• 제목/요약/키워드: experimental techniques

검색결과 3,179건 처리시간 0.027초

Experimental Investigation and Quantum Chemical Calculations of Some (Chlorophenyl Isoxazol-5-yl) Methanol Derivatives as Inhibitors for Corrosion of Mild Steel in 1 M HCl Solution

  • Sadeghzadeh, Rogayeh;Ejlali, Ladan;Eshaghi, Moosa;Basharnavaz, Hadi;Seyyedi, Kambiz
    • Corrosion Science and Technology
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    • 제18권5호
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    • pp.155-167
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    • 2019
  • In this study, two novel Schiff base compounds including (3-(4-Chlorophenyl isoxazole-5-yl) methanol and (3-(2,4 dichlorophenol isoxazole-5-yl) methanol as corrosion inhibitors for mild steel in 1 M hydrochloric acid solution were investigated by potentiodynamic polarization, electrochemical impedance spectroscopy (EIS), and density functional theory (DFT) computations. The results showed that the corrosion inhibition efficiency (IE) is remarkably enhanced with the growing concentration of the Schiff base inhibitors. The results from Tafel polarization and EIS methods showed that IE decreases with gradual increments of temperature. This process can be attributed to the displacement of the adsorption/desorption balance and hence to the diminution of the level of a surface coating. Also, the adsorption of two inhibitors over mild steel followed the Langmuir adsorption isotherm. Too, the results of the scanning electron microscope (SEM) images showed that the Schiff base inhibitors form an excellent protective film over mild steel and verified the results by electrochemical techniques. Additionally, the results from the experimental and those from DFT computations are in excellent accordance.

Laser micro-drilling of CNT reinforced polymer nanocomposite: A parametric study using RSM and APSO

  • Lipsamayee Mishra;Trupti Ranjan Mahapatra;Debadutta Mishra;Akshaya Kumar Rout
    • Advances in materials Research
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    • 제13권1호
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    • pp.1-18
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    • 2024
  • The present experimental investigation focuses on finding optimal parametric data-set of laser micro-drilling operation with minimum taper and Heat-affected zone during laser micro-drilling of Carbon Nanotube/Epoxy-based composite materials. Experiments have been conducted as per Box-Behnken design (BBD) techniques considering cutting speed, lamp current, pulse frequency and air pressure as input process parameters. Then, the relationship between control parameters and output responses is developed using second-order nonlinear regression models. The analysis of variance test has also been performed to check the adequacy of the developed mathematical model. Using the Response Surface Methodology (RSM) and an Accelerated particle swarm optimization (APSO) technique, optimum process parameters are evaluated and compared. Moreover, confirmation tests are conducted with the optimal parameter settings obtained from RSM and APSO and improvement in performance parameter is noticed in each case. The optimal process parameter setting obtained from predictive RSM based APSO techniques are speed=150 (m/s), current=22 (amp), pulse frequency (3 kHz), Air pressure (1 kg/cm2) for Taper and speed=150 (m/s), current=22 (amp), pulse frequency (3 kHz), air pressure (3 kg/cm2) for HAZ. From the confirmatory experimental result, it is observed that the APSO metaheuristic algorithm performs efficiently for optimizing the responses during laser micro-drilling process of nanocomposites both in individual and multi-objective optimization.

죽세품 공예디자인 발전을 위한 시장조사 및 실험연구 (A Market and Experimental Research on the Advancement of Bamboo Folkcraft Product Design)

