• Advanced Composite Materials
• /
• v.16 no.2
• /
• pp.95-113
• /
• 2007

Experimental investigations of interlaminar mechanical properties for carbon fiber reinforced plastic (CFRP) laminates were carried out using aramid fiber ($Kevlar^{(R)}$-29 1000d) and carbon fiber (TR40-1K 612d, Mitsubishi Rayon) stitching. Various carbon fiber (CF) stitch densities were used to prepare a number of CF stitched CFRP laminates for double cantilever beam (DCB) tests. An insert tongue-type loading fixture, developed by the Japan Aerospace Exploration Agency (formerly the National Aerospace Laboratory of Japan), was also employed in the DCB test. Interlaminar tension tests were carried out under an out-of-plane directional loading using a single CF stitch thread in the CFRP laminates. The DCB test results clarified that the relationship between the volume fractions of the CF stitch thread ($V_{ft}$) and mode I critical energy release rate ($G_{Ic}$) showed a mostly linear function with a higher gradient than that of the $Kevlar^{(R)}$ stitched CFRP laminates. The CF stitched CFRP tension test results indicated that the consumption energy per unit area ($E_i$) was larger than that of $Kevlar^{(R)}$ stitched CFRP laminates.

• Journal of the Microelectronics and Packaging Society
• /
• v.26 no.4
• /
• pp.101-105
• /
• 2019

The adhesion reliability of the epoxy molding compound (EMC) and the printed circuit board (PCB) interface is critical to the quality and lifetime of the chip package since the EMC protects PCB from the external environment during the manufacturing, storage, and shipping processes. It is necessary to measure adhesion energy accurately to ensure product reliability by optimizing the manufacturing process during the development phase. This research deals with the measurement of EMC/PCB interfacial adhesion energy of chip package that has warpage induced by the coefficient of thermal expansion (CTE) mismatch. The double cantilever beam (DCB) test was conducted to measure adhesion energy, and the spring back force of specimens with warpage was compensated to calculate adhesion energy since the DCB test requires flat substrates. The result was verified by comparing the adhesion energy of flat chip packages come from the same manufacturing process.

• Composites Research
• /
• v.12 no.5
• /
• pp.40-53
• /
• 1999

The interlaminar facture behavior of multidirectional carbon-fiber/epoxy composite laminates under low and high rates of test, up to rate of about 11.4m/s has been investigated using the double cantilever beam specimens. The mode I loasing with rates above 1.0m/s had considerable dynamic effects on the load-time curves and thus revealed higher values of the average crack velocity than thet expected from a simple proportional relationship with the test rate. The modified beam analysis utilizing only the opening displacement and crack length exhibited an effective means for evaluating the dynamic fracture energy $G_{IC}$. Flexural modulus increased gradually with an increase of the test rate, which was utilized in the evaluation of $G_{IC}$. Values of $G_{IC}$ at the crack initiation and arrest were scarcely changed with increasing test rate up to 1.0m/s. However the maximum $G_{IC}$ was much enlarged at 11.4m/s due to the large amount of fiber bridging the crack tip. The larger the initial crack length, the smaller the maximum $G_{IC}$ at high rate.

• Journal of Surface Science and Engineering
• /
• v.32 no.6
• /
• pp.647-657
• /
• 1999

Due to the inherently poor adhesion strength of Cu-based leadframe/EMC (Epoxy Molding Compound) interface, popcorn cracking of thin plastic packages frequently occurs during the solder reflow process. In the present work, in order to enhance the adhesion strength of Cu-based leadframe/EMC interface, black-oxide layer was formed on the leadframe surface by chemical oxidation of leadframe, and then oxidized leadframe sheets were molded with EMC and machined to form SDCB (Sandwiched Double-Cantilever Beam) and SBN (Sandwiched Brazil-Nut) specimens. SDCB and SBN specimens were designed to measure the adhesion strength between leadframe and EMC in terms of critical energy-release rate under quasi-Mode I ($G_{IC}$ ) and mixed Mode loading ($G_{C}$ /) conditions, respectively. Results showed that black-oxide treatment of Cu-based leadframe initially introduced pebble-like X$C_2$O crystals with smooth facets on its surface, and after the full growth of $Cu_2$O layer, acicular CuO crystals were formed atop of the $Cu_2$O layer. According to the result of SDCB test, $Cu_2$O crystals on the leadframe surface did not increase ($G_{IC}$), however, acicular CuO crystals on the $Cu_2$O layer enhanced $G_{IC}$ considerably. The main reason for the adhesion improvement seems to be associated with the adhesion of CuO to EMC by mechanical interlocking mechanism. On the other hand, as the Mode II component increased, $G_{C}$ was increased, and when the phase angle was -34$^{\circ}$, crack Kinking into EMC was occured.d.

