• Title/Summary/Keyword: effect of heat treatment

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Effect of Washing and Subsequent Heat Treatment on Water Repellency of Silk Fabric Treated with Fluorocarbon Resins

  • Park, Hyei-Ran;Lee, Mun-Cheul
    • Textile Coloration and Finishing
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    • v.24 no.3
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    • pp.173-179
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    • 2012
  • Silk fabric treated with fluorocarbon resins (Asahi Guard AG-7005 and AG-E061) were washed and subsequently heat treated varying the washing cycles and the temperature. After the processing, the water and oil repellencies, and contact angle to water were evaluated. The water and oil repellencies decreased by the washing and recovered by following heat treatment. Also ESCA measurement was carried out to investigate the surface chemical composition of the treated fiber. The $F_1s$ intensity of the treated fabric decreased by the washing and recovered by the subsequent heat treatment. On the other hand, the $O_1s$ intensity increased by the washing and decreased by following heat treatment. From the results, it is clear that change of the water and oil repellencies of the silk fabric treated with fluorocarbon resin occurred by the washing and subsequent heat treatment. Considering a change of the water repellency of the silk fabric treated with fluorocarbon resin, it seems likely that the fluoroalkyl group of the fluorocarbon resin rotates from surface to inside of the fiber by the washing to adapt to the hydrophilic circumstance, and the orientation of the fluoroalkyl groups of the resin disturbed by the washing recovers the orientation to the fiber surface after the subsequent heat treatment.

Effect of Heat Treatment on the Color Change of Blue-Stained Pinus densiflora Boards (열처리에 의한 청변균 변색 소나무 판재의 재색 변화)

  • Lee, Won-Hee;Lim, Ho-Mook;Kang, Ho-Yang
    • Journal of the Korea Furniture Society
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    • v.25 no.4
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    • pp.319-324
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    • 2014
  • Red pine is a popular species for making a cutting board in Korea, but easily sap stained. Heat treatment could improve its quality by darkening and equalizing the color of sap stained wood. The color change of sap stained red pine boards was investigated by heat treatment at $190^{\circ}C$. It was observed that the color of heat treated boards got darker and it made the color of sap stain vanished. A colorimeter was used to measure color indexes. It was revealed that the values of the lightness ($L^*$) and the yellowness ($b^*$) decreased as heat treatment repeated while the values of the redness ($a^*$) increased. The average of the color difference (${\Delta}E^*$) between the control and 1st heat treated boards was 16.1, which could be expressed as 'Extremely different' while that between the 1st and 2nd heat treated boards was 8.3, which could be expressed as 'Considerably different'. The fact that heat treatment equalized the color of boards was confirmed by a statistical analysis.

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Effect of Pre-Treatment Characteristics on the Gas Nitriding of Stainless Steels (스테인리스강의 가스질화에 미치는 전처리의 영향)

  • Kim, H.G.;Kim, Y.H.
    • Journal of the Korean Society for Heat Treatment
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    • v.17 no.5
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    • pp.278-282
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    • 2004
  • Effect of pre-treatment on the gas nitriding process of austenitic stainless steels has been investigated and the following results were obtained. Minimum pre-treatment time was decreased to 5min with increasing treatment temperature from $200^{\circ}C$ to $600^{\circ}C$. Surface activation effect by the pre-treatment was maintained in the air up to holding time of 64hr, judging from the analysis result of gas nitrided specimens. The Depth of nitrided layer of STS 304 and 316 stainless steels were ranged from $5{\mu}m$ to $90{\mu}m$ at $440^{\circ}C{\sim}600^{\circ}C$. The X-ray diffraction intensity for austenitic stainless steels were increases as nitriding temperature from $440^{\circ}C$ to $600^{\circ}C$.

Effect of heat treatment in $HfO_2$ as charge trap with engineered tunnel barrier for nonvolatile memory (비휘발성 메모리 적용을 위한 $SiO_2/Si_3N_4/SiO_2$ 다층 유전막과 $HfO_2$ 전하저장층 구조에서의 열처리 효과)

  • Park, Goon-Ho;Kim, Kwan-Su;Jung, Myung-Ho;Jung, Jong-Wan;Chung, Hong-Bay;Cho, Won-Ju
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2008.11a
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    • pp.24-25
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    • 2008
  • The effect of heat treatment in $HfO_2$ as charge trap with $SiO_2/Si_3N_4/SiO_2$ as tunnel oxide layer in capacitors has been investigated. Rapid thermal annealing (RTA) were carried out at the temperature range of 600 - $900^{\circ}C$. It is found that all devices carried out heat treatment have large threshold voltage shift Especially, device performed heat treatment at $900^{\circ}C$ has been confirmed the largest memory window. Also, Threshold voltage shift of device used conventional $SiO_2$ as tunnel oxide layer was smaller than that with $SiO_2/Si_3N_4/SiO_2$.

