• Title/Summary/Keyword: faceted phase

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Fluctuation of Solid-Liquid Interface of Faceted Phase and Nonfaceted Phase by Periodic Temperature Variation

  • Oh, Sung-Tag;Kim, Young Do;Song, Young-Jun;Suk, Myung-Jin
    • Korean Journal of Materials Research
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    • v.26 no.11
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    • pp.644-648
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    • 2016
  • In order to examine how the solid-liquid interface responds to temperature variation depending on the materials characteristics, i.e. faceted phase or nonfaceted phase, the moving solid-liquid interface of transparent organic material, as a model substance for metallic materials (pivalic acid, camphene, salol, and camphor-50wt% naphthalene) was observed in-situ. Plots of the interface movement distance against time were obtained. The solid-liquid interface of the nonfaceted phase is atomically rough; it migrates in continuous mode, giving smooth curves of the distance-time plot. This is the case for pivalic acid and camphene. It was expected that the faceted phases would show different types of curves of the distance-time plot because of the atomically smooth solid-liquid interface. However, salol (faceted phase) shows a curve of the distance-time plot as smooth as that of the nonfaceted phases. This indicates that the solid-liquid interface of salol migrates as continuously as that of the nonfaceted phases. This is in contrast with the case of naphthalene, one of the faceted phases, for which the solid-liquid interface migrates in "stop and go" mode, giving a stepwise curve of the distance-time plot.

The effect of grain shape on grain growth behavior of oxide system during liquid phase sintering (산화물계의 액상소결에서 입자 형상이 입자성장 거동에 미치는 영향)

  • 조동희;박상엽
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.11 no.3
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    • pp.127-131
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    • 2001
  • The effect of grain shape on the grain growth behavior of oxide system was investigated as afunction of liquid content during liquid phase sintering. As a model system, the solid grains of $Al_{2}O_{3}$ and MgO were selected during liquid phase sintering, i.e. faceted shape of $Al_{2}O_{3}$ in $CaAl_{2}Si_{2}O_{8}$ liquid phase and spherical shape of MgO in $CaMgSiO_{4}$ liquid phase. The average grain size of MgO with spherical shape was decreased with increasing the liquid phase content, whereas that of $Al_{2}O_{3}$ with faceted shape was independent of liquid phase content. In the case of $Al_{2}O_{3}$ grains with faceted shape, which interfaces are expected to be atomically flat, are likely to grow by the interfacial reaction controled process. Whereas, in the case of MgO grains with spherical shape, which interface are expected to be atomically rough, are likely to grow by the diffusion controlled process.

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Y2BaCuO4 Segregarion , a Possibility of Multi-Seeding and the Origin of Diagonal Line in YBa2Cu3O7-$\delta$ Superconductor Single Crystal (YBa_{2}Cu_{3}O_{7-\delta} 고온초전도체 단결정에서의 Y_{2}BaCuO_{5} 편석과 Multi-Seeding의 가능성, 대각선 흔적의 형성 원인)

  • 성현태
    • Progress in Superconductivity and Cryogenics
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    • v.1 no.1
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    • pp.1-6
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    • 1999
  • The microstructures of top seed mult processde $\textrm{YBa}_2\textrm{Cu}_3\textrm{O}_7$.$\delta$ single crystal were studied. Although shape of the seed was not faceted. the growth shape of Y123 single crystal was faceted. It was observed that Y211 phases were trapped in specific spaces of the faceted region. From the microstructural investigation. it was suggested that the segregation of Y211 is due to the difference of growth rates in crystal direction. When a single crystal was grown by the single seed with stepped multi surfaces. a microstrue was grown from multi-seed. The microstructure show the possibility of multi-seed growth. Corn kernel like structure without Y211 phase was observed and seemed to be formed by the diffusion reaction between Y211 phase in crystal and liquid wetted on the crystal. the diagonal line on Y123 crystal was observed that it was formed by the corn kernel like structure.

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Growth Behavior of (Ti,W)(C,N) and WC grains in a Co Matrix (Co 액상 내에 공존하는 (Ti,W)(C,N)과 WC입자의 성장 거동)

  • 이보아;윤병권;강석중
    • Journal of Powder Materials
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    • v.11 no.2
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    • pp.165-170
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    • 2004
  • Growth behavior of two different types of grains, faceted and rounded, in a liquid matrix has been studied in the (75WC-25TiCN)-30Co system. Powder samples were sintered above the eutectic temperature for various times under a carbon saturated condition. (Ti,W)(C,N) grains with a rounded shape and WC grains with a faceted shape coexisted in the same Co based liquid. With increasing sintering time, the average size of (Ti.W)(C,N) grains increased continuously and very large WC grains appeared. The growth of rounded (Ti,W)(C,N) grains followed a cubic law, r^3-r^3_0$=kt, where r is the average size of the grains, $r_0$ the initial average size, k the proportionality constant and t the sintering time. indicating a diffusion-controlled growth. On the other hand, the growth of the faceted WC grains resulted in a bimodal grain size distribution, showing an abnormal grain growth. These observations show that the growth behavior of different types of grains is governed by their shape, faceted or rounded, even in the same liquid matrix.

