• 한국세라믹학회지
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• 제31권2호
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• pp.129-136
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• 1994

Si3N4 with 6w/o Y2O3 and 1.5w/o Al2O3 has been gas pressure sintered and its densification behavior and the effect of the sintering variables on the microstructure and mechanical properties were investigated. Densification rate was higher at temperature below 1775$^{\circ}C$ and between 187$0^{\circ}C$ and 195$0^{\circ}C$ than between 1775$^{\circ}C$ and 187$0^{\circ}C$. The faster densification at temperature between 187$0^{\circ}C$ and 195$0^{\circ}C$ was thought to be due to the increased amount of liquid phase resulting from the increased amount of Si3N4 dissolving in the liquid. $\beta$-Si3N4 and Y-disilicate at temperatures below 1775$^{\circ}C$, and only $\beta$-Si3N4 at 187$0^{\circ}C$ and above were detected by XRD analysis. Three different two-step schedules were employed to obtain sintered body with above 99% theoretical density and to investigate the effect of the sintering variables on the density, the microstructure and the mechanical properties of the sintered body. The sintered density did not change with the heating rate, and the microstructure became coarser as the temperature increased. The strength decreased with the width of $\beta$-Si3N4 grain, while the fracture toughness increased with the square root of it. A ceramic cutting tool made of the sintered body showed an uniform flank wear after the cutting test.

• 한국세라믹학회지
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• 제35권7호
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• pp.740-748
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• 1998

The inertia friction properties of C/C composites manufactured by the processes of pressure and at-mospheric carbonizaton with a commerciallized and two kinds of modified coal-tar pitch as a matrix pre-cursor were investigated. The modifications of a pitch such as the introduction of mesophase and the ad-dition of sulphur into a raw pitch were not effective for a impregnation efficiency conducted in a vacuum and at the same time in a pressure of 5kg/cm2 due to the increase of the pitch viscosity. There was not a difference in the densification increment between the pitch modifications however it was revealed that a pressure carbonization was more advantageous than an atmospheric in the densification and the formation of anisotropic carbon matrix. The friction and wear propertis of C/C having higher degree of matrix cry-stallization higher density and hardness of friction surface showed superiority. As the braking energy was increased the friction coefficients were decreased and reached almost same level at the high kinetic energy of 99.6kJ. The wear trends at 99.6kJ were different from the behaviors of friction ceofficient under the same energy in which an oxidation wear is being considered along with a mechnical wear although the wear rates were almost similar to the friction coefficient at the low energy.

• 한국세라믹학회지
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• 제33권1호
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• pp.83-91
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• 1996

Monolithic AlN and AlN-W composites were fabricated by pressure-less sintering at 190$0^{\circ}C$ under nitrogen atmosphere and the influences of tungsten phase on the microstructure and mechanical properties were investi-gated. In the fabrication of sintered specimen no additive was used. And monolithic AlN showed substantial grain growth and low relative density. AlN-W composites were fully densified and grain growths of matrix were inhibited. The densification behavior of composites were inferred to be achieved through the liquid phase sintering process such as particle-rearrangement and solutino-reprecipitation. Also the oxid phases which is expected to form liquid phases duringsintering process were detected by XRD analysis. As the tungsten volume content increases fracture strength was decreased and fracture toughness was increased. It was suppo-sed that the strength decrease of composites with tungsten content was due to existence of interface phases. The subcritical crack growth behavior was observed from the stress-strain curve of composites. The effect of the secondary phase and interface phases on toughness in crease were studied through observation of crack propagation path and the influence of residual stress on crack propagation was investigated by X-ray residual stress measurement. In the result of residual stress measurement the compressive stress of matrix in composi-test was increased with tungsten volume content and the compressive stress distribution of matrix must have contributed to the inhibition of crack propagation.

