• 제목/요약/키워드: crystalline orientation

검색결과 200건 처리시간 0.023초

열증착방법에 의해 제조된 Si(100)/X(500$\AA$)/Zn(1000$\AA$) 이중박막 성장에 관한 연구 (A Study on the growth of Si(001)/X(500$\AA$)/Zn(1000$\AA$) double layers deposited by thermal evaporation process.)

  • 신동원;정순종;이동윤;민복기;정원섭;송재성
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2001년도 하계학술대회 논문집
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    • pp.1026-1029
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    • 2001
  • Zinc films have been deposited onto various buffer layers, Al, Al-Cu, Ag and Ag-Al, by vacuum evaporation method in order to investigate the film microstructure and its consequence on the film growth. Zn films were grown onto Al buffer layers with faster rates than on Ag buffer layers, because of the presence of preferred growth orientation. Especially, in the Zn film formation on the Ag layers, intermetallic compounds AgZn was formed to cause the different growth orientation from Zn film obtained on the Al layers.

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CoCr(-Ta)/Si 이층막의 c-축 우선 배향성에 관한 연구 (A Study on the c-axis preferred orientation of CoCr(-Ta)/Si doublelayer)

  • 김용진;박원효;신성권;손인환;최형욱;김경환
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2001년도 하계학술대회 논문집 C
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    • pp.1475-1477
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    • 2001
  • In odor to set high saturation magnetization and coercivity, it had need to orient axis of easy magnetization of CoCr-based thin film perpendicular direction(c-axis) to the substrate plane. It was known that crystalline orientation of CoCr-based thin film was improved by introducing underlayer like Ti, Ge. We prepared singlelayer and double layer with Si underlayer by Facing Targets Sputtering System. As a result, intensity and c-axis dispersion angle ${\Delta}{\theta}_{50}$ of singlelayer were improved with increasing film thickness. Also, it was found that CoCr/Si and CoCrTa/Si double layer showed good c-axis dispersion angle due to introducing Si.

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초고분자량 폴리에닐렌 미세구조가 변형과 마모에 미치는 영향 (Effect of crystalline lamellar orientation on the creep and wear of ultra-high molecular weight polyethylene)

  • 이권용
    • 한국윤활학회:학술대회논문집
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    • 한국윤활학회 1998년도 제28회 추계학술대회
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    • pp.100-105
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    • 1998
  • 초고분자량 폴리에틸렌(Ultra-High Molecular Weight Polyethylene)은 인공관절 라이너에 쓰이는 대표적 생체재료이다. 초고분자량 폴리에틸렌의 변형과 마모에 영향을 주는 인자에 대한 기본적 연구를 위하여 본 연구에서는 미세구조 결정상의 정도와 결정구조 방향성에 따른 초고분자량 폴리에틸렌의 크리프 변형 및 마모 특성의 연구를 행하였다. 압출 제작된 초고분자량 폴리에틸렌 봉(extruded UHMWPE rod)단면의 중앙(center) 부분과 원주(periphery)부분으로부터 각각 직사각형 및 원통형의 시편을 제작하여 크리프 실험과 마모 실험을 실시하였다. 원주 시편의 크리프 변형율은 중앙 시편의 크리프 변형율보다 11% 크며 (p<0.05), 마모양도 원주 시편이 중앙 시편보다 두 배나 큰 것으로(p<0.05)관측되었다. 이 결과들로부터 초고분자량 폴리에틸렌의 크리프 변형과 마모가 미세 결정구조 방향성에 영향을 받는 것으로 나타났다.

