• Title/Summary/Keyword: fine particle size

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Coercivity of Nd-Fe-B-type Fine Particles Prepared from Different Precursor Materials

  • Kim, K.M.;Kwon, H.W.;Lee, J.G.;Yu, J.H.
    • Journal of Magnetics
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    • v.20 no.1
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    • pp.21-25
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    • 2015
  • Fine Nd-Fe-B-type particles were prepared by ball milling of different types of Nd-Fe-B precursor materials, such as die-upset magnet, HDDR-treated material, and sintered magnets. Coercivity dependence on the grain and particle size of the powder was investigated. Coercivity of the milled particles was reduced as the particle size decreased, and the extent of coercivity loss was dependent upon the precursor material. Coercivity loss in the finely milled particles was attributed to the surface oxidation. The extent of coercivity loss in the fine particles was closely linked to grain size of the precursor materials. Coercivity loss was more profound for the fine particles with larger grain size. Contrary to the fine particles from the sintered magnets with larger grain size the fine particles (~10 um) from the die-upset magnet and HDDR-treated material with much finer grain size still retained high coercivity (> 10 kOe for die-upset magnet, > 4 kOe for HDDR-treated material).

Preparation and Characterization of Fine $TiO_2$ Powders by Vapor-Phase Hydrolysis of TiCl4 (사염화티타늄의 기상가수분해반응에 의한 $TiO_2$ 미분의 제조 및 입자특성)

  • 염선민;김광호;신동원;박찬경
    • Journal of the Korean Ceramic Society
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    • v.29 no.7
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    • pp.525-532
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    • 1992
  • TiO2 fine powder was synthesized in the gas phase by chemical vapor deposition using hydrolysis of TiCl4. Content of rutile phase in the powder was investigated. Powder characteristics such as size, crystallinity and morphology were also studied by means of TEM, SEM and XRD. Rutile phase in TiO2 powder started to be formed from 100$0^{\circ}C$ and the content increased with the reaction temperature and TiCl4 concentration. As the temperature increased from 80$0^{\circ}C$ to 140$0^{\circ}C$, the primary particle size increased while secondary particle size decreased. Spherical secondary particle with fine primary crystals agglomerated was produced at low temperature of 80$0^{\circ}C$ whereas the grown primary particle being final particle size was produced at higher temperature of 140$0^{\circ}C$. Other effects of TiCl4 and H2O partial pressures on particle size were also reported in this study.

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Effects of Particle Size of Barley on Intestinal Morphology, Growth Performance and Nutrient Digestibility in Pigs

  • Morel, P.C.H.;Cottam, Y.H.
    • Asian-Australasian Journal of Animal Sciences
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    • v.20 no.11
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    • pp.1738-1745
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    • 2007
  • A growth trial and a digestibility trial were conducted to examine the effect of feed particle size on the performance, nutrient digestibility, gastric ulceration and intestinal morphology in pigs fed barley-based diets. Barley was processed through a hammer mill to achieve four diets varying in particle size (average particle $size{\pm}standard $deviation): coarse ($1,100{\pm}2.19\;{\mu}m$), medium ($785{\pm}2.23\;{\mu}m$), fine ($434{\pm}1.70\;{\mu}m$) and mixed (1/3 of coarse, medium and fine) ($789{\pm}2.45\;{\mu}m$). Sixty-four entire male pigs were used in the growth trial and the diets were fed ad libitum between 31 kg and 87 kg live weight. Following slaughter, stomach and ileal tissues were scored for integrity (ulceration or damage) and histological measurements taken. Twenty-four entire male pigs were used in the digestibility trial, which involved total faecal collection. Over the entire growth phase, there were no differences (p>0.05) in average daily gain and feed conversion ratio between pigs fed diets of different particle size. Pigs fed the coarse and medium diets had lower (p<0.05) stomach ulceration scores (0.20 and 0.25, respectively, on a scale from 0 to 3) than those fed the mixed (0.69) or the fine diets (1.87). The stomachs of all animals fed the fine diet had lesions and stomach ulcerations were present only in this group. Pigs fed the fine diet had thicker (p<0.001) ileal epithelial cell layer with no differences (p>0.05) being observed for villous height or crypt depth. Faecal digestibility coefficients of neutral and acid detergent fibre were the highest (p<0.05) for the mixed diet, intermediate for the fine and coarse diets and the lowest for the medium diet. A similar numerical trend (p = 0.103) was observed for the apparent faecal energy digestibility coefficient. It is concluded that, with barley based diets, a variation in average particle size between $400{\mu}m$ and $1,100{\mu}m$ had no effect on pig performance but the fine dietary particle size affected the integrity of the stomach, as well as the structure of the small intestine, thus compromising overall gut health. Our data also demonstrate that changes in particle size distribution during the digestion process, rather than average particle size or particle size variation, are related to apparent faecal digestibility.

