• 대한기계학회:학술대회논문집
• /
• 대한기계학회 2000년도 춘계학술대회논문집A
• /
• pp.31-36
• /
• 2000

High temperature and pressure materials in power plant are degraded by creep damage, if they are exposed to constant loads for long times, which occurs in the load bearing structures of pressurized components operating at elevated temperatures. Many conventional measurement techniques such as replica method, electric resistance method, and hardness test method for measuring creep damage have been used. So far, the replica method is mainly used for the Inspection of High temperature and pressure components. This technique is, however, restricted to applications at the surface of the testpieces and cannot be used to material inside. In this paper, ultrasonic evaluation for the detection of creep damage in the form of cavaties on grain boundaries or integranular microcracks are carried out. And the absolute measuring method of quantitative ultrasonic velocity technique for Cr-Mo material degradation is analyzed. As a result of ultrasonic tests for crept specimens, we find that the sound velocity is decreased as the increase of creep life fraction$({\Phi}_c)$ and also, confirmed that hardness is decreased as the increase of creep life fraction$({\Phi}_c)$ but the coefficient of ultrasonic attenuation is increased as the increase of creep life fraction$({\Phi}_c)$. Finally based on the result in this paper, it can be recognized that the ultrasonic techniques using velocities and attenuation coefficient factor are very useful non-destructive methods to evaluate the degree of material degradation in fossile power plants.

• 한국구조물진단유지관리공학회 논문집
• /
• 제22권6호
• /
• pp.176-181
• /
• 2018

콘크리트 구조물은 시공 후 다양한 원인에 의해 물리적, 화학적 변형을 통해 물리적인 성능이 저하된다. 이러한 콘크리트 구조물의 성능저하는 사용수명을 감소하기 때문에 합리적인 보수보강이 필요하다. 최근 콘크리트 구조물의 효율적인 보수을 위해, 부착성능을 향상시킨 하이브리드 보수재료에 대한 연구가 활발히 수행되어오고 있다. 본 연구에서는 기존콘크리트와의 부착성능 및 수밀성을 향상시키기 위해 초속경 시멘트에 PVA 분말수지, 나일론 섬유, 라텍스를 혼입 한 하이브리드 보수재를 개발하였다. 보수재료의 성능평가를 위해 압축강도, 건조수축, 부착강도 실험을 수행하였다. 또한 미리 손상이 발생한 시험체를 제작한 후 보수 전후의 휨부착 성능평가를 수행하였다. 휨강도 평가결과, 기존의 초속경시멘트만 혼입한 시험체를 제외한 모든 실험체에서 110%~150%정도 휨강도가 크게 나타났고, 휨강도에 의해 발생된 균열패턴은 모든 실험체가 기존 콘크리트와 일체 거동하는 것으로 나타났다.

• 한국전기전자재료학회:학술대회논문집
• /
• 한국전기전자재료학회 2009년도 하계학술대회 논문집
• /
• pp.176-176
• /
• 2009

Influences of dose and particle size of $Al_2O_3$ filler and sintering time on the dielectric properties of $Al_2O_3$ filler/CaO-$Al_2O_3-SiO_2$ (CAS) glass composites were investigated with a view to applying the composites to the substrate material in low temperature co-firing ceramic (LTCC) technology. The increased addition of $Al_2O_3$ filler with the particle size of 1 ${\mu}m$ monotonically decreased the density of the sintered specimen at a given temperature, while sintering of the 10 wt% $Al_2O_3$ added specimen at $925^{\circ}C$ for 2 h demonstrated 96.0 % of the relative density, dielectric constant of 6.34, and quality factor of 2,760 GHz. As for the influence of the particle size of the $Al_2O_3$ filler, there existed an optimum particle size (30 ${\mu}m$) to ensure successful densification (96.5 %) of the 10 wt% $Al_2O_3$/CAS composites at $925^{\circ}C$ for 2 h, at which condition the specimen demonstrated dielectric constant of 5.45 and quality factor of 3,740 GHz. When the influence of the sintering time of the 10 wt% $Al_2O_3$) (30 ${\mu}m$) added specimen was investigated at the sintering temperature of $925^{\circ}C$, an overly long sintering time degraded dielectric properties due to the over-sintering and the significant growth of the second phase such as anorthite, while the sintering for 4 h demonstrated 96.58 % of the relative density, dielectric constant of 5.4, and quality factor of 4,050 GHz. These results demonstrate the feasibility of the investigated material as the substrate material in LTCC technology.

• Korean Chemical Engineering Research
• /
• 제45권2호
• /
• pp.172-177
• /
• 2007

신경작용제의 일종인 고농도의 사린(GB)을 무해한 물질로 전환하기 위한 실험 조건을 찾기 위하여 가성소다 수용액으로 가수분해 하였다. 가수분해 반응은 쟈켓이 부착된 소형 반응기에 circulator를 연결하여 사용하고 2.05 당량의 가성소다 용액에 농도 10 wt%의 사린을 주입한 후 각각의 반응온도(50, 70 및 $90^{\circ}C$)에서 반응 속도 상수를 구하고 이를 이용하여 각 온도에서 GB를 99% 이상 분해하는데 소요되는 가수분해 시간을 예측하였다. 가수분해 실험 결과 GB는 $90^{\circ}C$에서 1.2 시간 반응하면 99.99% 이상 분해되었으며 주요 분해생성물은 isopropyl methylphosphonate이었다.

