• Title/Summary/Keyword: curing agent

Search Result 427, Processing Time 0.034 seconds

A Low-elastic MRE Fabrication Process based on the Taguchi Method (다구찌법을 이용한 저탄성 MRE 제조공정 연구)

  • Shin, Dae-Yong;Tariq, Zakria;La, Moon-Woo;Park, Sung-Jea
    • Journal of the Korean Society of Manufacturing Process Engineers
    • /
    • v.19 no.2
    • /
    • pp.55-62
    • /
    • 2020
  • In this study, a PDMS-based low-elasticity magnetorheological elastomer (MRE) was fabricated and the Taguchi method was used to identify the factors affecting the elastic modulus. The mixing entropy was calculated using optical microscopy to confirm particle dispersion, which was referenced in the process establishment. In the MRE process, four parameters, namely the curing agent, particle type, particle fraction, and applied magnetic field, were divided into three levels. The elastic modulus of the specimen was compared at the off-state and at 0.2 T using compression tests, and the obtained signal to noise ratio indicated that the softness and change in the elastic modulus of the MRE was mainly affected by the curing agent and the particle fraction.

A Study of development on Mica/Epoxy Composite (2) (마이카/ 에폭시 복합재료의 개발에 관한 연구(2))

  • Park, Chung-Hoo;Jeung, Eun-Shik;Kim, Ki-Beom
    • Proceedings of the KIEE Conference
    • /
    • 1987.11a
    • /
    • pp.216-219
    • /
    • 1987
  • Dielectric and Mechanical Properties of Mica flake/ Epoxy Composite are investigated. The Mica content is about 50 wt % and its thickness is about $240{\mu}m$. The finished Mica flake/Epoxy Composite contains about 0.1-1.0 wt % of aminosilane coupling agent. Ruby Mica filler and high temperature curing Epoxy resin are used. From the viewpoint of dielectric and mechanical properities. the optimum properties is obtained for the sample post cured at $130^{\circ}C$ for 5 h ours after curing at $80^{\circ}C$ for 2 hours and with 0.5 weight % silane coupling agent.

  • PDF

Shrinkage Properties of High Performance Concrete with Specimen Size (공시체 크기 변화에 따른 고성능 콘크리트의 수축특성)

  • Han, Cheon-Goo;Jin, Hu-Lin;Han, Min-Cheol;Kang, Soo-Tae;Koh, Kyoung-Taek
    • Proceedings of the Korea Concrete Institute Conference
    • /
    • 2004.11a
    • /
    • pp.549-552
    • /
    • 2004
  • This paper investigated the drying and autogenous shrinkage of high performance concrete(HPC) with mixture adjustment under various specimen size. For fresh concrete properties, HPC with mixture adjustment need a higher dosage of SP agent due to fluidity reduction, and a larger dosage of AE agent due to the reduction of air content. HPC with mixture adjustment exhibited a smaller strength development than control HPC. For drying shrinkage, an increase in specimen size occurred with small expansion during water curing and at air curing, less drying shrinkage was observed. Autogenous shrinkage was not affected by specimen size. Autogenous shrinkage of HPC with mixture adjustment exhibited less than half of control HPC.

  • PDF

Time-Temperature-Transition Diagrams with Liquid Crystalline Phase Changes of Liquid Crystalline Epoxy (열경화성 액정 에폭시 수지의 액정상 변화를 포함한 시간-온도-전이 다이어그램)

  • Seung Hyun Cho
    • Composites Research
    • /
    • v.37 no.3
    • /
    • pp.215-218
    • /
    • 2024
  • Liquid crystalline thermosetting epoxy oligomer DD-A was synthesized with Diglycidyl ether of 4,4'-dihydroxy-α-methylstilbene (DGE-DHMS) and aniline in a ratio of 2:1 and cured with a catalytic curing agent, 1-Methyl Imidazole. The gelation times and vitrification times were measured to create Time-Temperature-Transition Diagrams with liquid crystalline phase changes. It was found that the gelation and vitrification times were decreased as the concentration of curing agent increased, and the vitrification curve showing a typical S-shape was confirmed.

Fundamental Properties of Low-Heat Concrete According to the Mixing Rate of Super Retarding Agent (초지연제 혼입률에 따른 저발열 콘크리트의 양생온도별 기초물성평가)

  • Park, Byoung-Joo;Choi, Yoon-Ho;Hyun, seung-Yong;Kim, Jong;Han, Min-Cheol;Han, Cheon-Goo
    • Proceedings of the Korean Institute of Building Construction Conference
    • /
    • 2020.06a
    • /
    • pp.90-91
    • /
    • 2020
  • As the construction site has become narrower recently, the importance of mass concrete is naturally being highlighted as skyscrapers become popular. However, it is not possible to install the entire volume per day if the mass concrete is installed due to the Remicon 8⦁5 system and the 52-hour workweek system. When the mass concrete base is divided into several days, cold joints occur because the consolidation of joints is not integrated due to different degree of hardening in the case of the previous layer and the next day. As a result, existing research has shown that if super retarding agent are mixed into Ready Mixed Concrete (hereinafter referred to as Remicon) using sugar as a raw material to delay the curing time of concrete, cold joints are inhibited and cracks are inhibited by reducing the initial hydration heat.