  • 한선주
    • 디자인학연구
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    • 제14권2호
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    • pp.27-36
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    • 2001
  • 본 논문은 전통문화의 현대화, 대중화 차원에서 담양지역의 죽세공예 및 죽세산업에 대해서 소비자 및 생산업체를 대상으로 설문조사 하였으며, 특정 죽세품인 대발을 가지고 다양한 소재, 기법, 디자인을 적용하여 샘플실험 및 작품을 제작하였다. 소비자 대상의 설문조사는 새로운 디자인 개발에 의한 다양한 용도의 제품개발에 대한 매우 높은 선호도 및 구매의사를 보여 향후 신제품 개발 및 디자인 개선의 필요성을 시사하고 있다. 생산업체 또한 새로운 디자인 적용에 의한 신제품개발에 관심이 높으며 전문기관의 디자인 지원을 가장 바라고있었다. 대발개발을 위한 실험조사 결과는 새로운 섬유재료, 천연염색, 현대적 디자인의 조합을 통해 오늘날의 소비자에 소구할 수 있는 제품개발 가능성을 발견하였다. 본 연구는 전통문화의 재창조를 위한 하나의 좋은 사례가 될 것으로 생각되며, 전문기관과 생산업체 간의 산학협동을 통해 전통문화의 제품화·상용화를 기할 수 있다는 점을 제안했다.

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Synthesis and characterization of poly(vinyl-alcohol)-poly(β-cyclodextrin) copolymer membranes for aniline extraction

  • Oughlis-Hammache, F.;Skiba, M.;Hallouard, F.;Moulahcene, L.;Kebiche-Senhadji, O.;Benamor, M.;Lahiani-Skiba, M.
    • Membrane and Water Treatment
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    • 제7권3호
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    • pp.223-240
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    • 2016
  • In this study, poly(vinyl-alcohol) and water insoluble ${\beta}$-cyclodextrin polymer (${\beta}$-CDP) cross-linked with citric acid, have been used as macrocyclic carrier in the preparation of polymer inclusion membranes (PIMs) for aniline (as molecule model) extraction from aqueous media. The obtained membranes were firstly characterized by X-ray diffraction, Fourier transform infrared and water swelling test. The transport of aniline was studied in a two-compartment transport cell under various experimental conditions, such as carrier content in the membranes, stirring rate and initial aniline concentration. The kinetic study was performed and the kinetic parameters were calculated as rate constant (k), permeability coefficient (P) and flux (J). These first results demonstrated the utility of such polymeric membranes for environmental decontamination of toxic organic molecules like aniline. Predictive modeling of transport flux through these materials was then studied using design of experiments; the design chosen was a two level full factorial design $2^k$. An empirical correlation between aniline transport flux and independent variables (Poly ${\beta}$-CD membrane content, agitation speed and initial aniline concentration) was successfully obtained. Statistical analysis showed that initial aniline concentration of the solution was the most important parameter in the study domain. The model revealed the existence of a strong interaction between the Poly ${\beta}$-CD membrane content and the stirring speed of the source solution. The good agreement between the model and the experimental transport data confirms the model's validity.

비행체의 궤적 예측을 위한 순환 신경망 기반 기법들의 정량적 비교 평가에 관한 연구 (Objective Evaluation of Recurrent Neural Network Based Techniques for Trajectory Prediction of Flight Vehicles)

  • 이창진;박인희;정찬호
    • 전기전자학회논문지
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    • 제25권3호
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    • pp.540-543
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    • 2021
  • 본 논문에서는 비행체의 궤적 예측에 적절한 순환 신경망 기반 기법을 탐구하기 위하여 정량적인 비교 평가 연구를 수행하였다. 이를 위해 본 논문에서는 비행체의 궤적 예측 작업을 수행하기 위한 다양한 입력 및 출력 관계들을 정의하고 동일한 실험 환경에서 비교 평가하였다. 특히 비행체 위치의 상대값 기반 입출력 관계를 제안하여 비행체의 궤적 예측에 적합함을 보였다. 또한 비행체 궤적 예측에 효율적인 네트워크 구조 및 하이퍼파라미터를 결정하기 위한 다양한 ablation study(비교 실험)를 진행하였다. 본 논문에서 제시된 정량적 비교 평가 결과는 비행체의 궤적 예측을 위해 순환 신경망 기반 기법을 이용하거나 비행체의 궤적 예측에 특화된 딥러닝 기법을 연구하고자 하는 연구자 및 개발자들에게 실질적인 도움이 될 것으로 예상된다.

