• Bulletin of the Korean Chemical Society
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• v.28 no.4
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• pp.553-556
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• 2007

We previously reported a 27.12 MHz inductively coupled plasma source at atmospheric pressure for atomic emission spectrometry based on polymer microchip plasma technology. For the PDMS polymer microchip plasma, molecular emission was observed, but no metallic detection was done. In this experiment, a lab-made electrothermal vaporizer (ETV) with tantalum coil was connected to the microchip plasma for aqueous sample introduction to detect metal ions. The electrode geometry of this microchip plasma was redesigned for better stability and easy monitoring of emission. The plasma was operated at an rf power of 30-70 W using argon gas at 300 mL/min. Gas kinetic temperatures between 800-3200 K were obtained by measuring OH emission band. Limits of detection of about 20 ng/mL, 96.1 ng/mL, and 1.01 μ g/mL were obtained for alkali metals, Zn, and Pb, respectively, when 10 μ L samples in 0.1% nitric acid were injected into the ETV.

• Nuclear Engineering and Technology
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• v.56 no.4
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• pp.1441-1453
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• 2024

The yield stability of the neutron generator directly affects the accuracy of elemental analysis. This paper presents an industrial fully automatic neutron generator with a 48 mm neutron tube based on PLC to improve the stability and reliability of the neutron generator in industrial applications. By integrating a Kalman Filter with the PID algorithm in a PLC, the neutron yield of the generator is remarkably stabilized, achieving 1 × 10⁸n/s. The neutron generator has been employed for industrial online elemental analysis. The results demonstrate that only a slight fluctuation of ±0.82 % exists in the neutron yield, and the reproducibility of the generator holds at a significant level of 0.05. This improved neutron generator can be applied to the online bulk analysis of carbon in coal-fired power stations and absolute measurement of neutron source emission rate.

• Tunnel and Underground Space
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• v.10 no.1
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• pp.59-69
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• 2000

Acoustic emission is n burst of microseismic waves generated by microscopic failure due to deformation in materials. The study on the detection of initiation and propagation of microcracks from acoustic emission measurement is very important for the evaluation of the stability of underground rock structures by the nondestructive letting method. In this study, acoustic emission was measured under uniaxial stiffness loading test used to obtain the complete stress-strain curves of marble and concrete used as reinforced materials of rock structures. The analysis of acoustic emission parameters and source location were performed to discuss the characteristics of the deformation and failure behavior of rock and concrete. And acoustic emission was measured under cyclic loading test to verify the Kaiser effect associated with the damage of materials, in situ stress of rock, and stress history of concrete structure.

• Journal of the Korean Vacuum Society
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• v.9 no.2
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• pp.122-129
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• 2000

Field emission behavior from vitreous carbon powders deposited on Mo coated glass by electro-phoretic method was investigated. Although the vitreous carbon has only $sp^2$ hybridized carbon bond, we could observe an excellent field emission behavior. Reproducible electron emission was observed without initiation process which is known to be needed in most carbon cathode materials. Critical electric field for electron emission was in the range from 3 to 4 MV/m. The effective work function was estimated to be about 0.06 eV, as obtained from the slope of Fowler-Nordheim plot. The stability of the emission behavior characterized by repeated I-V measurements, was much superior to the Si tips. We observed the possibility of full area light emission in vitreous carbon materials. This results showed that the field emission is not intimately related to the $sp^3$ hybridization of carbon, but the electrical properties of cathod/electrode interface or the conductivity of the cathode materials which required for the electron transport to the cathode surface.

• 한국정보디스플레이학회:학술대회논문집
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• 2004.08a
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• pp.582-584
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• 2004

The light-emitting properties of poly(2-triethylgermyl-1,4-phenylenevinylene) (TEG-PPV) are compared with those of the silyl-substituted PPV homologue, poly(2-trimethylsilyl-1,4phenylenevinylene) (TMS-PPV). The precursor polymer is solution-processable. After carrying out thermal elimination on the precursor polymer film, the resulting fully conjugated polymer film was found to exhibit high thermal stability in air, and absorption that is shifted to the longer wavelength region owing to the extension of the n-conjugated system. TEG-PPV exhibits efficient green light emission; the maximum PL emission of a TEG-PPV thin film was found to be at 515 nm. The HOMO and LUMO energy levels were also determined using photo-emission spectroscopy. The performance of the TEG-PPV EL device was found to be comparable to that of the TMS-PPV device.

• Proceedings of the Korean Society of Machine Tool Engineers Conference
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• 2004.04a
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• pp.508-512
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• 2004

An ultra-sharp tungsten electrode for field emission was manufactured by using an electrochemical etching method, and its beam characteristics were investigated. KOH and NaOH were the electrolytes used in this research, and the taper length of the tip varied form 150 $\mu\textrm{m}$ to 250 $\mu\textrm{m}$ according to the applied voltage and the concentration of the electrolyte. The electron-beam stability was measured to be within 5% for a total emission current of 5 ${\mu}\textrm{A}$ during 4 hours of operation, and the Ignition voltages were found to be ∼300 V. The tip radius was experimentally found to be 250${\AA}$ from a linear fitting of Fowler-Nordheim plots, which was in remarkably good agreement with that of the image size from scanning ion-microscopy.

• Journal of the Korean Society for Precision Engineering
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• v.16 no.1 s.94
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• pp.26-33
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• 1999

Automatic monitoring of cutting process is one of the most important technologies for increasing the stability and the reliability of unmanned manufacturing system. In this study, basic methods which use the acoustic emission (AE) signals and cutting forces were proposed to monitor flank wear (width of flank wear) quantiatively. First, in order to detect flank wear, it was investigated that the influence of cutting conditions, that is, cutting velocity, feed and depth of cut, on AE signals (${AE_rms}$) and cutting forces. Furthermore, the relation between flank wear and the measured signals (${AE_rms}$, cutting force) was discussed.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.27 no.5
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• pp.312-316
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• 2014

Photoemission is a process in which photons are converted into free electrons. Photocathodes are the typical materials for the process. They emit electrons when a light is irradiated upon. The traditional method of manufacturing photocathodes is complicated, requires specialized equipment, and is limited very small sized samples. $Cs_3Sb$ photocathode was formed on a substrate in $N_2$ atmospheric conditions. The photocathode formation was a gas phase reaction with the substrate. Vacuum devices were made to test electron emission characteristics of the formed photocathode. Visible light of wavelength 475 nm was used for the primary light source. The results showed high current density and long term stability of the photoelectron emission.

• Journal of the Korean Society of Combustion
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• v.4 no.2
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• pp.35-41
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• 1999

The purpose of this study is to establish the flame structure and NOx emission characteristics of the swirl flow coaxial diffusion combustion in the model gas turbine combustor. The mean temperature, ion currents and NOx emission measurement technique showed the effect of equivalence ratio into flame length and flame stability. As a result of this study, NOx emission was increased by increasing the equivalence ratio, and the peak value of the NOx was appeared near the flame front.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2002.04b
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• pp.89-92
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• 2002

Carbon nano tubes(CNTs) have been reported as field emission source because has a sharp tip, a high aspect tip, high chemical stability, high mechanical strength and low work function properties. In this study, we fabricated successfully the back-lamp of the I-inch flat type using CNTs, which was grown directly on cathode substrate of sodalime glass at low temperature. The brightness of CNT back-lamp is measured to $14 Kcd/m^{2}$ at $2000V_{dc}$ in spacing of $500{\mu}m$. And, the emission properties of packaged CNT back-lamp was analyzed as function of applying voltage and times.