• Fibers and Polymers
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• 제6권3호
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• pp.206-218
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• 2005

Structural studies of series of 'as spun' and drawn PEEK fibers have been carried out using X-ray diffraction and optical microscopy techniques. The analysis of results suggest that fibers produced at a constant draw ratio with increasing draw temperatures show enhanced orientation and crystalline behaviour. The resolved equatorial and meridional traces provide additional structural parameters in terms of crystallinity, crystallite size, and crystallite thickness. It is concluded that drawing at a temperature below $T_g(i.e.,\;144^{\circ}C)$ results in poorly oriented non-crystalline materials, whereas drawing above $T_g$ results in highly oriented semi crystalline materials. Additional drawing proved to increase the overall orientation with slight improvements in lateral order of the chain molecules. Quantitative analysis revealed that the crystallite size increases with increasing drawing temperature. The results also revealed the increased crystallite size upon additional drawing. Crystalline orientation parameter, $_c$, suggests almost perfect orientation. In all cases, the amorphous orientation is found to be lower than the overall orientation parameter obtained from the optical birefringence. As a result of additional drawing, crystalline orientation was found to increase slightly but the increase in the orientation of non-crystalline material was found to be substantial. An average crystalline density was determined from the orthorhombic unit cell dimensions. It was found to vary as a result of processing conditions. It was also found that the value of the maximum birefringence shows heavy dependence on the chain conformation.

• 대한기계학회논문집A
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• 제26권8호
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• pp.1645-1652
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• 2002

The failure analysis on fractured parts is divided into the qualitative method by naked eyes and metallurgical microscope etc. and the quantitative method by SEM and X-ray diffraction etc. X-ray fractography can be applied to contaminated surface as well as clean surface and gain the plastic deformation and the residual stress near the fractured surface. Turbine blade is subject to cyclic bending force by steam pressure and suffers fatigue damage according to the increasing operating time. Therefore, to clean up the fracture mechanism of torsion-mounted blade in nuclear plant, the fatigue and the X-ray diffraction test was performed on the 12%Cr steel fur turbine blade and the fractured parts. The correlation of X-ray parameter and fracture mechanics parameter was determined, and then the load applied to actual broken turbine blade was predicted. Failure analysis was performed by contact stress analysis and Goodman diagram of torsion-mounted blade.

• 한국해양공학회지
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• 제34권4호
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• pp.245-252
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• 2020

Wave run-up is an important phenomenon that should be considered in ocean structure design. In this study, the wave run-up of a surface-piercing circular cylinder was calculated in the time domain using the three-dimensional linear and fully nonlinear numerical wave tank (NWT) techniques. The NWT was based on the boundary element method and the mixed Eulerian and Lagrangian method. Stokes second-order waves were applied to evaluate the effect of the nonlinear waves on wave run-up, and an artificial damping zone was adopted to reduce the amount of reflected and re-reflected waves from the sidewall of the NWT. Parametric studies were conducted to determine the effect of wavelength, wave steepness, and the draft of the cylinder on the wave run-up of the cylinder. The maximum wave run-up value occurred at 0°, which was in front of the cylinder, and the minimum value occurred near the circumferential angle of 135°. As the diffraction parameter increased, the wave run-up increased up to 1.7 times the wave height. Furthermore, the wave run-up was 4% higher than the linear wave when the wave steepness was 1/35. In particular, the crest height of the wave run-up increased by 8%.

• Applied Microscopy
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• 제44권4호
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• pp.144-149
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• 2014

A strategy for phase identification of precipitates in high Al-containing austenitic and ferritic steels using electron diffraction (ED) is studied. Comparative studies of the various Al-containing precipitates (k-carbide, $Ni_3Al$, $Fe_3Al$, FeAl) show the similarities of crystal structure and lattice parameter. However, the slight differences of lattice parameter and structure display characteristic ED patterns (EDPs) which can be identified. $L1_2$ k-carbide and $Ni_3Al$ can be differentiated by the length of ${\rightarrow}_g$ (the reciprocal lattice vector), even though they show perfectly identical shapes of EDPs. $DO_3$ $Fe_3Al$ and $B_2$ FeAl show the characteristic EDs in [110] and [112] beam directions due to the differences of Fe site occupancies in unit cells. k-carbide, $Ni_3Al$, and FeAl show also the similar EDs in [112], [112], and [110] beam directions, respectively. All the possible similarities of EDs among each phases and the strategy for phase identification are discussed on the bases of kinematical ED simulation.