뇌졸중 노인에게 PNF의 안정적 반전과 율동적 안정화 기법을 이용한 몸통 안정화 훈련이 몸통 근력과 호흡기능에 미치는 영향 (The Effects of Trunk Stability Exercise Using Stabilizing Reversal and Rhythmic Stabilization Techniques of PNF on Trunk Strength and Respiratory Ability in the Elderly after Stroke)

  • 이영훈;조용호
    • PNF and Movement
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    • 제19권1호
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    • pp.105-113
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    • 2021
  • Purpose: The purpose of this study was to investigate the effect of trunk-stabilization training using stabilizing reversal and rhythmic stabilization techniques of PNF on trunk muscle strength and respiratory function in elderly stroke patients. Methods: There were 26 stroke patients included in the study. Patients were divided into two groups, and all patients performed exercise 30 min five times per week for six weeks. The experimental group performed trunk stability exercise using stabilizing reversal and rhythmic stabilization techniques of PNF, and the control group performed flexibility and strength training. Trunk muscle strength, forced vital capacity, maximum inspiratory pressure, and maximum expiration pressure were measured to determine the changes after the intervention. For statistical processing, a paired t-test was performed within the group, and the value after intervention was performed as an independent t-test to find out the difference between the two groups. Results: In the experimental group, all of the trunk muscle strength, forced vital capacity, maximum inspiratory pressure, and maximum expiration pressure showed significant differences according to the intervention. In the control group, there were statistically significant differences in trunk muscle strength and forced vital capacity, but the maximum inspiratory pressure and the maximum expiration pressure did not show any statistical change. Conclusion: From these results, it can be seen that the trunk stability exercises that use the proprioceptive neuromuscular promotion method of stable reversal and rhythm stabilization can be a good intervention for the respiratory function of stroke patients.

멀티 에이전트 에지 컴퓨팅 환경에서 확장성을 지원하는 딥러닝 기반 동적 스케줄링 (Deep Learning-Based Dynamic Scheduling with Multi-Agents Supporting Scalability in Edge Computing Environments)

  • 임종범
    • 정보처리학회논문지:소프트웨어 및 데이터공학
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    • 제12권9호
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    • pp.399-406
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    • 2023
  • 클라우드 컴퓨팅은 에지 서버가 동작하는 포그(fog) 레이어가 결합된 에지(edge) 컴퓨팅 아키텍처로 진화하고 있다. 에지 컴퓨팅 아키텍처가 관심을 받는 이유는 짧은 통신 지연으로 실시간 IoT 응용을 지원할 수 있기 때문이다. 이와 동시에 인공지능 기술을 도입한 많은 클라우드 작업 스케줄링 기법들이 제안되었다. 인공지능 기반의 클라우드 작업 스케줄링 기법은 기존 기법보다 더 좋은 성능을 보이지만 스케줄링 시간이 다소 소요된다는 단점이 있다. 이 논문에서는 에지 컴퓨팅 환경에서 분산 딥러닝 학습 기반의 동적 스케줄링 기법을 제안한다. 제안하는 기법은 기존 기법보다 스케줄링 시간이 짧은 장점이 있다. 또한 멀티 에이전트를 통한 분산 딥러닝 학습의 효과성을 보이기 위해 확장적인 실험 환경에서 제안 기법과 기존 인공지능 기법의 성능일 비교 평가하였다. 성능 실험 결과 기존 인공지능 기반 클라우드 작업 스케줄링 기법보다 짧은 스케줄링 시간을 보여 IoT 실시간 응용에 적합함을 보였으며, 확장적인 실험에서도 제안 기법이 완료된 작업의 수에 대하여 우수한 성능을 보임을 증명하였다.