• 한국분말재료학회지
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• 제12권1호
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• pp.70-78
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• 2005

Mechanical alloying using high-energy ball mill and subsequent spark plasma sintering (SPS) process was applied to understand mechanical alloying processing of Al-Fe alloy system. The thermal stability of mechanically alloyed Al-Fe alloy was intended to be enhanced by SPS process. Various analytical techniques including particle size analysis, density measurement, micro-Vickers hardness test, SEM, TEM, and X-ray diffractometry were adopted to find optimum processing conditions for mechanical alloying and subsequent SPS and to estimate thermal stability of the prepared alloy. It was found from the treatment of mechanically alloyed Al-8wt.%Fe powder mixture that needle-shaped $Al_3Fe$ precipitates was formed in the Al-Fe matrix, and the alloy compact showed enhanced densification and reached its full density with little loss of its fine microstructure. After heat treatment at $500^{\circC}$, it was also shown that the thermal stability of Al-8wt.%Fe alloy fabricated in the present study was enhanced, which was due to its fine microstructure developed by fast densification of SPS.

• 한국추진공학회지
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• 제22권6호
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• pp.142-148
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• 2018

발사체 연료 케로신은 발사체의 성능 향상을 위해 고밀도화 과정을 거치게 된다. 고밀도화 방법 중 액체질소 주입 냉각법은 시스템이 간단하고 비용이 저렴한 효과적인 방법이다. 하지만 냉각과정 중 질소가 케로신에 용해되어 물성을 변화시키는 원인이 되기도 한다. 따라서 냉각 후 케로신 내 용존질소의 양을 측정하고 제거하는 작업이 필수적이다. 본 연구에서는 케로신 내 용존질소 함유량을 측정할 수 있는 진공추출 원리를 소개하였다. 또한 질소 샘플링 장치를 설계/제작하여 수행한 실험 결과를 설명하였다. 실험결과로부터 질소 샘플링 장치와 용존질소 측정법/제거법의 유효성을 입증하였다.

• Nuclear Engineering and Technology
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• 제37권4호
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• pp.317-326
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• 2005

The burning-out of excess plutonium from the reprocessing of spent nuclear fuel and from the dismantlement of nuclear weapons is recently emphasized due to the difficulties in securing the final repository for the spent fuel and the necessity to consume the ex-weapons plutonium. An irradiation test in the Halden reactor was launched by the OECD Halden Reactor Project (HRP) to investigate the in-pile behavior of plutonium-embedded fuel as a form of mixed oxide (MOX) and of inert matrix fuel (IMF). The first cycle of irradiation was successfully accomplished with good integrity of test fuel rods and without any undesirable fault of instrumentations. The test results revealed that the MOX fuel is more stable under irradiation environments than IMF. In addition, MOX fuel shows lower thermal resistance due to its better thermal conductivity than IMF. The on-line measured in-pile performance data of attrition milled MOX fuel are used in the analysis of the in-pile performance of the fuel with the fuel performance code, COSMOS. The COSMOS code has been developed for the analysis of MOX fuel as well as $UO_2$ fuel up to high burnup and showed good capability to analyze the in-reactor behavior of MOX fuel even with different instrumentation.

• 소성∙가공
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• 제21권4호
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• pp.228-233
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• 2012

In this study, powder compaction of AZO (alumina doped zinc oxide) powder was performed with a MTS 810 test system using a cylindrical die having a diameter of 10mm. Pressure-density curves were measured based on the load cell and displacement of the punch. The AZO powder compacts with various densities were formed to investigate the mechanical properties such as fracture stress of the AZO powder as a function of the compact density. Two types of compression tests were conducted in order to estimate the fracture stress using different loading paths: a diameteral compression test and a uniaxial compression test. The pressure-density curves of the AZO powder were obtained and the fracture stress of the compacted powders with various densities was estimated. The results show that the compact pressure dramatically increases as the density increases. Based on the experimental results, calibration of the modified Drucker-Prager/Cap model of the AZO powder for use in FE simulations was developed.