• Journal of the Korean Society of Fisheries and Ocean Technology
• /
• v.19 no.1
• /
• pp.79-84
• /
• 1983

The test specimen, designated the double cantilever beam, was employed for a fracture mechanics study of stress corrosion cracking (SCC) of type 5083 Al-alloy in seawater. Stress intensities for this DCB specimen were calculated by using compliance, strain energy release rate and relation between stress intensity and strain energy release rate. Analytical expression for compliance as a function of crack length was obtained by applying beam theory. It was investigated that the polarization potentials affected the growth rate and surface of stress corrosion cracking. The results are as follows, The critical stress intensity was 134.81-148.38kg/mm super(3/2) and K sub(Ii) under polarization potentials was 75.92-145.78kg/mm super(3/2). The minimum stress corrosion crack growth rate was occurred at-987mV SCE. Insoluble compound on $\beta$ phase was looked into through SCC. The greater anodic potential is, the larger insoluble compound on $\beta$ phase becomes.

• Transactions of the Korean Society of Mechanical Engineers A
• /
• v.28 no.8 s.227
• /
• pp.1109-1115
• /
• 2004

The objective of this study is to elucidate what governs delayed hydride cracking (DHC) in Zr-2.5Nb tubes by correlating the striation spacings with DHCV(DHC Velocity). To this end, DHC tests were conducted on the compact tension specimens taken from the Zr-2.5Nb tubes at different temperatures ranging from 100 to $300^{\circ}C$ with a 3 to 6 data set at each test conditions. The compact tension specimens were electrolytically charged with 27 to 87 ppm H before DHC tests. After DHC tests, the striation spacings and DHCV were determined with the increasing the test temperature and yield strength. The striation spacing and DHCV increased as a function of yield $strength^2$ and the temperature. Since the plastic zone size ahead of the crack tip can be represented by ${\sim}(K_{IH}/{\sigma}_{Y})^2$, we conclude that the striation spacing is governed by the plastic zone size which in turn determines a gradient of hydrogen concentration at the crack tip. The relationship between the plastic zone size and the striation spacing was validated through a complimentary experiment using double cantilever beam specimens. Two main factors to govern DHCV of Zr-2.5Nb tubes are concluded to be hydrogen diffusion and a hydrogen concentration gradient at the crack tip that are controlled by temperature and yield strength, respectively. The activation energy of DHCV in the Zr-2.5Nb tubes is discussed on the basis of temperature dependency of hydrogen diffusion and the striation spacing.

• Nuclear Engineering and Technology
• /
• v.32 no.1
• /
• pp.1-9
• /
• 2000

Delayed hydride cracking (DHC) velocity and threshold stress intensity factor for DHC ($K_{IH}$) tests in the radial direction on M11 pressure tube material in Wolsong unit 1 were carried out following the Atomic Energy Canada Limited (AECL) standard test procedure in order to identify the effect of undercooling on DHCV and to acquire the $K_{IH}$ data. The results showed that $K_{IH}$ 's were 8.8$\pm$0.8 MPa√m in the back offcut and 11.4$\pm$0.7 MPa√m in the front offcut. The fact that $K_{IH}$ in the front offcut is about 20% higher than that in the back offcut is attributed to the microstructural difference between the materials of the front and back ends. $K_{IH}$ 's in M11 pressure tube appeared to be higher than the values from the tubes made of double melted ingot reported earlier. This can be interpreted by the fact that very small amounts of Chlorine (Cl) and Phosphorus (P) are contained in the ingot and that the content of the harmful elements in the M11 pressure tube is equivalent to that made of a quadruple melting process. DHC velocities at 25$0^{\circ}C$ in the front offcut in the radial direction are measured to be 5~8$\times$10$^{-8}$ m/s. The results show that the prior thermal history change the DHC velocity significantly. This effect was confirmed by the experiment of undercooling prior to the DHC tests.DHC tests.

• Transactions of the Korean Society of Mechanical Engineers A
• /
• v.37 no.4
• /
• pp.497-502
• /
• 2013

In this study, the interlaminar fracture toughness in mode I of a hybrid composite inserted with different types of non-woven tissues was determined. The interlaminar fracture toughness in mode I is obtained by a double cantilever beam test. The experiment is performed using three types of non-woven tissues: 8 $g/m^2$ of carbon tissue, 10 $g/m^2$ of glass tissue, and 8 $g/m^2$ of polyester tissue. Considering a specimen with no non-woven tissue as a reference, the interlaminar fracture toughness in mode I of specimens inserted with non-woven carbon and glass tissues decreases by as much as 6.3% and 11.4%, respectively. However, the fracture toughness of a hybrid composite specimen inserted with non-woven polyester tissue increases by as much as 69.4%. It is considered that the specimen inserted with non-woven polyester tissue becomes cheaper, and lighter, and the value of the fracture toughness becomes much greater than that of the non-woven carbon tissue.