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Effect of the Heat treatment and Boron on the Hot Corrosion Resistance of the Al Diffusion Coating (Al 확산피복층의 고온 내식성에 미치는 후열처리와 B첨가의 영향)

  • 김태원;윤재홍;이재현;김현수;변응선
    • Journal of the Korean institute of surface engineering
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    • v.32 no.1
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    • pp.67-77
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    • 1999
  • The Ni base superalloy Mar-M247 substrate was aluminized or aluminized after boronizing by the pack cementation under Ar atmosphere. The hot corrosion resistance and after-heat-treatment effect of aluminized specimens were studied by the cyclic hot corrosion test in $Na_2SO_4$-NaCl molten salt. XRD analysis showed that the $Ni_2Al_3$ phase was formed between the coated layer and substrate below 1273K but the NiAl phase above 1273K. The peak of the NiAl phase was developed after heat treatment. Corrosion test showed that corrosion resistance of the specimen with the NiAl phase was better than that with the $Ni_2Al_3$ phase. Corrosion resistance could be improved by heat treatment to form ductile NiAl phase, where cracks were not formed by thermal shock on coating layer. Moreover, it appeared that heat treatment played a role to improve corrosion resistance of Al diffusion coating above 1273K. The existence of boron in the Al diffusion coating layer obstructed outwared diffusion of Cr from the substrate, and it influenced on corrosion resistance of the coating layer by weakening adherence of the oxide scale.

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The Effect of Cold Working and Heat Treatment on the Magnetic Properties of in-situ Formed Cu-Fe Composites (In-situ 법(法)에 의한 Cu-Fe 복합조직(複合組織)의 자기적(磁氣的) 특성(特性)에 미치는 가공(加工) 및 열처리(熱處理)의 영향(影響))

  • Shur, S.J.;Park, H.S.
    • Journal of the Korean Society for Heat Treatment
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    • v.2 no.2
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    • pp.38-45
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    • 1989
  • The Cu-Fe permanent magnet were prepared in situ process, which has economic and mass productive merits in producing multi filamentary composites. The purpose of this research was to study the effect of reduction ratio and heat treatment on magnetic property. As the reduction ratio of Cu-Fe wire increased, the filament structure became finer and interfilament distances decreased and the morphology of filament cross section became ribbon shape. As Fe content increased significantly. The coercivity and squareness of Cu-55 wt%Fe composite increased as a reduction ratio became higher, whereas they increased to maximum values at 0.09 mm ${\phi}$ for Cu-30 wt%Fe, and 0.066 mm ${\phi}$ for CU-45 wt%Fe respectively, and decreased for further reduction. The magnetic properties of Cu-Fe composites can be more enhanced by intermediate heat treatment. The best magnetic properties were obtained from Cu-55 wt%Fe composite deformed to 0.054 mm ${\phi}$ and annealed.

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Effects of Heat Treatment and Ti addition on Microstructures in Modified Invar Alloys (개량형 인바합금의 미세조직에 미치는 열처리 및 Ti 첨가 영향)

  • Huh, Min-Sun;Lee, Jung-Han;Lee, Chan-Gyu;Lee, Jae-Hyun
    • Journal of the Korean Society for Heat Treatment
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    • v.13 no.6
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    • pp.412-419
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    • 2000
  • There has been a considerable attention on Invar alloys due to its low thermal expansion property. A low thermal expansion property of Invar alloys, lower than $10^{-6}$ near the room temperature, is attractive for electric transmission lines and precision machine tools. However, the expansion property of Invar alloys is limited below about 520K, and mechanical properties are relatively low to apply to electric transmission line. In order to improve mechanical properties in this alloy, Ti alloying element was added to the $Ni_{38}-Mo_2-Cr_1-Fe$ invar alloy. The microstructure Ti added alloy showed finer than that of the unalloyed one. It was found that the (Mo, Ti), Mo carbide formed by Ti addition obstacled grain growth by pinning effect and supplyed recrystallization sites during heat-treatment. Optimum heat-treatment conditions with Ti addition were also discussed in the modified Invar alloy.

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Effect of Heat Treatment Conditions on the Microstructure and Wear Behavior of Ni-based Self-flux Alloy Coatings (니켈기 자융성 합금 코팅층의 미세구조 및 마모거동에 미치는 후열처리 조건의 영향)

  • Kim, K.T.;Oh, M.S.;Kim, Y.S.
    • Journal of Power System Engineering
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    • v.11 no.1
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    • pp.121-126
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    • 2007
  • This study aims at investigating the effect of heat treatment conditions on the dry sliding wear behavior of thermally sprayed Ni-based self-flux alloy coatings. Ni-based self-flux alloy powders were sprayed onto a carbon steel substrate and then heat-treated at 700, 800, 900 and $1000^{\circ}C$ for 30 minutes in a vacuum furnace. Dry sliding wear tests were performed using sliding speed of 0.4 m/s and applied load of 6 N. AISI 52100 ball(diameter 8 mm) was used as counterparts. Microstructure and wear behavior of both as-sprayed and heat-treated Ni-based self-flux alloy coatings were studied using a scanning electron microscope(SEM), energy dispersive X-ray spectroscopy(EDX), electron probe micro-analysis(EPMA) and X-ray diffraction(XRD). It was revealed that microstructure and wear behavior of thermally sprayed Ni-based self-flux alloy coatings were much influenced by heat treatment conditions.

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