• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2010.06a
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• pp.227-227
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• 2010

The intercalation chemistry of graphite presents an attractive route to obtain few-layered graphene platelets based on the expanded interlayer spacing. We report that the lithium can be intercalated into the graphite in a controllable manner by adjusting the variables such as temperature, pressure, and reaction time. From the X-ray diffraction experiments, the lithium-graphite intercalaltion compounds (Li-GICs) can be produced as the first stage compounds ($LiC_6$), the second-stage compounds ($LiC_{12}$), and the mixtures, which is most likely to be dependent on the temperature and reaction time. Since these Li-GICs are expected to facilitate the exfoliation of graphite, we investigated the feasibility of Li-GICs as a effective precursors for the generation of single-or few-layered graphite nano-platelets.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2010.03b
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• pp.30-30
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• 2010

In order to prepare a epoxy/multilayered silicate nanocomposite, various mixing processes were tried and it was found that the silicate could not be fully exfoliated in the epoxy matrix through various mechanical mixing process. In this study, a new AC electric application method was developed to prepare epoxy/multilayered silicate nanocomposite. The exfoliation of the silicate was confirmed by XRD (X-Ray Diffraction) and TEM observation.

• Journal of the Korean Society of Manufacturing Technology Engineers
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• v.7 no.4
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• pp.117-122
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• 1998

Glass fiber epoxy composite material is widely used in the structures of aircrafts, robots and other machines because of their high specific strength, high specific stiffness and high damping. In order for the composite materials to be used in the aircraft structures or machine elements, accurate surfaces for bearing mounting or joint must be provided, which require precise machining. In this paper, the machinability of the glass fiber epoxy composite material was experimentally investigated. The results can be summarized as follows : 1. The entrance of hole is very good manufacturing existing, but exit come to occur sever surface exfoliation. 2. The cutting force in drilling of the glass fiber epoxy composite material is decreased as the drilling speed increased. 3. If the glass fiber epoxy composite material is drilling by the standard twist drill, then the hole recommand cutting condition is spindle speed 400∼600rpm, feed 40∼50mm/min.

• Bulletin of the Korean Chemical Society
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• v.35 no.7
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• pp.2009-2012
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• 2014

An anionic surfactant, sodium dodecylbenzene sulfonate (SDBS), was introduced during the ultrasonication process for exfoliation of graphene. The surfactant plays the roles of exfoliator and stabilizer by binding to the graphene surface. The obtained modified graphene was characterized by Fourier-transform infrared spectroscopy (FT-IR) and solid state $^{13}C$ CP/MAS NMR to analyze the binding between molecules, and by X-ray diffraction (XRD) to characterize the bulk structure. The resulting graphene exhibited good dispersion stability in both water and organic solvents.

• Proceedings of the Korean Institute of Building Construction Conference
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• v.y2004m10
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• pp.27-30
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• 2004

The objectives of the present study is to solve problems in PC tile before-fixing method using ordinary concrete by adopting the liquefaction method in manufacturing PC to which the tile before-fixing method is applied, and to provide basic information for the practical use of the PC tile before-fixing method, which uses high workable concrete, through manufacturing a complex body based on the optimal mix proportion,

• Proceedings of the Korean Institute of Building Construction Conference
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• 2008.05a
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• pp.73-77
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• 2008

In this study, we would like to study on the application of roof exposure waterproofing method of joint stability through shiplap rubberized asphalt color sheet to complement problem of fracture, exfoliation and water leakage by existing roof exposure sheet waterproofing material joint weakness. Accordingly, examined basis performance and stability for joint that shiplap rubberized asphalt color sheet through test of that tensile strength, bonding strength, water permeability after bonding, peel resistance after bonding, lengthen resistance after bonding and hang resistance after bonding. The results of this study, waterproofing method to using shiplap rubberized asphalt color sheet is judged to solved fracture, exfoliation and water leakage problems happened in joint by problem was joint of exposure sheet by minimizing gap of joint being integration by shiplap.

• Journal of the Korean Society for Precision Engineering
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• v.15 no.10
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• pp.203-208
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• 1998

Carbon fiber epoxy composite materials are widely used in the structures of aircrafts, robots and other machines because of their high specific strength, high specific stiffness and high damping. In order for the composite materials to be used in the aircraft structures or machine elements, accurate surfaces for bearing mounting or joints must be provided, which require precise machining. In this paper, the machinability characterisitcs of the drilling operation of the carbon fiber epoxy composite materials was experimentally investigated. The experimental results are as follows 1.The entrance of hole is very good manufacturing existing, but exit come to occur sever surface exfoliation. 2. The cutting force in drilling of the carbon fiber epoxy composite materials is decreased as the drilling speed increased. 3.The hole of the carbon fiber epoxy composite materials is not good manufacturing by use of the standard twist, therefore, the new drill designed in order to accurate hole.

• Bulletin of the Korean Chemical Society
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• v.33 no.1
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• pp.209-214
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• 2012

In this work, the reduced graphene nanosheets were synthesized from pre-exfoliated graphite flakes. The pristine graphite flakes were firstly pre-exfoliated to graphite nanoplatelets in the presence of acetic acid. The obtained graphite nanoplatelets were treated by Hummer's method to produce graphite oxide sheets and were finally exfoliated to graphene nanosheets by ultrasonication and reduction processes. The prepared graphene nanosheets were studied by X-ray photoelectron spectroscopy (XPS), X-ray diffraction (XRD), atomic force microscopy (AFM), and transmission electron microscopy (TEM). From the results, it was found that the preexfoliation process showed significant influence on preparation of graphite oxide sheets and graphene nanosheets. The prepared graphene nanosheets were applied to the preparation of conductive materials, which yielded a greatly improved electrical resistance of $200{\Omega}/sq$.

• Bulletin of the Korean Chemical Society
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• v.31 no.11
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• pp.3225-3227
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• 2010

The thermal conductivity of layered metal chalcogenides such as $MT_2$ (M = Mo, W; T = S, Se) shows a marked decrease after exfoliation and subsequent restacking process. Random stacking of two-dimensional crystalline sheets circumvents thermal conduction pathways along a longitudinal direction, which results in a reduction in thermal conductivity. $WS_2$ and $WSe_2$ compounds retain p-type conducting behavior after exfoliation and restacking with decreased electrical conductivity due to the change in carrier concentration. $MoSe_2$ compound exhibits metallic behavior < $130^{\circ}C$ with a small Seebeck coefficient, which results from metastable 1T-$MoSe_2$ structure of the restacked phase.

• Corrosion Science and Technology
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• v.9 no.6
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• pp.265-269
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• 2010

This paper describes the exfoliation and surface modification of muscovite mica for UV coating formulation. For the exfoliation of the mica, hydrothermal process was used in the presence of lithium nitrate ($LiNO_3$). After the cation exchange with $Li^+$ ions, the surface of the mica was modified with several amphiphilic substances to increase compatibility and storage stability in UV coating formulation. Such a hydrophobic surface modification affected colloidal stability as well as dispersibility of the exfoliated mica in UV coating solution. Anticorrosive property of mica/UV coated steel plates was tested by salt spray test (SST) and compared with sodium montmorillonite ($Na^+$-MMT)/UV coated steel plates.