  • PDF

An Experiment on the Structure Application of Cold Weather Concreting Using Anti-freeze Agent and Insulating Form (내한제 및 단열거푸집을 이용한 한중콘크리트의 구조체 적용 실험)

  • 김경민;손성운;김기철;오선교;한천구
    • Proceedings of the Korean Institute of Building Construction Conference
    • /
    • 2002.05a
    • /
    • pp.21-26
    • /
    • 2002
  • This paper is intended to verify the efficiency of anti-freeze agent and insulating form by analyzing the temperature history and the property of strength-increase about the concrete that is placed in the insulating form and normal form, using new type anti-freeze agent in batcher plant According to the results about the temperature history, while the lowest temperature shows 3$^{\circ}C$ in case of normal concrete + euroform, 4$^{\circ}C$ in case of normal concrete + insulating form, it shows 6$^{\circ}C$ in anti-freeze agent + the insulating form, so the effect is most favorable. The compressive strength with mixing anti-freeze agent or not, shows high in order of standard curing, structure-managing and open air-placed specimen and the concrete mixing anti-freeze agent shows the highest compressive strength-increase.

  • PDF

A study on the spin on glass (SOG) from polysilazane resin for the premetal dielectric (PMD) layer of sub-quarter micron devices (초고집적소자의 층간절연막용 polysilazane계 spin on glass (SOG)에 관한 연구)

  • 나사균;정석철;이재관;김진우;홍정의;이원준
    • Journal of the Korean Vacuum Society
    • /
    • v.9 no.1
    • /
    • pp.69-75
    • /
    • 2000
  • We have investigated the feasibility of spin on glass (SOG) film from polysilazane-type resin as a premetal dielectric (PMD) layer of the next-generation ultra-large scale integrated (ULSI) devices. A commercial polysilazane resin and a polysilazane-type resin with oxidizing agent were spin-coated and cured to form SOG films. In order to study the effect of oxidizing agent and annealing, the SOG films were characterized as cured and after annealing at $400^{\circ}C$ to $900^{\circ}C$. the density and the resistance against wet chemical of the SOG films were improved by the addition of oxidizing agent, because oxidizing agent enhanced the conversion from polysilazane polymer to $SiO_2$. The hole profile issue associated with insufficient curing of polysilazane in narrow gaps was also resolved by oxidizing agent, while the gapfill capability of SOG was not deteriorated by oxidizing agent.

  • PDF

Surface and Chemical Properties of Surface-Modified UHMWPE Powder and Mechanical and Thermal Properties of Its Impregnated PMMA Bone Cement V. Effect of Silane Coupling Agent on the Surface Modification of UHMWPE Powder

  • Yang Dae Hyeok;Yoon Goan Hee;Shin Gyun Jeong;Kim Soon Hee;Rhee John M.;Khang Gilson;Lee Hai Bang
    • Macromolecular Research
    • /
    • v.13 no.2
    • /
    • pp.120-127
    • /
    • 2005
  • Conventional poly(methyl methacrylate) (PMMA) bone cement has been widely used as an useful biopolymeric material to fix bone using artificial prostheses. However, many patients had to be reoperated, due to the poor mechanical and thermal properties of conventional PMMA bone cement, which are derived from the presence of unreacted MMA liquid, the shrinkage and bubble formation that occur during the curing process of the bone cement, and the high curing temperature ($above 100^{\circ}C$) which has to be used. In the present study, a composite PMMA bone cement was prepared by impregnating conventional PMMA bone cement with ultra high molecular weight polyethylene (UHMWPE) powder, in order to improve its mechanical and thermal properties. The UHMWPE powder has poor adhesion with other biopolymeric materials due to the inertness of the powder surface. Therefore, the surface of the UHMWPE powder was modified with two kinds of silane coupling agent containing amino groups (3-amino propyltriethoxysilane ($TSL 8331^{R}$) and N-(2-aminoethyl)-3-(amino propyltrimethoxysilane) ($TSL 8340^{R}$)), in order to improve its bonding strength with the conventional PMMA bone cement. The tensile strengths of the composite PMMA bone cements containing $3 wt\%$ of the UHMWPE powder surface-modified with various ratios of $TSL 8331^{R}$ and $TSL 8340^{R}$ were similar or a little higher than that of the conventional PMMA bone cement. However, no significant difference in the tensile strengths between the conventional PMMA bone cement and the composite PMMA bone cements could be found. However, the curing temperatures of the composite PMMA bone cements were significantly decreased.