• Title/Summary/Keyword: defect engineering

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Comprehensive Structural Characterization of Commercial Blue Light Emitting Diode by Using High-Angle Annular Dark Filed Scanning Transmission Electron Microscopy and Transmission Electron Microscopy (고각 환형 암시야 주사투과전자현미경기법과 투과전자현미경기법을 이용한 상용 청색 발광다이오드의 종합적인 구조분석)

  • Kim, Dong-Yeob;Hong, Soon-Ku;Chung, Tae-Hoon;Lee, Sang Hern;Baek, Jong Hyeob
    • Korean Journal of Materials Research
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    • v.25 no.1
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    • pp.1-8
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    • 2015
  • This study suggested comprehensive structural characterization methods for the commercial blue light emitting diodes(LEDs). By using the Z-contrast intensity profile of Cs-corrected high-angle annular dark field scanning transmission electron microscope(HAADF-STEM) images from a commercial lateral GaN-based blue light emitting diode, we obtained important structural information on the epilayer structure of the LED, which would have been difficult to obtain by conventional analysis. This method was simple but very powerful to obtain structural and chemical information on epi-structures in a nanometer-scale resolution. One of the examples was that we could determine whether the barrier in the multi-quantum well(MQW) was GaN or InGaN. Plan-view TEM observations were performed from the commercial blue LED to characterize the threading dislocations(TDs) and the related V-pit defects. Each TD observed in the region with the total LED epilayer structure including the MQW showed V-pit defects for almost of TDs independent of the TD types: edge-, screw-, mixed TDs. The total TD density from the region with the total LED epilayer structure including the MQW was about $3.6{\times}10^8cm^{-2}$ with a relative ratio of Edge- : Screw- :Mixed-TD portion as 80%: 7%: 13%. However, in the mesa-etched region without the MQW total TD density was about $2.5{\times}10^8cm^{-2}$ with a relative ratio of Edge- : Screw- :Mixed-TD portion of 86%: 5%: 9 %. The higher TD density in the total LED epilayer structure implied new generation of TDs mostly from the MQW region.

Effect of Alloy Elements on Microstructure of Modified Area via Friction Stir Process in Steel Materials (마찰교반공정을 통한 강재의 개질 영역에서의 미세조직에 미치는 합금원소의 영향)

  • Kim, Sang Hyuk;Lee, Kwang Jin;Woo, Kee Do
    • Korean Journal of Materials Research
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    • v.25 no.8
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    • pp.370-375
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    • 2015
  • In this study, to confirm the effect of alloying elements on the phase transformation and conditions of the friction stir process, we processed two materials, SS400 and SM45C steels, by a friction stir process (FSP) under various conditions. We analyzed the mechanical properties and microstructure of the friction stir processed zone of SS400 and SM45C steels processed under 400RPM - 100mm/min conditions. We detected no macro (tunnel defect) or micro (void, micro crack) defects in the specimens. The grain refinement in the specimens occurred by dynamic recrystallization and stirring. The microstructure at the friction stir processed zone of the SS400 specimen consisted of an ${\alpha}$-phase. On the other hand, the microstructure at the friction stir processed zone of the SM45 specimen consisted of an ${\alpha}$-phase, $Fe_3C$ and martensite due to a high cooling rate and high carbon content. Furthermore, the hardness and impact absorption energy of the friction stir processed zone were higher than those of base metals. The hardness and impact absorption energy of FSPed SM45C were higher than that of FSPed SS400. Our results confirmed the effect of alloying elements on the phase transformation and mechanical properties of the friction stir processed zone.

Theoretical Study on Hoop Wrap of the Metal Wire for Type 2 High Pressure Tank (Type 2 고압용기를 위한 금속선재의 Hoop Wrap에 관한 이론 연구)

  • KIM, SEUNGHWAN;HAN, JINMOOK;JUNG, YOUNGGUAN
    • Journal of Hydrogen and New Energy
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    • v.31 no.2
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    • pp.194-201
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    • 2020
  • Recently, Type 2 high-pressure hydrogen storage tank is studied due to fast defect detection, easy manufacturing, and cost efficiency. Moreover, the dry winding a high-strength metal wire will make increased economic efficiency compare with the wet winding method and the carbon/glass fiber winding method. In this study, a theoretical study on the dry winding of a Type 2 high pressure hydrogen tank using a metal wire was done, and the equations of the total stress on the aligned and the staggered winding for the hoop winding were derived, and the following results were obtained by using these equations. As the diameter of the metal wire, the number of winding layers, and the outer diameter of the liner increase, the maximum stress decreases, but the difference between the maximum stress occurring in the aligned winding and the staggered winding increases. As the pressure increases, the thickness of the winding layer increases, but as the strength of the metal wire increases, the thickness of the winding layer decreases. In addition, regardless of the strength of the metal wire, the thickness of the winding layer of the staggered winding was about 13.4% thinner than that of the aligned winding.

