• Composites Research
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• v.29 no.6
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• pp.369-374
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• 2016

In this study, a structural optimal design of 10 MW composite blade was performed using bend-twist coupled(BTC) design concept. Bend-twist coupling of blade means the coupling behavior between the bending and torsional deflections due to the composite lamina with fiber angle biased from the blade longitudinal axis. This can potentially improve the overall performance of composite blade and reduce the dynamic loading. Parametric studies on layup angle, thickness and area of off-axis carbon UD were conducted to find the optimum coupling effect with weight reduction. Comparing the results of fatigue load analysis between conventional model and BTC applied model, the damage equivalent load(DEL) of blade root area were decreased about 3% in BTC model. To verify the BTC effect experimentally, a 1:29 scaled model was fabricated and the torsion at the tip under deflection behavior of blade stiffener model was measured by static load test.

• Macromolecular Research
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• v.12 no.1
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• pp.119-126
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• 2004

In this study, the influence of silane coupling agents, featuring different organo-functional groups on the interlaminar and thermal properties of woven glass fabric-reinforced nylon 6 composites, has been by means of short-beam shear tests, dynamic mechanical analysis, scanning electron microscopy, and thermogravimetric analysis. The results indicate that the fiber-matrix interfacial characteristics obtained using the different analytical methods agree well with each other. The interlaminar shear strengths (ILSS) of glass fabric/nylon 6 composites sized with various silane coupling agents are significantly improved in comparison with that of the composite sized commercially. ILSS of the composites increases in the order: Z-6076 with chloropropyl groups in the silanes > Z-6030 with methacrylate groups> Z-6020 with diamine groups; this trend is similar to that of results found in an earlier study of interfacial shear strength. The dynamic mechanical properties, the fracture surface observations, and the thermal stability also support the interfacial results. The improvement of the interfacial properties may be ascribed to the different chemical reactivities of the reactive amino end groups of nylon 6 and the organo-functional groups located at the ends of the silane chains, which results from the increased chemical reactivity in order chloropropyl > methacrylate > diamine.

• Proceedings of the Korean Fiber Society Conference
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• 2003.10a
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• pp.23-24
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• 2003

We synthesized a poly[2-(2'-hydroxyphenyl) benzoxazole] under the two step procedures of Suzuki coupling polymerization with corresponding monomers followed by the deprotection of benzyl group. The polymer in DMF solution is applicable to colorimetric sensing fluoride anion, which shows a color change from colorless to yellow. High sensitivity to fluoride anion compared to other anions such as phosphate, chloride, and sulfate is ascribed to the high coordination ability of the 2-(2'-hydroxy phenyl)benzoxazole moiety in the polymer chain. Emission shift by metal cations, which can be applied to fluorescent sensing w as also observed in the polymer solution.

• Textile Coloration and Finishing
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• v.15 no.1
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• pp.48-55
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• 2003

As the polyester fiber becomes thinner, thermomigration that is the most important factor deteriorating the washfastness, is more dominant. For improving the washfastness of ultrafine polyester dyed with disperse dye, it is necessary either to decrease the amount of thermomigrated dyes on the fiber surface, or to use a disperse dye containing diester group in the coupling component. This paper is concerned to investigate the relation between the chemical structure of three disperse dyes and their dyeing properties and washfastness. The disperse dye whose molecular size is big, can dye ultrafine polyester with good build-up, and its washfastness is reasonably good. Other disperse dye which has diester group, shows the same dyeing properties as the standard disperse dye, and its washfastness is better than that of the standard disperse dye.

• Journal of Institute of Control, Robotics and Systems
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• v.13 no.3
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• pp.210-217
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• 2007

The theoretical formulations are derived for calculating optical power change for intensity modulated fiber optical microphone. The optical power change is due to optical paths, misalignment and geometry of optical coupler. Based on the theoretical equations, three different optical couplers are simulated with respect to several angles of optical couplers. In order to evaluate the formulation, a multi-mode to multi-mode coupler which is one of abovementioned optical couplers is designed and characterized by carving out both static experiments and dynamic experiments. Considering experimental results, this paper conclude that the theoretical formulations is very useful for design optical coupler and this kind of fiber optic sensor is adequate to microphone.