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Magnetic Contactor Upper Frame 사출성형시 유리섬유 배향에 따른 뒤틀림 변형에 관한 연구 (A study of warpage caused by glass fiber orientation in Injection Molding to Upper Frame of Magnetic Contactor in 85 AF)

  • 박진영;조해용;김길수;황한성
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2000년도 추계학술대회논문집A
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    • pp.766-771
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    • 2000
  • As using of insulating material of plastic to industrial electric field, thermoset has been gradually substituted for thermoplastic. But changing the material with crystalline has some problem, which is strength or warpage, Especially getting a strength to endure inner pressure is necessary when arc is occurred. So we use the material that is composed of glass fiber to compensate strength. By the way as the reinforced glass-fiber material is used in injection molding, unstableness of dimension is appeared frequently and it is difficult to know warpage pattern. So this paper will be contributed to know warpage pattern of mold product that is upper frame of magnetic contactor caused by glass-fiber orientation with fixed gate-system, when glass-fiber reinforced material with classification of poly-amide is used in injection molding.

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PREFERRED ORIENTATION AND MICROSTRUCTURE OF MOD DERIVED SrBi$_{2x}$Ta$_2$O$_9$ THIN FILMS WITH Bi CONTENT x

  • Yeon, Dae-Joong;Park, Joo-Dong;Oh, Tae-Sung
    • 한국표면공학회지
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    • 제29권6호
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    • pp.621-627
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    • 1996
  • $SrBi_{2x}TaO_9$ ferroelectric thin films were prepared on platinized silicon substrates using MOD proces, and crystallization behavior of the films was investigated with variation of the annealing temperature and Bi content x. Crystalline phase of bismuth layered perovskite structure was formed even by baking the films at $800^{\circ}C$ for 5 minutes in air, and was not changed by annealing at temperatures raning from $700^{\circ}C$ to $900^{\circ}C$ for 1 hour in oxygen ambient. When $SrBi_{2x}TaO_9$ thin films ($0.8\lex\ie1.6$) were annealed at $800^{\circ}C$, Preferred orientation of the films along c-axis was observed with $x\ge1.2$. With increasing Bi content x, surface morphology of the films was changed from equiaxed grains to elongated grains.

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Structure and Properties of TLCP/Polyester Composite Fibers

  • Kim, Jun-Young;Kim, Seong-Hun
    • 한국섬유공학회:학술대회논문집
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    • 한국섬유공학회 2003년도 The Korea-Japan Joint Symposium
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    • pp.102-102
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    • 2003
  • TLCP/polyester composite fibers (TPCFs) based on melt blends of PEN, PET, and TLCP were prepared by melt blending and spinning process to achieve high performance fibers. Reinforcement effect and TLCP fibrillar structure resulted in improvement of mechanical properties for TPCFs. The increase in the apparent crystallite size was attributed to the development of larger crystallites and more ordered crystalline structures in the annealed TPCFs. Molecular orientation was an important factor to determine mechanical property of TPCFs.

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폴리에스테르 부분배향사의 용매처리에 따른 내부구조 및 표면형태의 변화 (The Effect of Solvent Treatment on the Microstructure and Surface Morphology of PET POY)

  • 신혜원;유효선
    • 한국의류학회지
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    • 제20권3호
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    • pp.467-480
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    • 1996
  • Interactions between PET POY and solvents were estimated by the changes in microstructure and surface morphology. Changes in microstructure and surface morphology by the solvent treatments were: an increase in crystallite size, a decrease in interplanar spacing, a change in degree of orientation of crystalline region, a change in surface characteristics.

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열처리조건이 LaNiO3 졸-겔 박막의 배향성과 구조 및 저항성에 미치는 영향 (Effect of Heat-treatment Conditions on Orientation, Structures and Resistances of LaNiO3 Thin Films by Sol-gel process)

  • 박민석;김대영;서병준;김강언;정수태
    • 한국전기전자재료학회논문지
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    • 제17권8호
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    • pp.859-865
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    • 2004
  • LaNiO$_3$(LNO) thin films on (100) Si substrates are prepared by sol-gel method on heat treatment conditions, such as heat transfer direction, pyrolysis and annealing process, and annealing temperatures and times. The effect of heat treatment conditions on the (100) orientations, structures and resistances of the thin films are investigated by XRD, SEM(FESEM), and a lout probe method. Highly (100) orientation factor(0.97), a pseudocubic crystalline structure with a dense and uniform microstructure could be formed by the following conditions: 1) the heat transfer direction is from Si substrate to LNO, 2) the pyrolysis and annealing process are alternated, 3) the annealing temperature is $650^{\circ}C$ and 4) the annealing times is 3 minutes. The sheet resistance of thin films decreased with increasing of a annealing temperature and time, and a number of coating.

