• Journal of Pharmaceutical Investigation
• /
• v.37 no.2
• /
• pp.113-117
• /
• 2007

The aim of this study was to investigate the effect of different wall material on the microencapsulation efficiency of microcapsules containing fish oil. The present work reports on the microencapsulation of fish oil by spray drying using hydroxypropyl methylcellulose (HPMC) 2910, maltodextrin, gelatin, sodium caseinate as wall materials. The emulsion stability was assessed by emulsion stability index value (ESI). The microstructural properties of microcapsules was evaluated by scanning electron microscopy (SEM) and microencapsulation efficiency (ME) was assessed by soxhlet method. The highest ESI and ME were observed in the case of a 1:1 gelatin/sodium caseinate ratio and 1:1 glycerin fatty acid ester/lecithin ratio, and ME of microcapsules was increased with increasing the ESI of emulsion. Thus, the stability of emulsion was a critical factor for the encapsulation of fish oil.

• Journal of the Korean Society of Clothing and Textiles
• /
• v.2 no.2
• /
• pp.245-252
• /
• 1978

In order to obtain some information for solvent dyeing, polyethylene terephthalate (PET) was treated with water, tetrachloroethylene yarn (TCE), and water/TCE emulsion for three hours at the temperatures from $40^{\circ}$ to $140^{\circ}C$. The change of fine structure of substratum by measuring the shrinkage, the degree of crystallinity, the stress relacxation modulus and Young's modulus. The P.E.T. film was also treated in water (at $140^{\circ}C$) for 4 hours to stabilize the substratum. By means of film roll cyliderical method, the Disperse Blue 27 was diffused. Then, calculated the diffusion coefficient and examined the application of WLF equation. However, the temperature dependence of the shrinkage could be explain with WLF equation, the diffusion coefficient couldn't be applied the WLF equation when the substratum was stabilized. From the result, the effects on shrinkage were in the order of water

• Explosives and Blasting
• /
• v.19 no.1
• /
• pp.31-40
• /
• 2001

일반적으로 장공발파(長孔發破) 방법(Long hole blasting method)은 그동안 주로 대규모 채탄막장이나 댐 기초굴착, 광산 등에서 행하여져 왔으나 최근 토목터널에서 시공 효율성 및 경제성을 목적으로 관심이 높아지고 있다. 기존의 터널설계 패턴은 I -Type을 기준으로 3.5~3.8m 천공이며 신공법 적용시 최대 4.Om까지 설계되는 것이 보통이었다. 과거 착암장비는 천공장이 늘어남으로서 슬러지에 의한 천공속도가 저하되어 천공비가 증가하기 때문에 빠른 슬러지 배제가 필요하고 Rod의 휨 현상에 의한 천공오차의 증대를 초래할 수 있는 단점이 있었다. 그러나 최근 장비의 발달로 인하여 천공각도 및 천공장 등을 Computer로 모니터링하여 제어할 수 있어 정밀한 천공이 가능하여 졌고 또한, 고성능 에멀젼계 폭약(Super Emulsion)의 개발로 그동안 극 경암터널에서 에멀젼계 폭약의 단점으로 여겨졌던 비 장약량의 증대와 사압현상의 발생, 굴진효율 저하문제론 극복할 수 있었다. 따라서 본 연구는 현재 건설중인 대상현장을 중심으로 장공 터널발파의 효율성과 경제성을 분석하고 나아가 암질에 따른 새로운 Type별 설계기준을 마련하는 기초자료로서 활용하고자 하였다. 된 연구의 대상현장은 충북 괴산군 영풍면 소재 중부내륙(여주-구미간) 고속도로 제 9공구 이화터널 건설공사현장으로 $\varphi{102mm}$ 무 장약공 Cylinder 4공을 이용한 심발법을 사용하였으며 천공장은 최대 5.0m로 2000년 11일 15일에서 동년 12월 15일까지 31일간 총 112회의 시험발파를 실시하여 평균 92%의 높은 굴진 효율을 기록하였다.

• Journal of Powder Materials
• /
• v.9 no.2
• /
• pp.89-95
• /
• 2002

Spherical fine powders of tungsten oxide powders were prepared by the emulsion evaporation method. The characteristics of the powders prepared were examined by means of TGA, X-ray diffraction, SEM and image analysis. The emulsions were prepared by fast mixing of aqueous phase containing tugsten and the organic phase which composed of kerosene, surfactant, and paraffin oil. Precursors were made by evaporating the emulsionin the kerosene bath at $160^{\circ}C$, and then calcined at $650^{\circ}C$ in order to produce tungsten oxide powders. The average particle size of the tungsten oxide powders was $0.5\mutextrm{m}$ and their shapes were spherical at the both case of w/o and o/w type emulsions. As the HLB value of the surfactant increased and the concentration of tungsten ions decreased the mean particle siqe of tungsten oxide powders decreased whereas agglomerationsize increased. The optimum concentration of Span 80 was 8 percent by volume, and the optimum stirring speed in the emulsion formation was 5000 rpm in order to obtain fine and well dispersed $WO_3$ powders.