• Textile Coloration and Finishing
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• v.9 no.5
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• pp.75-81
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• 1997

o-Aminobenzene sulfone-N-ethylanilide, the diazo component of C.I. Acid Red 57, is currently being diazotised by the use of nitrosylsulphuric acid because of its high molecular weight and weak basicity. However, this method has many problems such as complicated manufacturing process and discharge of large volume of strong acidic effluent. In this study, the possibility of replacing nitrosylsulphuric acid method by direct method, which is simpler and produces less effluent, has been checked and the optimum process condition was studied. The effect of HCl concentration, the amount of sodium nitrite and particle size of diazo component on diazotisation yield was investigated. The optimum pH condition for coupling reaction was also evaluated.

• Applied Chemistry for Engineering
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• v.9 no.4
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• pp.603-607
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• 1998

Cellulose was reacted with ethylene oxide to get hydroxyethylcellulose. Quaternary ammonium salt was produced by reaction of epichlorohydrin and trialkylamine. The epoxide ring was opened by acid addition to 3-chloro-2-hydroxypropyltrialkylammonium chloride. Previously unreported two compounds, hydroxyethylcellulose-2-hydroxypropylammonium chloride ether and hydroxyethylcellulose-2-hydroxypropyltriethylammonium chloride ether were synthesized by substitution reaction of hydroxyethylcellulose with glycidyltrialkylammonium chloride or 3-chloro-2-hydroxypropyl-glycidyltrialkylammonium trialkylammonium chloride. All of the compounds including starting materials and reaction intermediates were characterized by $^1H$-NMR and FT-IR spectroscopy.

• Proceedings of the Korean Fiber Society Conference
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• 1987.06b
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• pp.12-12
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• 1987

To improve the fibrillation phenomenon and processibili to of poly(p-phenyleneterephthalamide) (PPD-T) , a P/E copolyamide was prepared by introducing 4,4'-ethylene dianiline (EDA) into rigid chain backbone. The effects of semi-flexible segment on the liquid crystalline properties were investigated. The EDA, used as a comonomer, was prepared by catalylitic reduction of p,p'-dinitrophenyl , obtained by oxidative coupling of p,p'-dinitrotoluene. Various high molecular weight PIE copolyamides were prepared by low temperature solution polycondensation of terephthaloyl chloride (TPC) with various mixtures of p-phenylene diamine (PPD) and EOA. The PfE copolyamides were completely dissolved in 100% svlfuric acid, and the phase transition of P/E copolyamide-sulfuric acid systems was examined in teams of concentration and temperature. Over the chemical compositions, PIE=911, 812, and 713, solutions of anisotropic single phase were acquired. In particular, the two mixing ratios, 911 and 812, gave a good anisotropic spinning dope.

• Proceedings of the Korean Society Of Semiconductor Equipment Technology
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• 2006.05a
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• pp.216-220
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• 2006

평면 광 신호 분리기와 광 케이블의 정밀결합을 위하여 V-groove를 제작하였다. V-groove 는 실리콘웨이퍼 (100) 면을 KOH 용액으로 선택적 습식 식각하여 제작되었다. V-groove 를 효과적으로 제작하기 위하여 KOH 의 조성 (10, 20, 30, 33, 40 wt%)과 온도 (50, 60, 70, $80^{\circ}C$)를 변화시켜 식각률과 표면조도를 측정하였다. 식각률은 $80^{\circ}C$에서 20 wt.% KOH 로 식각했을 경우 $1.84{\mu}m/min$ 로 가장 빨랐으며, 표면조도는 $80^{\circ}C$에서 33 wt.% KOH로 식각했을 경우 1.6nm로 가장 양호하였다.

• Journal of KSNVE
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• v.5 no.2
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• pp.215-224
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• 1995

In this paper, the three-dimensional finite element model is established to investigate the structural dynamic characteristics of rotor blade using a finite element analysis. Six natural frequencies and mode shapes are calculated by computer simulation. The first three flapping modal frequencies, the first two lead-lag modal frequencies, and the first feathering modal frequency are validated through comparison with the modal test results of the fixed rotor blade. The computer simulation results are found in good agreement with experimentally measured natural frequencies. The important results are obtained as follows: (1) Natural frequencies are changed due to the variation of rotational speed and fiber angle of rotor blade, (2) Weak coupling between flapping mode shape and lead-lag mode shape are detected, (3) Centrifugal force has more effect on flapping modal frequency than lead-lag modal frequency.