Two-Facing-Targets (TFT) 스퍼터링장치를 이용하여 증착한 AlN박막의 잔류응력 측정 (Measurement of Residual Stress of AlN Thin Films Deposited by Two-Facing-Targets (TFT) Sputtering System)

  • 한창석;권용준
    • 한국재료학회지
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    • 제31권12호
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    • pp.697-703
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    • 2021
  • Aluminum nitride having a dense hexagonal structure is used as a high-temperature material because of its excellent heat resistance and high mechanical strength; its excellent piezoelectric properties are also attracting attention. The structure and residual stress of AlN thin films formed on glass substrate using TFT sputtering system are examined by XRD. The deposition conditions are nitrogen gas pressures of 1 × 10-2, 6 × 10-3, and 3 × 10-3, substrate temperature of 523 K, and sputtering time of 120 min. The structure of the AlN thin film is columnar, having a c-axis, i.e., a <00·1> orientation, which is the normal direction of the glass substrate. An X-ray stress measurement method for crystalline thin films with orientation properties such as columnar structure is proposed and applied to the residual stress measurement of AlN thin films with orientation <00·1>. Strength of diffraction lines other than 00·2 diffraction is very weak. As a result of stress measurement using AlN powder sample as a comparative standard sample, tensile residual stress is obtained when the nitrogen gas pressure is low, but the gas pressure increases as the residual stress is shifts toward compression. At low gas pressure, the unit cell expands due to the incorporation of excess nitrogen atoms.

경상분지 북동부의 제3기 결정질 응회암에서 발달하는 미세균열의 방향성 (Microcrack Orientations in Tertiary Crystalline Tuff from Northeastern Gyeongsang Basin)

  • 박덕원
    • 암석학회지
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    • 제18권2호
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    • pp.115-135
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    • 2009
  • 경상분지 북동부 일대의 제3기 결정질 응회암에서 분포하는 미세균열의 전반적인 분포특성을 규명하였다. 포항시 흥해읍 및 청하면 지역에서 채취한 6개 암석시료의 수평면 상에서 발달하는 108조의 미세균열은 영상처리를 통하여 구별하였다. 이들 108조의 미세균열은 38장의 영상에서 뚜렷한 선상배열을 보여 주었다. 결정질 응회암에 대한 방향각(${\theta}$)-빈도수(N) 관계도의 전 영역은 미세균열의 분포상에 의하여 20개의 영역으로 분류할 수가 있다. 관계도에서 미세균열의 여러 조는 수직상의 일반적인 절리의 방향과 일치하는 강한 배향성을 보여 준다. 따라서 관계도의 각 영역내에서 빈도가 높은 방향각으로부터 거시적인 수직상 절리의 잠재성을 추측할 수가 있다. 관계도에서 나타난 이러한 절리의 형태는 강화군 석모도의 중생대 화강암의 경우와 거의 동일하다. 결정질 응회암에서 도출한 미세균열의 방향을 종합한 장미도에서, 빈도등급에 따른 미세균열의 우세한 조들의 방향성은 암체에 작용한 최대 압축 주응력의 대표적인 방향성을 시사한다. 한편 결정질 응회암의 미세균열의 방향성에 대하여 경상분지 남서부의 불국사 화강암류에서 분포하는 열린 미세균열 그리고 국내 중생대 화강암류의 석산에서 발달하는 수직 결의 방향성과 비교하였다. 광역 분포도에서 상기한 결정질 응회암 및 불국사 화강암류의 미세균열 조 그리고 수직 결 사이의 분포형이 일치한다는 사실은 결정질 응회암에서 내재하는 미세균열의 계는 국내 중생대 화강암류에서도 광역적으로 발달함을 시사한다.