딥러닝 기반의 딥 클러스터링 방법에 대한 분석 (Analysis of deep learning-based deep clustering method)

  • 권현;이준
    • 융합보안논문지
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    • 제23권4호
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    • pp.61-70
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    • 2023
  • 클러스터링은 데이터의 정답값(실제값)이 없는 데이터를 기반으로 데이터의 특징벡터의 거리 기반 등으로 군집화를 하는 비지도학습 방법이다. 이 방법은 이미지, 텍스트, 음성 등 다양한 데이터에 대해서 라벨링이 없이 적용할 수 있다는 장점이 있다. 기존 클러스터링을 하기 위해 차원축소 기법을 적용하거나 특정 특징만을 추출하여 군집화하는 방법이 적용되었다. 하지만 딥러닝 기반 모델이 발전하면서 입력 데이터를 잠재 벡터로 표현하는 오토인코더, 생성 적대적 네트워크 등을 통해서 딥 클러스터링의 기술이 연구가 되고 있다. 본 연구에서, 딥러닝 기반의 딥 클러스터링 기법을 제안하였다. 이 방법에서 오토인코더를 이용하여 입력 데이터를 잠재 벡터로 변환하고 이 잠재 벡터를 클러스터 구조에 맞게 벡터 공간을 구성 및 k-평균 클러스터링을 하였다. 실험 환경으로 pytorch 머신러닝 라이브러리를 이용하여 데이터셋으로 MNIST와 Fashion-MNIST을 적용하였다. 모델로는 컨볼루션 신경망 기반인 오토인코더 모델을 사용하였다. 실험결과로 k가 10일 때, MNIST에 대해서 89.42% 정확도를 가졌으며 Fashion-MNIST에 대해서 56.64% 정확도를 가진다.

다구찌 기법과 요인실험의 실험 데이터의 산포 크기에 따라 결과 변화 고찰 (Study on the Result Changes with the Size of the Variance in Taguchi Method and Factor Experimental)

  • 이상복
    • 품질경영학회지
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    • 제41권1호
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    • pp.119-134
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    • 2013
  • Purpose: The purpose of this paper is to show whether the results are changed with respect to the variance of the data, by analysis of data obtained from the Taguchi experimental techniques and general experiment. Because which cannot be prove by mathematical Formula, through experimental examples will show. Methods: Taguchi experiments were carried out with paper Helicopter experiment. Experimental Data are obtained by special designed Drop Test Equipment. While Experimental value arbitrarily changed, we looked at how Significant control Factor of Taguchi Methods and Factor experiments are changed. This process cannot be expressed as a Mathematical formula, but showed as a numerical example. Results: Saw significant changes in the factors when data is outside a certain range of the experimental data. By Test of Equivalence Variance, Experiment data is verified reliability. To find the Control Factor, Taguchi Method is better than the general experiment. Conclusion: We know that a Significant Factor is changed with the range of Variance of Experiment Data. The value of this paper is verified change process with Numerical Data obtained Experiment.

A review of experimental and numerical investigations about crack propagation

  • Sarfarazi, Vahab;Haeri, Hadi
    • Computers and Concrete
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    • 제18권2호
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    • pp.235-266
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    • 2016
  • A rock mass containing non-persistent joints can only fail if the joints propagate and coalesce through an intact rock bridge. Shear strength of rock mass containing non-persistent joints is highly affected by the both, mechanical behavior and geometrical configuration of non-persistent joints located in a rock mass. Existence of rock joints and rock bridges are the most important factors complicating mechanical responses of a rock mass to stress loading. The joint-bridge interaction and bridge failure dominates mechanical behavior of jointed rock masses and the stability of rock excavations. The purpose of this review paper is to present techniques, progresses and the likely future development directions in experimental and numerical modelling of a non-persistent joint failure behaviour. Such investigation is essential to study the fundamental failures occurring in a rock bridge, for assessing anticipated and actual performances of the structures built on or in rock masses. This paper is divided into two sections. In the first part, experimental investigations have been represented followed by a summarized numerical modelling. Experimental results showed failure mechanism of a rock bridge under different loading conditions. Also effects of the number of non-persistent joints, angle between joint and a rock bridge, lengths of the rock bridge and the joint were investigated on the rock bridge failure behaviour. Numerical simulation results are used to validate experimental outputs.