A Study on the Improvement of Public Facility Management System Using Life-cycle Management (Life-cycle Management를 활용한 공공시설 유지관리 시스템 개선방안)

  • Jeon Ick-Sung;Shon Jeong-Rak;Kim Kyung-Suk;Kim Jae-Jun
    • Korean Journal of Construction Engineering and Management
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    • v.5 no.2 s.18
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    • pp.55-63
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    • 2004
  • A building structures was used the facility management phase through $planing\cdotdesign\cdotconstruction$. phase. building's length of life was shorter than its physical length of life, because of the lack of law and institution, the lack of related agencies' preparation and owner's preparation. Also, considering the construction life-cycle, the facility phase accounted for $70\%$ of whole official lift, therefore, it needed to be opposed to systemic facility management. Current facility management system practically managed the defect of facility and almost never communicated between the other phase. In the side of policy, domestic law, institution, and policy related to building structure focused built-up market. and then the management of existing facilities was not consolidated efficiently. The purpose of this study was to suggest the direction of facility management construction for managing, utilizing, and operating public facilities, moreover, to study the direction of current facility management system improvement corresponding to total computer integrated construction system under government agencies.

A Study for Analyzing Life Cycle Cost of Membrane Water-proofing of Roof - Focused on precaution for securing quality - (건축공사 옥상 도막방수 공법의 LCC 분석 - 품질확보를 위한 사전대책을 중심으로 -)

  • Bae, Jae-Wook;Shin, Seung-Moon;Kim, Sang-Gap;Koo, Choong-Wan;Hong, Tae-Hoon;Koo, Kyo-Jin;Hyun, Chang-Taek
    • Korean Journal of Construction Engineering and Management
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    • v.9 no.4
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    • pp.57-65
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    • 2008
  • As the society is being developed, the desire about life quality is also growing. Even though the process of waterproof work has very close relation with these life quality, we always focus on management after problem than the precaution of problem. So this process has the highest rate of mengel. We develop LCC analysis model considering the precaution and try to show the necessity of the precaution by comparing and analyzing every alternative proposal during LCC. By studying of the previous work and the result of questionnaire, we deduce the problem of waterproof work in construction area. By discussion with an expert in this process and research, we make solutions about precaution and set the cost items in every alternative proposal about these solutions. We understand the effect of each elements through sensitive analysis of the cost items, and find the economically best suited solution.

Design and Fabrication of the Triple Band(DCS, PCS, UPCS) Internal Chip Antenna (내장형 트리플(DCS, PCS, UPCS) 칩 안테나 설계 및 제작)

  • Park, Seong-Il;Park, Sung-Ha;Ko, Young-Hyuk
    • Journal of the Korea Institute of Information and Communication Engineering
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    • v.13 no.7
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    • pp.1261-1266
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    • 2009
  • In this paper, triple band mobile chip antenna for DCS(1.71${\sim}$1.88GHz) / PCS(1.75${\sim}$1.87GHz) / UPCS(1.8S${\sim}$1.99GHz) on PCB Layout is designed. To analyze the characteristics of the designed antenna, we used commerical simulation tool(HFSS). Triple and wide band characteristic could be realized the measured bandwidth(V.S.W.R<2.0) of the designed antenna operated in 1.71GHz${\sim}$1.99GHz. The size of the designed antenna is about 19mm${\times}$4mm${\times}$1.6mm, narrow bandwidth which is a defect of chip antenna is improved. And its experimental results were a good agreement with simulation performance.

Effect of NaOH Concentration on the PEO Film Formation of AZ31 Magnesium Alloy in the Electrolyte Containing Carbonate and Silicate Ions

  • Moon, Sungmo;Kim, Yeajin;Yang, Cheolnam
    • Journal of Surface Science and Engineering
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    • v.50 no.5
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    • pp.308-314
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    • 2017
  • Anodic film formation behavior of AZ31 Mg alloy was studied as a function of NaOH concentration in 1 M $Na_2CO_3$ + 0.5 M $Na_2SiO_3$ solution under the application of a constant anodic current density, based on the analyses of voltage-time curves, surface appearances and morphologies of the anodically formed PEO (plasma electrolytic oxidation) films. The anodic film formation voltage and its fluctuations became largely lowered with increasing added NaOH concentration in the solution. Two different types of film defects, large size dark spots indented from the original surface and locally extruded white spots, were observed on the PEO-treated surface, depending on the concentration of added NaOH. The large size dark spots appeared only when added NaOH concentration is less than 0.2 M and they seem to result from the local detachments of porous PEO films. The white spots were observed to be very porous and locally extruded and their size became smaller with increasing added NaOH concentration. The white spot defects disappeared completely when more than 0.8 M NaOH is added in the solution. Concludingly it is suggested that the presence of enough concentration of $OH^-$ ions in the carbonate and silicate ion-containing electrolyte can prevent local thickening and/or detachment of the PEO films on the AZ31 Mg alloy surface and lower the PEO film formation voltage less than 70 V.

