• The Journal of Korean Academy of Prosthodontics
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• v.44 no.6
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• pp.712-721
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• 2006

Statement of problem. Acrylic resin is most commonly used for denture bases. However, acrylic resin has week points of volumetric shrinkage during polymerization that reduces denture fit. The expandability of POSS (Polyhedral Oligomeric Silsesquioxane) containing polymer could be expected to reduce the polymerization shrinkage of denture bases and would increase the adaptability of the denture to the tissue. Purpose. The purpose of this study was to compare the dimensional stability in the conventional acrylic resin base, POSS-containing acrylic resin base, and metal bases. Materials and methods. Thirty six maxillary edentulous casts and dentures of different base were fabricated. Tooth movement and tissue contour change of denture after processing (resin curing, deflasking, decasting and finishing without polishing) and immersion in artificial saliva at $37^{\circ}C$ for 1 week and 4 weeks were measured using digital measuring microscope and threedimensional laser scanner. Results. The results were as follows: 1. The conventional resin group showed significant (p<0.01) dimensional change throughout the procedure (processing and immersion in artificial saliva). 2. After processing, the metal group and POSS resin group showed lower linear and 3-dimensional change than conventional resin group (p<0.01). 3. There was no statistically significant linear and 3-dimensional change after immersion for 1 week and 4 weeks in metal and POSS resin group. 4. In all groups, the midline and alveolar ridge crest area presented smaller 3-dimensional change compared with vestibule and posterior palatal seal area after processing and soaking in artificial saliva for 1 week and 4 weeks (p<0.01). Conclusion. In this study, a reinforced acrylic-based resin with POSS showed good dimensional stability.

• Journal of the Korean Society of Clothing and Textiles
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• v.30 no.3 s.151
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• pp.481-486
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• 2006

There are attempts to utilize Hanji for apparel material, but, the reason that the strength and durability of Hanji decrease to a great extent in the wet condition, restricts the usability of Hanji. In order to improve the resistance against water, Hanji was treated with silicone type water repellent agents. The treatment was carried out by conventional pad-dry-cure method. The optimum treatment condition was obtained by varying the concentration of repellent agent, curing temperature and time. Water repellency was tested by spray rating method. Wet and dry tensile strength, tearing resistance and abrasion resistance were examined after the treatment. Flexural stiffness and wrinkle recovery angles of hanji were also measured. In result, the optimum condition of treatment was at resin concentration of 40g/l, catalyst concentration of 20g/l(half of resin concentration), curing temperature of 160$^{circ}C$, curing time of 120 sec. Flexural stiffness of Hanji was hardly increased and wrinkle recovery angle of Hanji was improved a little by resin treatment. After the treatment, in dry condition, tensile strength and tearing resistance were little changed but abrasion resistance was improved. In wet condition, tensile strength, tearing strength and abrasion resistance were improved.

• Journal of the Korea Concrete Institute
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• v.22 no.3
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• pp.287-295
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• 2010

In this study, ordinary Portland cement was used and the air void was minimized by using minute quartz as the filler. In addition, steel fibers were used to mitigate the brittle failure problem associated with high strength concrete. This study is in progress to make an Ultra-high strength powdered concrete (UHSPC) which has compressive strength over 300 MPa. To increase the strength of concrete, we have compared and analyzed the compressive strengths of the concretes with different mix proportions and curing conditions by selecting quartz sand, dolomite, bauxite, ferro silicon which have diameters less than 0.6 mm and can increase the bond strength of the transition zone. Ultra-high strength powdered concrete, which is different from conventional concrete, is highly influenced by the materials in the mix. In the study, the highest compressive strength of the powdered concrete was obtained when it is prepared with ferro silicon, followed in order by Bauxite, Dolomite, and Quartz sand. The amount of ferro silicon, when the highest strength was obtained, was 110%, of the weight of the cement. SEM analysis of the UHSPC showed that significant formation of C-S-H and Tobermorite due to high temperature and pressure curing. Production of Ultrahigh strength powdered concrete which has 28-day compressive strength upto 341MPa has been successfully achieved by the following factors; steel fiber reinforcement, fine particled aggregates, and the filling powder to minimize the void space, and the reactive materials.