Growth Behavior and Mechanisms in Cemented Carbides

  • Yoon, Byung-Kwon;Kang, Suk-Joong L.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.891-892
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    • 2006
  • To test the correlation between grain shape and growth behavior we prepared WC-TiC-Co samples with rounded (Ti, W)C grains and faceted WC grains. The growth of rounded (Ti, W)C grains was normal. In contrast, the growth of faceted WC grains was abnormal or suppressed depending on the initial size of WC particles. These observations were explained using growth theories of crystals in a liquid and were also confirmed by a simulation using their growth equations. The present results thus demonstrate that the growth behavior of carbide grains in a liquid is governed only by their shape, irrespective of the presence of another phase.

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열거식 계층분류체계에 분석합성식 기법의 도입에 관한 연구-KDC를 중심으로

  • 도태현
    • Journal of Korean Library and Information Science Society
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    • v.29
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    • pp.241-272
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    • 1998
  • The purpose of this paper is to examine the analytic-assembling(faceted analysis) methods applied in enumerative-hierarchical classification schemes. (mainly in KDC) The methods are summarized as follows : 1. For the enumerative-hierarchical classification schemes, in principle the subjects are divided into subdivisions by only one facet at the same level, and step by step. However some subjects, for example 'library and information science' 'education' and others in KDC, are divided into subdivisions by multiple facets at same level like Colon Classification. 2. Most of enumerative-hierarchical classification schemes have various kinds of auxiliary tables, such as standard subdivisions, areas, periods, and languages. Each of them is considered as foci by a facet applied to subdivide all kinds of subjects or some special subjects into lower level. 3. To classify the compound subjects with phase relation, KDC provides ready-made classification numbers or notes that says 'divide by 001-999'(whole subjects) of 'divide by xxx-xxx'(limited scope of subjects). The ready-made compound subjects, or subdividing by whole or limited scope of subjects are similar to representation of phase relation in Colon Classification. Yet these analytic-assembling methods in KDC are needed to be supplemented and amended. Subdividing methods for faceted analysis have to be unified through the whole schedule. The auxiliary tables should be enlarged and subdivided more specifically. And for representation of phase relation, the linking signs can be useful in KDC as well as UDC and other analytic-assembling classification schemes like Colon Classification.

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Analysis of Faceted-Reflector Antenna (각면 반사판 안테나의 해석)

  • Kwak, Chang-Soo;Uhm, Man-Seok;Yom, In-Bok
    • Journal of Satellite, Information and Communications
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    • v.5 no.2
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    • pp.34-39
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    • 2010
  • Due to big demand for satellite and communication service using personal handheld terminals, demand for satellites with huge antennas is increasing correspondingly. While such large antennas are realized by various types of deployable antennas, the reflecting surface is made by many facets irrespective of deploying mechanisms. In order to analyze the faceted-reflector more accurately, an existing ray-tracing method is improved. The algorithm allows the rays to cross each other, which is the main characteristic of the faceted-reflector, and takes unevenness of amplitude and phase over the aperture plane into consideration. For the study of the effect of facet configuration, facet generating algorithm is devised. From the analysis algorithm and the facet-generating algorithm, it has been found that the number of facets in a radial direction affects both directivity and sidelobe level. On the other hand, the number of facets in a circumferential direction affects sidelobe level only.

The Grain Growth Mechanism of Sm123 Superconductor in Melt-Textured Growth Method (용융-응고법으로 제조된 Sm123 초전도체의 결정성장 기구)

  • 한상철;성태현;한영희;이준성;김상준
    • Proceedings of the Korea Institute of Applied Superconductivity and Cryogenics Conference
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    • 2001.02a
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    • pp.9-12
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    • 2001
  • The microstructure evolution and the peritectic solidification of Sm$Ba_{2}$$Cu_{3}$ $O_{7-\delta}$ superconducting materials during the isothermal annealing were studied over the temperature range 1030-$1060^{\circ}C$ The faceted growth of the peritectic phase and its dependence upon Sm-diffusion in the liquid phase are discussed. A growth model is proposed to explain the growth shape of Sm123 crystals.

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Influences of Electrochemical Vapor Deposition Conditions on Growth Rate ad Characteristics of YSZ Thin films(II) (YSZ 박막의 성장속도와 특성에 미치는 전기화학증착의 조건의 영향(II))

  • 박동원;전치훈;김대룡
    • Journal of the Korean Ceramic Society
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    • v.33 no.3
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    • pp.355-361
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    • 1996
  • Yttria stabilized zirconia (YSZ) thin films were prepared by the electrochemical vapor deposition (EVD) method on the porous Al2O3 substrates. Y2O3 mol% of thin film was linearly increased with yttrium mole fraction of vapor phase. As yttrium mole fraction(Zyc13=0.18) increased dense and faceted thin films were enhanced. However as the yttrium mole fraction (Zyc13=0.04) decreased porous thin films with monoclinnic phase prevailed. With increasing pressure difference of substrate sides penetration depth decreased porosity and amount of monoclinic phase in the films increased.

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