Effect of Process Parameters on Friction Stir Welds on AA2219-AA2195 Dissimilar Aluminum Alloys (마찰교반접합의 공정변수가 AA2219-AA2195 이종 알루미늄 접합에 미치는 영향)

  • No, Kookil;Yoo, Joon-Tae;Yoon, Jong-Hoon;Lee, Ho-Sung
    • Korean Journal of Materials Research
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    • v.27 no.6
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    • pp.331-338
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    • 2017
  • This study was carried out to investigate the optimum condition of a friction stir welding process for a joint of AA2219-T87 and AA2195-T8 dissimilar aluminum alloys. These alloys are known to have good cryogenic properties, and as such to be suitable for use in fuel tanks of space vehicles. The welding parameters include the travelling speed, rotation speed and rotation direction of the tool. The experiment was conducted under conditions in which the travelling speed of the tool was 120-300 mm/min and the rotation speed of the tool was 400-800 rpm. To investigate the effect of the rotation direction of the tool, the joining was performed by switching the positions of the two dissimilar alloys. After welding, the microstructure was observed and the micro-hardness were measured; non-destructive evaluation was carried out to perform tensile tests on defect-free specimens. The result was that the microstructure of the weld joint underwent dynamic recrystallization due to sufficient deformation and frictional heat. The travelling speed of the tool had little effect on the properties of the joint, but the properties of the joint varied with the rotation speed of the tool. The conditions for the best joining properties were 600 rpm and 180-240 mm/min when the AA2219-T8 alloy was on the retreating side(RS).

A Comparative Study of Pulse-echo Method and TOFD Method for the Defect in the Welding Joint of the STS304 Stainless Steel (STS304 스테인리스강 용접부 결함평가에 대한 Pulse-echo법과 TOFD법의 비교연구)

  • Kil, Doo-Song;Choi, Won-Doo
    • Journal of Power System Engineering
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    • v.6 no.4
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    • pp.68-72
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    • 2002
  • For the evaluation of a flaw in a welded stainless steel by the Time of Flight Diffraction(TOFD) Method, we have made the reference specimen for experimentation. As a result, we could analyze a specific character and the inner state of the structure in a welded stainless steel and we came to the conclusion as followed. (1) For analyze the structure state of a section in a welded stainless steel through the optical microscope, we could have analyzed the generated shape and the location of a flaw and the inner parts of the structure state through the microscope of eighty magnification and two hundred magnification about the soundness, the heat affected zone(HAZ) and the welded part. (2) Through the comparison with the shape and the size of a flaw in the welded part about the conventional ultrasonic test and the TOFD Method, we could make an observation the special character of the TOFD Method and principles. (3) We analyzed and collected the merit of the TOFD Method on the basis of the experimental result by the shape and the size of a flaw in the inner welded parts. So, we made up a base that we could use as a basic data for a similar flaw like that. Through the study as mentioned above, we could make an observation the flaw detective method and principles used in the TOFD Method.

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High Cyclic Fatigue Life and Fracture Behaviors of Shot-Peened Bearing Steel (쇼트피닝 처리를 한 베어링강의 고사이클 피로수명 및 파괴거동)

  • Yoon, Sang-Jae;Choi, Nak-Sam
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.35 no.9
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    • pp.1119-1129
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    • 2011
  • Shot-peening effects on the fatigue behavior of bearing steel were investigated under the high cyclic loading. Hourglass shape specimens were made of bearing steel(JIS-SUJ2) for rotary bending fatigue tests. Two kinds of treatments were performed : a heat treatment and a shot-peened surface treatment after the heat treatment. The fracture surfaces of specimens were classified into two types of fracture mode : the surface fracture mode induced by a surface defect and the internal fracture mode induced by a nonmetallic inclusion. Inclusion depth and shape affected considerably the fatigue life. Shot-peening treatment improved much the fatigue life of the bearing steel under low and high levels of cyclic loads. Probabilistic-stress-life (P-S-N) curves were suggested for the reliable fatigue life estimation of the improved bearing steel.