• Journal of the Korea Concrete Institute
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• v.16 no.6 s.84
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• pp.767-776
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• 2004

Polymer concrete shows excellent mechanical properties and chemical resistance compared with conventional normal cement concrete. The polymer concrete is drawing a strong interest as high-performance materials in the construction industry. Resins using recycled PET offer the possibility of a lower source cost of materials for making useful polymer concrete products. Also the recycling of PET in polymer concrete would help solve some of the solid waste problems posed by plastics and save energy. The purposed of this paper is to propose the model for the stress-strain relation of recycled-PET polymer concrete at monotonic uniaxial compression and is to investigate for the stress-strain behavior characteristics of recycled-PET polymer concrete with different variables(strength, resin contents, curing conditions, addition of silane and ages). The maximum stress and strain of recycled-PET polymer concrete was found to increase with an increase in resin content, however, it decreased beyond a particular level of resin content. A ascending and descending branch of stress-strain curve represented more sharply at high temperature curing more than normal temperature curing. Addition of silane increases compressive strength and postpeak ductility. In addition, results show that the proposed model accurately predicts the stress-strain relation of recycled-PET polymer concrete

• Journal of the Korea Concrete Institute
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• v.18 no.6 s.96
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• pp.759-767
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• 2006

This paper presents a method to estimate the setting time of concrete using super retarding agent(SRA) and fly ash(FA) under various curing temperature conditions by applying maturity based on equivalent age. To estimate setting time, the equivalent age using apparent activation energy($E_a$) was applied. Increasing SRA content and decreasing curing temperature leads to retard initial and final set markedly. $E_a$ at the initial set and final set obtained by Arrhenius function showed differences in response to mixture type. It is estimated to be from $24{\sim}35KJ/mol$ in all mixtures, which is smaller than that of conventional mixture ranging from $30{\sim}50KJ/mol$. Based on the application of $E_a$ to Freisleben-Hansen and Pederson's equivalent age function, equivalent age is nearly constant, regardless of curing temperature and SRA contents. This implies that the concept of maturity is applicable in estimating the setting time of concrete containing SRA. A high correlation between estimated setting time and measured setting time is observed. Multi-regression model to determine appropriate dosage of SRA reflecting FA contents and equivalent age was provided. Thus, the setting time estimation method studied herein can be applicable to the concrete containing SRA and FA in construction fields.

• Journal of the korean academy of Pediatric Dentistry
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• v.33 no.4
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• pp.606-614
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• 2006

The purpose of this study was to evaluate the polymerization contraction of composite resin(Tetric $ceram^{(R)}$, Ivoclar Vivadent Liechtenstein) according to various liners(Tetric $flow^{(R)}$, Ivoclar Vivadent, Liechtenstein/$Ionosit^{(R)}$, DMG, German/ $Vitrebond,^{TM}$ 3M-ESPE, USA). The strain gauge method was used for measurement of polymerization shrinkage strain. Specimens were divided by 8 groups according to curing units and liners. Group A, E: Tetric $ceram^{(R)}$ bulk filing, Group B, F: Tetric $flow^{(R)}$ lining, Tetric $ceram^{(R)}$ filling, Group C, G: $Ionosit^{(R)}$ lining, Tetric $ceram^{(R)}$ filling, Group D, H: $Vitrebond^{TM}$ lining, Tetric $ceram^{(R)}$ filling. Group A, B, C and D were cured using the conventional halogen light($XL3000^{TM}$ 3M ESPE, USA) for 40 seconds at $400mW/cm^2$. Group E, F G and H were cured using light emitted diode(LED) light(Elipar Freelight $2^{TM}$, 3M-ESPE, USA) for 15 seconds at 800 $mW/cm^2$. Strain gauge attached to each sample was connected to a strainmeter. Measurements were recorded at each second for the total of 750 seconds including the periods of light application. Obtained data were analyzed statistically using Repeated measures ANOVA and Tukey test. The results of this were as follows : 1. Contraction stresses in flowable resin and glass ionomer lining group were lower than that in compomer lining group(p<0.05). 2, Contraction stresses in LED curing light groups were higher than that in halogen curing light groups, but there was no significant difference (p>0.05).