• 대한전기학회:학술대회논문집
• /
• 대한전기학회 2004년도 하계학술대회 논문집 C
• /
• pp.1676-1678
• /
• 2004

Class-F resin-rich type insulating tapes are generally used for the groundwall insulations of the large turbine generators with air-cooled and hydrogen-cooled stator windings. In this paper, mechanical strength properties degraded over aging time in higher temperature than designed one in normal condition were experimentally investigated and the results of comparative tests were presented on the existing class-F resin-rich type tape and a developed one after curing. The resin-rich insulating tapes with composite material of Mica/Epoxy/support currently were used in this test. The tests for tensile and flexural strength properties were conducted with the specimens which were composed of unaged and the aged specimens accelerated for one, two, and three thousand hours at 180 $^{\circ}C$. The tensional strength was only measured for the unaged specimens and the results are also presented to make a comparative test for their initial mechanical characteristics.

• 청정기술
• /
• 제22권3호
• /
• pp.203-207
• /
• 2016

Here, we report a novel fabrication technique for patchable organic lasing sheet based on non-volatile liquid organic semiconductors and freestanding polymeric film with high flexibility and patchability. For this work, we have fabricated the second-order DFB grating structure, which leads to surface emission, embedded in the freestanding polymeric film. Using an ultra-violet (UV) curable polyurethaneacrylate (PUA) mixture, the periodic DFB grating structure can be easily prepared on the freestanding polymeric film via a simple UV curing process. Due to unsaturated acrylate remained in the PUA mixture after UV curing, the freestanding PUA film provides adhesive properties, which enable mounting of the patchable organic lasing sheet onto non-flat surfaces with conformal contact. To achieve laser actions in the freestanding resonator structure, a composite material of liquid 9-(2-ethylhexyl)carbazole (EHCz) and organic laser dyes was used as the laser medium. Since the degraded active materials can be easily refreshed by a simple injection of the liquid composite, such a non-volatile liquid organic semiconducting medium has degradation-free and recyclable characteristics in addition to other strong advantages including tunable optoelectronic responses, solvent-free processing, and ultimate mechanical flexibility and uniformity. Lasing properties of the patchable organic lasing sheet were also investigated after mounting onto non-flat surfaces, showing a mechanical tunability of laser emission under variable surface curvature. It is anticipated that these results will be applied to the development of various patchable optoelectronic applications for light-emitting displays, sensors and data communications.

• Transactions on Electrical and Electronic Materials
• /
• 제17권6호
• /
• pp.329-334
• /
• 2016

In this work, the temperature dependence of electrical parameters of nanoscale SOI (silicon-on-insulator) TG (triple gate) n-FinFET (n-channel Fin field effect transistor) was investigated. Numerical device simulator $ATLAS^{TM}$ was used to construct, examine, and simulate the structure in three dimensions with different models. The drain current, transconductance, threshold voltage, subthreshold swing, leakage current, drain induced barrier lowering, and on/off current ratio were studied in various biasing configurations. The temperature dependence of the main electrical parameters of a SOI TG n-FinFET was analyzed and discussed. Increased temperature led to degraded performance of some basic parameters such as subthreshold swing, transconductance, on-current, and leakage current. These results might be useful for further development of devises to strongly down-scale the manufacturing process.

• 동력기계공학회지
• /
• 제21권5호
• /
• pp.79-85
• /
• 2017

Vickers hardness is an important material in the design and reliability is required. Therefore, these values are very important as the basic data for design, manufacture and development, and the identification of quantitative probability distribution characteristics such as mean and dispersion is a very important parameter in design. In this study, Vickers hardness was measured after artificially heat-treated in the temperature range 753K, where chrome depletion near the grain boundary occurred for three kinds of stainless steels, and the Vickers hardness were evaluated. From the results, Vickers hardness increased with increasing heat treatment temperature. In Weibull distribution for Vickers hardness, the dispersion of STS310S at 813K and 873K was small, and the dispersion of STS316L at 753K, 933K and 993K was small. Also, STS347H exhibited the lowest dispersion at 753K in three kinds of stainless steels. The scale parameter increased with increasing heat treatment temperature in three kinds of stainless steels.

• 한국신뢰성학회지:신뢰성응용연구
• /
• 제15권4호
• /
• pp.262-269
• /
• 2015

Accelerated degradation mechanism of the heat-resistant steel for high temperature plant was analysed in terms of microstructure and hardness. In order to simulate the microstructure of the steel actually used at $540^{\circ}C$ in the field, isothermal exposure was carried out at $630^{\circ}C$ up to 4,800 hours. The artificial degradation mechanism was comparatively verified to successfully simulate degradation of the long-time used field material. For the artificially degraded specimens, databases including size and aspect ratio of carbide, chemical composition (i.e., Cr/Mo ratio) of grain boundary carbide were built up. These degradation parameters were suggested as fingerprints for PHM (i.e., prognostics health management) of power plants.

• Journal of Welding and Joining
• /
• 제15권4호
• /
• pp.166-177
• /
• 1997

The high strength AlZnMgCu0.5 alloy is a light metal with good age hardenability, and has a high tensile and yielding strength. Therefore, it can be used for structures requiring high speciple strength. Even though high strength AlZnMgCu alloy has good mechanical properties, it has a lot of problems in TIG and MIG welding processes. Since lots of high heat absorption is introduced into the weldment during TIG and MIG processes, the microstructural variation and hot cracks take place in heat affected zone. Therefore, the mechanical properties of high strength AlZnMgCu0.5 alloy can be degraded in weldment and heat affected zone. Welding process utilizing high density heat source such as electron beam should be developed to reduce pore and hot cracking, whichare usually accompanied by MIG and TIG welding processes. In this work, electron beam welding process were used with or without AlMg4.5Mn as filler material to avoid the degradation of mechanical properties. Mechanical and metallurgical characteristics were also studied in electron beam weldment and heat affected zone. Moreover hot cracking mechanism was also investigated.