• 대한토목학회논문집
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• 제11권4호
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• pp.133-141
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• 1991

실용성과를 갱신하기 위하여 새로운 측지망을 국가 기준점망에 결합하는 문제는 조정원점의 선택방법에 따라 조정결과가 바뀌는 측지망의 독특한 특성 때문에 경험적인 최선의 방법을 채용해 오고 있다. 이 논문에서는 기지점의 좌표를 가상의 측점량으로 고려하여 미지점으로 취급하는 가중측점망(Weighted Station Parameter Network) 방식을 적용하고자 하였으며, 기설 기준점의 공분산 행렬을 사용하는 대신에 대각선 요소만을 고려하는 개선된 방법을 제안하였다. 기설삼각망의 측정량이 미지인 국내의 측지망에서는 개선된 방법이 변동점 검출과 결합조정에 효과적으로 적용될 수 있음을 보여주고 있으며, 작업규정과 테스트망에 대한 분석을 통하여 기설 2등 삼각점의 정확도는 ${\pm}16^{{\prime}{\prime}}$(${\pm}0.08m$)의 정확도를 갖는 것으로 평가되었다. 또한 정밀 2차 기준점망을 1, 2등 삼각점에 결합할 경우에 ${\pm}2.3^{{\prime}{\prime}}$의 정확도를 확보할 수 있을 것으로 기대된다.

• 한국결정성장학회지
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• 제30권6호
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• pp.271-276
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• 2020

본 연구에서는 유기 규소 폴리머(organosilicon polymer)인 폴리카보실란(polycarbosilane, PCS)을 사용하여 비정질 탄화규소 블록을 제조를 진행하였다. 다양한 형상의 치밀한 탄화규소 블록은 큐어링된 PCS 미세분말을 일축가압성형기를 통해 2~8 ton 하중을 가한 후 1100℃, 1200℃, 1300℃, 1400℃의 열처리 과정을 거쳐 제조되었으며, 물리적 화학적 특성 분석을 위해 열중량분석기(TGA), 주사전자현미경(SEM), 에너지분광분석법(EDS), 만능시험기(UTM)을 이용하였다, 제조된 탄화규소 성형체는 열분해 온도가 증가함에 따라 SiO와 CO 가스로의 분해가 발생하였고, 비정질의 구조에서 β-SiC 결정입자가 성장함을 보였다. 또한, 밀도와 굴곡강도는 1100℃의 열분해 온도에서 제조된 탄화규소 성형체가 1.9038 g/㎤과 6.189 MPa으로 가장 높았다. 제조된 비정질 탄화규소 블록은 이전에 보고된 마이크로파 도움 발열체와 같이 다른 분야에 적용 가능할 것으로 기대된다.

• 한국지반공학회논문집
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• 제22권1호
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• pp.25-34
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• 2006

본 연구에서는 비교적 높은 초기 유효응력을 가진 지반구조물의 액상화연구에 사용된 동적 원심모형실힘결과를 이용하여 유효응력모델검증에 관한 연구를 수행하였다. 원심모형 지반은 최대 유효응력 380kPa를 가진 충분히 포화된 느슨한 Nevada 모래 지반으로 구성되었으며, 수치해석에서는 1차원의 기둥형태로 가정하였다. 수치해석에 이용한 두 종류의 원심모형실험에서는 상당한 깊이(37m 및 22m)까지도 액상화가 발생하였으나, 깊이에 따른 액상화발생 경향은 경험적 액상화 평가방법과 상반된 결과를 보였다. 즉, 원심모형실험에서 계측된 과잉간극수압을 기준으로 해석하였을 때, 액상화는 모형지반의 윗부분에서 먼저 발생한 후 점차적으로 아랫부분으로 이동함을 알았다. 이와 같은 실험결과는 수치해석에서 비교적 잘 예측된 것으로 판단되었다 원심모형 지반의 초기 포화도와 원심력 증가에 따른 지반의 상대밀도 증가가 액상화모형실험의 수치해석에서 중요한 역할을 함을 알 수 있었다.