• Title/Summary/Keyword: field annealing

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Synthesis and Magnetic Properties of Nano-sized Mn Ferrite Powder and Film

  • Kwon, Woo-Hyun;Lee, Jae-Gwang;Lee, Young-Bae;Chae, Kwang-Pyo
    • Journal of Magnetics
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    • v.16 no.1
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    • pp.27-30
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    • 2011
  • Nano-sized manganese ferrite powders and films, $MnFe_2O_4$, were fabricated by the sol-gel method, and the effects of annealing temperature on the crystallographic and magnetic properties were studied by using X-ray diffractometry, field emission scanning electron microscopy, M$\"{o}$ssbauer spectroscopy, and vibrating sample magnetometry. X-ray diffraction spectroscopy of powder samples annealed above 523 K indicated the presence of spinel structure, and the film samples annealed above 773 K also had spinel structure. The particle size increased with the annealing temperature. For the powder samples, the Mossbauer spectra annealed above 573 K could be fitted as the superposition of two Zeeman sextets due to the tetrahedral and octahedral sites of $Fe^{3+}$ ions. Using the M$\"{o}$ssbauer subspectrum area ratio the cation distribution could be written as ($Mn_{0.52}Fe_{0.48}$) $[Mn_{0.48}Fe_{1.52}]$ $O_4$. However the spectrum annealed at 523 K only showed as a doublet due to a superparamagnetic phase. As the annealing temperature was increased, the saturation magnetization and the corecivity of the powder samples increased, as did the coercivity of film samples.

Efficiency Characteristics of DSSC Using TiO2 Paste for Low Temperature Annealing with TTIP (TTIP가 첨가된 저온소성용 TiO2 Paste를 이용한 DSSC의 효율 특성)

  • Kwon, Sung Yeol;Sim, Chang Soo;Yang, Wook
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.32 no.1
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    • pp.53-57
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    • 2019
  • Recently, the application field of solar panels is increasing. Accordingly, the demand for flexible devices is also steadily increasing. It is therefore necessary to develop $TiO_2$ paste for low-temperature annealing for flexible DSSC fabrication. In this study, the $TiO_2$ paste for low-temperature annealing with varying molar ratio of titanium isopropoxide (TTIP) was prepared, and DSSC was fabricated and its characteristics were compared. As a result, there was no deformation of the particles on the surface in the SEM data. However, the highest open circuit voltage, short circuit current, and fill factor were measured in the DSSC unit cell prepared by adding 0.5 mol of TTIP to the $TiO_2$ paste, and the highest efficiency was 4.148%.

Development of a novel reconstruction method for two-phase flow CT with improved simulated annealing algorithm

  • Yan, Mingfei;Hu, Huasi;Hu, Guang;Liu, Bin;He, Chao;Yi, Qiang
    • Nuclear Engineering and Technology
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    • v.53 no.4
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    • pp.1304-1310
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    • 2021
  • Two-phase flow, especially gas-liquid two-phase flow, has a wide application in industrial field. The diagnosis of two-phase flow parameters, which directly determine the flow and heat transfer characteristics, plays an important role in providing the design reference and ensuring the security of online operation of two-phase flow system. Computer tomography (CT) is a good way to diagnose such parameters with imaging method. This paper has proposed a novel image reconstruction method for thermal neutron CT of two-phase flow with improved simulated annealing (ISA) algorithm, which makes full use of the prior information of two-phase flow and the advantage of stochastic searching algorithm. The reconstruction results demonstrate that its reconstruction accuracy is much higher than that of the reconstruction algorithm based on weighted total difference minimization with soft-threshold filtering (WTDM-STF). The proposed method can also be applied to other types of two-phase flow CT modalities (such as X(𝛄)-ray, capacitance, resistance and ultrasound).

Dependence of GMI Profile on Size of Co-based Amorphous Ribbon

  • Jin, L.;Yoon, S.S.;Kollu, P.;Kim, C.G.;Suhr, D.S.;Kim, C.O.
    • Journal of Magnetics
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    • v.12 no.1
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    • pp.31-34
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    • 2007
  • The Co-based ribbons with different length were annealed in different magnetic field and GMI profiles were investigated in order to clarify the influence of ribbon size on GMI effect. The GMI ratio decreased with the decreasing in length and also decreased with increasing annealing field. While, the slope of GMI profiles inclined and the field range showing linearity was broadened. It shows prospect to low field sensor, especially for a navigation sensor.

Ferroelectric Properties of PZT thin Films by Rapid Thermal Annealing (RTA처리한 PZT 박막의 강유전 특성)

  • Jeong, Kyu-Won;Park, Young;Ju, Pil-Yeon;Cho, Ik-Hyun;Lim, Dong-Gun;Yi, Jun-Sin;Song, Joon-Tae
    • The Transactions of the Korean Institute of Electrical Engineers C
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    • v.49 no.4
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    • pp.232-238
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    • 2000
  • PZT thin films(3500 ) have been prepared onto $Pt/Ti/SiO_2/Si$ substrates with a RF magnetron sputtering system using PB1.05(Zr0.52,Ti0.48)O3 ceramic target. We used two-step annealing techniques. As the RTA times and temperatures were increased, crystallization of PZT thin films were enhanced. The ferroelectric characteristics of PZT capacitors fabricated at $700^{\circ}C$ for 60 seconds were like these remanent polarization were $12.1 \muC/cm^2$, coercive field were 110 kV/cm, leakage current density were $4.1\times10-7 A/cm^2,\; \varepsilonr=442,$ and remanent polarization were decreased by 22% after 1010 cycles, respectively.