• Journal of Adhesion and Interface
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• v.10 no.4
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• pp.155-161
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• 2009

The most upcoming technical issue of automotive coating is the compact coating process. Pre-primed coating is the outstanding technology eliminating electro-deposition and primer coating process. The main properties of pre-primed coating for automotive are flexibility, corrosion resistance, and weldability. Therefore, we synthesized the conventional polyester, elastomeric polyester and polyvinylidene fluoride resins and evaluated their properties to use as weldable pre-primed automotive coatings. As the results of flexibility and curing behavior, the elastomeric polyester coating was most appropriate to use for the pre-primed automotive coatings.

• The korean journal of orthodontics
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• v.34 no.5 s.106
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• pp.429-438
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• 2004

The purpose of this study was to compare the effects of different light direction exposure times and setting times when using plasma arc light on shear bond strength of metal brackets. 240 extracted human premolars were randomly assigned to one of 16 groups Standardized brackets were bonded to enamel using different light curing units (Plasma arc light and Halogen light), exposure times (Plasma arc light 2. 4, 6 seconds and Halogen light 20 seconds). and light directions [Vertical direction [V] and Oblique direction [O]). 8 groups were tested after 5 minutes and the remaining 8 groups after 24 hours. The metal brackets were bonded with Transbond XT. Shear bond strength was measured by a universal testing machine. The results were as fellows: There were as differences between the shear bond strengths of the Vertical groups (V) and Oblique groups (O). regardless of exposure times and types of light curing units (p>0.05). The shear bond strength of the group with 2 seconds of plasma light were significantly lower than other exposure time groups (P<0.05). The shear bond strength tested after 5 minutes was lower than after 24 hours (p<0.05) The Adhesive Remment Index (ARI) score showed no statistically significant difference among the different groups. The results of this study suggested that the light direction of plasma arc light had no influence on the shear bond strength of metal brackets to enamel. and exposure times more than 4 seconds produced shear bond strengths similar to those Produced with a conventional halogen curing light.

• Journal of the Korean Recycled Construction Resources Institute
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• v.9 no.1
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• pp.66-74
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• 2021

The objective of this study is to evaluate the practical application potential and limitations of the modified fly ash(MFA) by vibration grinding as a partial replacement of ordinary portland cement(OPC). The test parameters investigated were the replacement level of fly ash(FA) and FA for OPC, varying from 10% to 40%, and curing temperatures of 5, 20, and 40℃. The various characteristics(including slump, air content, bleeding, setting time, compressive strength development, and hydration products) of MFA concrete were measured and then compared with those of the concrete with conventional FA. Test resul ts showed that the MFA prefers to FA in reducing the bl eeding of fresh concrete and enhancing the compressive strength gain at an early age. The compressive strength ratios between MFA and FA concrete specimens at an age of 1 day were 135%, 146%, and 111% at the curing temperatures of 5, 20, and 40℃, respectively. The corresponding ratios at an age of 28 days were approximately 110%, regardless of the curing temperatures. The X-ray diffraction analysis also revealed less calcium hydroxide products in MFA pastes than in FA pastes.

• Corrosion Science and Technology
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• v.12 no.1
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• pp.1-6
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• 2013

Recently Digital TV industry has drastically been moving the illuminating system, which causes an obvious product change from PDP and LCD to LED model to provide high-definition image. Due to strong competition in the digital industry, TV manufacturers make a great efforts to reduce production cost by using low-priced materials such as steels instead of aluminum and plastic etc. In this paper we have developed a new low-priced electrogalvanized steel sheet, which has a black resin composite layer, to substitute conventional high-priced PCM steel and plastic mold for rear cover panel in the digital TV. The black resin composite was prepared by mechanical dispersion of the mixture solution that consists of high solid polyester resin, melamine hardener, black pigment, micronized silica paste, polyacrylate texturing particle and miscellaneous additives. The composite solution was coated on the steel sheet using roll coater followed by induction furnace curing and cooling. Although the coated layer has a half thickness compared to the conventional PCM steels having $23{\mu}m$ thickness, it exhibits excellent quality for the usage of rear cover panel. The new steel sheet was applied to test products to get quality certification from worldwide electronic appliance customers. Detailed discussion provides in this paper including preparation of composite solution, roll coating technology, induction curing technology and quality evaluation from customers.