• International Journal of Advanced Culture Technology
• /
• v.3 no.1
• /
• pp.13-20
• /
• 2015

The self-cleaning properties of nano-zinc oxide on cotton fabrics have been investigated. The cotton fabric has been prepared by pad-dry method. The nano-zinc oxide was encapsulated in the polystyrene particle by mini-emulsion process prior used. The loading amount of zinc oxide particles into the mini-emulsion were various from 1% wt to 40%wt. The particles sizes of ZnO-encapsulated polystyrene mini-emulsion were determined using dynamic light scattering. It was showed that the particle size of the mini-emulsion was in the range of 124-205 nm. The topography and morphology of ZnO-encapsulated polystyrene which coated on cotton fabrics was observed using scanning electron microscopy. The crystal structure of ZnO-coated on cotton fabrics was explored by X-ray diffraction spectroscopy. The photocatalytic activities of zinc oxide were present through the self-cleaning properties. The presents of the zinc oxide on cotton fabrics significantly showed the improving of the self-cleaning properties under UV radiation.

• Journal of the Society of Cosmetic Scientists of Korea
• /
• v.21 no.2
• /
• pp.49-56
• /
• 1995

Chitosan microcapsules and microbeads were prepared by W/O emulsion method, and their morphologies were observed through SEM. The microcapsules have skin layer of 8 Um and 250 Um of mean diameter, The swelling test showed higher s welling ability in protic solvents than in aphotic solvents. After containing moth-yl violet in the microcapsules, the release patterns were investigated. The results sho wed that the addition of Iysozyme in pH 5.1 acetate buffer accelerated the re-lease rate. In case of the microbeads, the mean diameter was about 70 Um. The surface of the microbeads showed porous structures. The swelling ability of the beads revealed two times higher than the one of the microcapsules.

• Journal of the Korean Society of Food Culture
• /
• v.38 no.5
• /
• pp.356-364
• /
• 2023

This study compared the physicochemical properties of soybean curd residue and black soybean curd residue produced by hot air-drying and freeze-drying. Regardless of drying method, the crude protein, crude ash, crude fiber contents, pH, L, a, b color values and water soluble index were higher in soybean curd residue, whereas total polyphenol contents and antioxidant activity were higher in black soybean curd residue. Significant differences in water absorption index, oil absorption capacity and emulsion activity were observed between soybean curd residue and black soybean curd residue in freeze-drying. On the other hand, the emulsion stability was not significant difference in both hot-air drying and freeze-drying. The crude protein and crude fiber contents of soybean curd residue were not significant difference between hot-air drying and freeze-drying. Freeze-drying resulted in higher crude ash contents, pH, water absorption index, water soluble index, oil absorption capacity, emulsion activity and emulsion stability than hot-air drying. Hot-air drying have caused significantly higher water contents, water activity, total polyphenol contents and antioxidant activity in soybean curd residue than freeze-drying. In conclusion, soybean type and drying methods affect the physicochemical and quality characteristics of soybean curd residue, which could be important factors in the manufacture of processed foods.

• Proceedings of the Korean Fiber Society Conference
• /
• 2003.04a
• /
• pp.13-16
• /
• 2003

Vinyl acetate monomer can be polymerized through bulk, solution, emulsion, and suspension polymerization processes. However, in the preparation of PVA from bulk or solution polymerization, there are several technical limitations for obtaining high yield and high molecular weight simultaneously. Thus, the improvement of polymerization method is necessary to prepare the PVA with high yield and high molecular weight because that the difficulty in control of high viscosity and in removal of the heat of polymerization, which might lead to side reactions like branching. (omitted)

• Proceedings of the Korean Society of Dyers and Finishers Conference
• /
• 2009.03a
• /
• pp.158-159
• /
• 2009

Conducting polyaniline (PAni)-titanium dioxide ($TiO_2$) nanocomposites have been synthesized by the inverted emulsion polymerization method. The resultant PAni-$TiO_2$ nanocomposites are characterized with their structural, morphological, conducting and optical properties.

• Applied Chemistry for Engineering
• /
• v.9 no.2
• /
• pp.300-305
• /
• 1998

Kinetics of termonomer emulsion polymerization during interval II (i.e, after completion of latex particle formation) were studied through pseudo-homopolymerization (PHP) method. Extended Smith-Ewart equation and equation of instantaneous polymer composition are respectively reduced to the corresponding equation for homopolymerization by defining average rate constants. Average number of radicals per particle and instantaneous polymer compositions were respectively predicted by varying termonomer composition within latex particles for systems containing no more than one growing radical per particle. Styrene-Methyl methacrylate-Acrylonitrile (SMA) system was used for model calculation.