lycopodium, Anthraquinone, and Polyacry-lonitrile-were tested and the data of MIE were compared with those of a conventional apparatus (the Hartmann tube). Two of them agreed satisfactory, but the other, Anthraquinone, showed quite different values. It is guessed that the agglomerations of the powder particles appear because of particle shapes, static-charge and humidity.