• Journal of applied mathematics & informatics
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• 제26권1_2호
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• pp.45-60
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• 2008

Here we consider the evaluation of the the dynamic component of the second order force due to wave diffraction by a circular cylinder analytically and numerically. The cylinder is fixed, vertical, surface piercing in water of finite uniform depth. The formulation of the wave-structure interaction is based on the assumption of a homogeneous, ideal, incompressible, and inviscid fluid. The nonlinearity in the wave-structure interaction problem arises from the free surface boundary conditions, namely, dynamic and kinematic free surface boundary conditions. We expand the velocity potential and free surface elevation functions in terms of a small parameter and then consider the second order diffraction problem. After deriving the pressure using Bernoulli's equation, we obtain the analytical expression for the dynamic component of the second order force on the cylinder by integrating the pressure over the wetted surface. The computation of the dynamic force component requires only the first order velocity potential. Numerical results for the dynamic force component are presented.

• Applied Microscopy
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• 제41권1호
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• pp.75-79
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• 2011

For quantitative analysis of nano-crystal structure, we reported the accuracy improvement method of lattice parameters measured from electron diffraction. For calculation of Au lattice parameters used as a standard crystal structure, it was considered two different acquisition methods (detector and enegy-filter) and three different calculation methods (conventional, least-square and regression fit). As a result, the measurement reliability could be enhanced by using CCD camera which gives higher performance, while energy-filtering did not affect the improvement the camera constant accuracy. Also, the accuracy of lattice parameters could be improved up to $10^{-4}$ order by regression fitting with correction formula. Finally, it is expected that the combination of regression fitting and intensity extraction from energy-filtered precession electron diffraction gives a solution of quantitative structure analysis for unknown nano-crystals.

• 한국광학회지
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• 제3권3호
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• pp.148-154
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• 1992

홀로 그래피 은염 감광 물질에 위상형 회절격차를 기록하여 71%가 넘는 회절 효율을 얻었다. 화학적 처리가 끝난 후 전자 주사 현미경을 통해 Agfa 8E75 감광유제의 부풀은 모습을 밝혔다. 비경화 정착액, 중크롬산 표백액과 알코올에 의한 급속 전조가 강한 변조효과를 가져와 회절 효율이 20% 이상 증가하였다. Kogelnik 결합과 이론의 중요한 특성 파라미터들에 대해 검토하였으며, 두께 변화에 따른 새로운 파라미터 값을 컴퓨터 시뮬레이션을 통해 제시하였다. 결론적으로 감광유제의 정밀한 두께 제어가 고회절 효율을 얻기 위한 잠재적인 원천으로 작용함을 보였다.

• 한국환경보건학회지
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• 제24권2호
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• pp.145-150
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• 1998

This study was carried out to investigate the loss amount of collection at the different of precipitatation time, high voltage and gas speed. This work has focused on the dependence of the collection efficiency in the collector zone with gas speed and high voltage. This advanced Model is developed by research of the different parameter as the conventionnal modem of study. In order to investigate collection efficiency of electrostatic precipitator, the loss amount of knocking was measured with Monitek-Treubung and the particle size was analyzed by He-Ne laser diffraction spectroscopy.

• 한국결정성장학회지
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• 제21권4호
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• pp.169-174
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• 2011

합성된 biphasic calcium phosphate(BCP) 분말의 나노크기 생분해성 거동은 X-선 회절 분석방법, 격자 매개변수 및 전계방출형 주사전자현미경을 통해 특성평가 하였다. BCP 분발은 공침반응 및 하소과정을 통해 합성하였고, 합성된 분발은 행크 용액 (pH = 7.4, $36.5^{\circ}C$)을 이용하여 3주 동안 in vitro 시험 하였다 분해 시험(in vitro) 후, BCP 단위포의 매개변수는 a 및 c축의 불규칙한 변화와 비슷한 격자 왜곡 및 팽창 거동을 보였다.

• 한국정밀공학회지
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• 제19권4호
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• pp.117-123
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• 2002

X-ray diffraction observation of fracture surfaces yields useful information to analyze the causes of failure accidents of engineering structures. This experimental technique, named X-ray fractography, has been developed especially in metal and mechanical engineering fields. The distributions of the residual stress and the half value breadth of diffraction profiles beneath the fatigue fracture surface were measured with SNCM 439, HT100 and Ti-6Al-4V alloy. The size of the maximum plastic zone was successfully determined on the basis of the measured distributions. This size was correlated to maximum stress intensity factor. The distributions of the half value breadth of diffraction profiles on the fatigue fracture surfaces were measured with SNCM 439. HT100. The equations of x-ray parameter distribution were possible to estimated fracture parameters of fatigue fracture surfaces.