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Poly-Si TFT Fabricated at 170$^{\circ}C$ Using ICP-CVD and Excimer Laser Annealing for Plastic Substrates

  • Han, Sang-Myeon;Shin, Moon-Young;Park, Hyun-Joong;Lee, Hye-Jin;Han, Min-Koo
    • 한국정보디스플레이학회:학술대회논문집
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    • 2004.08a
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    • pp.1003-1006
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    • 2004
  • We have fabricated poly-Si TFTs at 170$^{\circ}C$ using inductively coupled plasma chemical vapor deposition (ICP-CVD) and excimer laser annealing (ELA). A Poly-Si film with large grains exceeding 5000${\AA}$ and a $SiO_2$ film with high breakdown field are deposited by ICP-CVD. A high mobility exceeding 100$cm^2$/Vs with a low sub-threshold swing of 0.76V/dec was obtained.

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A study on characterization of directional coupler using LiNbO$_3$ (LiNbO$_3$ 기판을 이용한 방향성결합형 광 변조기 특성 연구)

  • 강기성;김창원;소대화
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1995.05a
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    • pp.81-85
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    • 1995
  • A guide-wave electro-optical modulatored direct-ional coupler 1X2 was fabricated on LiNbO$_3$ by proton exchange with self-aligned method After proton exchange process, the waveguide is formed by annealing process, The relationship between refractive index change of waveguide and maximun output was studied a long the annealing time. A self-alinged method was used to simplify the fabrication process of the waveguide and the maximize the efficiency of electric field. The modulatored directional coupler 1${\times}$2 has very good figures of merits; The measured crosstalk was -29.5[dB] and the modulating voltage of 8.0[V].

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Magnetic Properties of Clamped Amorphous Transformer Core (주상 변압기용 비정질 코어의 클램핑압력에 따른 자기 특성의 변화)

  • Song, Jae-Sung;Jeong, Soon-Jong;Kim, Ki-Uk;Kim, Byung-Geol;Hwang, See-Dole;Jeong, Young-Ho
    • Proceedings of the KIEE Conference
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    • 1996.07a
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    • pp.196-198
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    • 1996
  • The manufacturing process of the amorphous transformer core consists of winding, cutting, forming, annealing. Clamping of cores during this process are required for shape forming. Clamping of cores enhances the space factor, but degrades the magnetic properties and core loss characteristics of the cores. In this study, we investigated the optimal clamping pressure required in magnetic field annealing of 5 kVA amorphous transformer core.

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Electrical Properties of Plasma Polymerized Hexamethyldisiloxane Thin Film (플라즈마 중합법에 의한 헥사메틸디실록산 박막의 전기적 특성)

  • 이상희;이덕출
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.14 no.1
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    • pp.43-47
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    • 2001
  • Plasma polymerized hexamethyldisiloxane thin film was fabricated by employing an inter-electrode capacitively coupled type apparatus under the following conditions : carrier gas flow rate of 11 sccm, reaction pressure of 0.1 torr, discharge frequency of 13.56 MHz and discharge power of 30∼90 W. Polymerization rate of thin film fabricated at the discharge power of 90W is 32.5nm/min. Relative dielectric constant and dielectric loss tangent of thin film shows 3.2∼3.8 and 2.6x10$\^$-3/∼4.51x10$\^$-3/ respectively in the frequency range of 1 kHz∼1 MHz. As the annealing temperature is increased, the relative dielectric constant gradually decreases while the dielectric loss tangent increases. The current density increase gradually with increasing annealing temperature and electric field. The electric conduction of the heaxamethyldisiloxane thin film shows Schottky effect.

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Breakdown characteristics of gate oxide with tungsten polycide electrode (텅스텐 폴리사이드 전극에 따른 게이트 산화막의 내압 특성)

  • 정회환;이종현;정관수
    • Journal of the Korean Institute of Telematics and Electronics A
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    • v.33A no.12
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    • pp.77-82
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    • 1996
  • The breakdown characteristics of metal-oxide-semiconductor(MOS) capacitors fabricated by Al, polysilicon, and tungsten polycide gate electrodes onto gate oxide was evaluated by time zero dielectric breakdwon (TZDB). The average breakdown field of the gate oxide with tungsten polycide electride was lower than that of the polysilicon electrode. The B model (1~8MV/cm) failure of the gate oxide with tungsten polycide electrode was increased with increasing annealing temperature in the dry $O_{2}$ ambient. This is attributed ot fluorine and tungsten diffusion from thungsten silicide film into the gate oxide, and stress increase of tungsten polcide after annealing treatment.

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