Condensational Growth of Fine Aerosol Particles to Increase Precipitation Efficiency (집진효율 향상을 위한 미세 에어로졸 입자의 응축에 의한 성장 연구)

  • Han, Sang-Woo;Hwang, Jung-Ho
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.24 no.8
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    • pp.1069-1076
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    • 2000
  • As the environmental problems grow, the regulation of the pollutants emitted from power plants increases. Most of the pollutants in particle phase are removed by particle removal facilities, but fine particles between 0.1 micron and I micron in diameter have a low removal efficiency compared to particles in other size ranges. Therefore the present concern has concentrated on the removal of those fine particles. The purpose of this study is to grow fine particles by condensation to the range larger than I micron. Theoretically the general dynamic equation is solved with an assumption that the particle size follows a log-normal distribution to calculate the temporal behavior of the size distribution. Experiments have been carried out to compare the results with the theoretical predictions. Particles grown by condensation are sampled by impactors and observed with SEM photographs.

Characterizations of fine Bi-2223 precursor powder by spray pyrolysis process (분무 열분해법으로 제조된 미세 Bi-2223 전구분말의 특성)

  • Kim S. H.;Yoo J. M.;Ko J. W.;Kim Y. K.
    • Progress in Superconductivity
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    • v.6 no.2
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    • pp.124-128
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    • 2005
  • Homogeneous and fine powders for Bi-2223 tape were prepared by ultrasonic spray pyrolysis (SP) method from an aqueous solution of metal nitrates. Bi-2223 precursor powders were synthesized with various solutes concentration and pyrolysis temperature. The synthesized precursor powders had a narrow particle size distribution and an average particle size was $\~{\cal}um$. The reactivity of precursor powder by SP method is very high, attributed to the fine and narrow particle size distribution. Bi-2223/Ag tape was prepared using PIT method and followed by various sintering conditions. The precursor powder by SP method promoted a very quick formation of the Bi-2223 phase for short sintering time while the secondary phase such as large AEC phase and $Ca_2PbO_4$ were minimized for SP tapes.

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Influence of Atomizing Condition on Particle Size Distributions for High Pressure Water Atomized Powder

  • Nakabayashi, Koei;Tanaka, Yoshinari;Hirai, Masazumi
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.18-19
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    • 2006
  • To improve the properties of fine metal powder, such as particle size distribution and geometric standard deviation, this work was done at various atomizing conditions. The new atomization mechanism and the correlation equation were proposed to estimate the mean particle diameter.

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Fabrication of fine BSCCO-2223 precursor powder by spray pyrolysis process (분무 열분해방법에 의한 미세 BSCCO-2223 전구분말의 제조)

  • 김성환;유재무;고재웅;김영국;박기호
    • Progress in Superconductivity
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    • v.5 no.1
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    • pp.65-69
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    • 2003
  • Many researches on fabrication process for BSCCO precursor powders have been developed for high J$_{c}$ BSCCO-2223 tape. Spray pyrolysis method for fabrication of precursor powder has many advantages, such as high purity, fine particle size and low carbon content of BSCCO precursor powder. Fine, spherical powders were prepared by ultrasonic spray pyrolysis from the aqueous solution of metal nitrates. BSCCO precursor powders were synthesized with various solutes concentration and heat treatment conditions. Average particle size for spray pyrolysis powders was $1.5∼3\mu\textrm{m}$. Bi-2223/Ag tape was prepared by PIT method and followed by various sintering conditions. BSCCO precursor powders were characterized by XRD, SEM, EDS, Carbon content and particle size analysis.s.

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Effect of Wood Particle Size on Physical and Mechanical Composites by Nonwoven Web Process

  • Chae, Shoo Geun;Eom, Young Geun
    • Journal of the Korean Wood Science and Technology
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    • v.33 no.2 s.130
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    • pp.40-55
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    • 2005
  • This study was carried out to discuss the feasibility of wood and plastic wastes as the raw materials for wood particle-plastic composites. For this purpose, composites were manufactured from coarse and fine wood particles and polypropylene fibers by nonwoven web process. And the effect of wood particle size on the performance of the composites were analyzed according to ASTM D 1037-93. In the physical properties of composites, water absorption decreased with the increase of target density and polypropylene fiber content. And the composites with fine wood particles appeared to have slightly lower water absorption than those with coarse wood particles. Thickness swelling did not vary significantly with the increase of target density but increased with the increase of wood particle content. And the composites with fine wood particles were significantly lower in thickness swelling than those with coarse wood particles. In the mechanical properties of composites, dry and wet MOR showed the increasing tendency with the increase of polypropylene fiber content and target density. Dry and wet MOE showed the increasing tendency with the increase of target density but only wet MOE exhibited the increasing tendency with the increase of polypropylene fiber content. Composites with fine wood particles appeared to be generally higher in wet MOR and MOE than those with coarse wood particles. In conclusion, composites with fine wood particles showed generally higher performance than those with coarse ones. Also, composites were significantly superior to control particleboards in the performance, especially in water absorption and thickness swelling.

Physical Characteristics of Aerosol Concentrations Observed in an Urban Area, Busan (부산 도심지에서 측정된 에어로졸 농도의 물리적 특성)

  • Kim, Yun-Jong;Kim, Cheol-Hee
    • Journal of Environmental Science International
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    • v.19 no.3
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    • pp.331-342
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    • 2010
  • Aerosol physical properties have been measured at Pusan National University by using the 16-channel LPC(Laser Particle Counter), and particle characteristics have been examined for the period from Aug. 4 2007 to Dec. 30, 2008. Annual total average, seasonal average, and other averages of the meteorologically classified four categories such as Asian dust, precipitation, foggy, and clear days are respectively described here. Both annually and seasonally averaged number concentration show three peaks at the particle diameter of 0.3, 1.3, and $4{\mu}m$, respectively. However, the first peak for summer season tends to be shifted toward smaller size than other seasons, implying the strong fine particle generation. Meteorological condition shows strong contrast in aerosol concentrations. In Asian dust case, relatively lower number concentrations of fine particles (i.e., smaller than $0.5{\mu}m$) were predominant, while higher concentrations of coarse particles were found particularly for the size bigger than $0.5{\mu}m$. In precipitation day, number concentrations were decreased by approximately 30% due to the removal process of precipitation. Foggy day shows significantly higher concentrations for fine particles, implying the importance of the aerosol condensation process of micro-fine-particle growing to fine-particle. Finally the regressed particle size distribution function was fitted optimally with two log-normal distribution, and discussed the similarities and differences among four categorized cases of the Asian dust, precipitation, foggy, and clear days.

The effect of precipitation conditions on the particle size and size distribution of zinc oxide prepared by high temperature precipitation (고온침전반응에 의한 산화아연 제조공정에서 입자의 형상 및 입도분포에 미치는 침전조건의 영향)

  • 주창식
    • Journal of the Korean Graphic Arts Communication Society
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    • v.16 no.2
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    • pp.11-22
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    • 1998
  • For the purpose of preparation of monodispersed spherical zinc oxide fine particles, an experimental research on the preparation of zinc oxide particles from zinc salts solutions by high temperature precipitation reaction was performed. Zinc oxide particles were precipitated from all the precipitation solutions tested if the precipitation temperature was higher than 60$^{\circ}$. As the precipitation temperature Increased until 80$^{\circ}$, the average particle diameter of zinc oxide particles decreased and the narrower particle size distribution were obtained. Spherical zinc oxide fine particles with relatively narrow particle size distribution were precipitated from the ZnSO$_4$ solutions with NaOH as precipitant. Final pH of precipitation solution had an effect on the amount of zinc oxide precipitated, but had no effect on the their particle size or size distribution.

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