• Title/Summary/Keyword: conventional curing

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AN EXPERIMENTAL STUDY ON THE PHYSICAL PROPERTIES OF THE DENTURE BASE RESINS CURED BY MICROWAVE IRRADIATION (마이크로파 중합에 의한 의치상 레진의 물리적 성질에 관한 연구)

  • Kim, Hak Sun;Kim, Kwang Nam;Chang, Ik Tae
    • The Journal of Korean Academy of Prosthodontics
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    • v.28 no.2
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    • pp.109-124
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    • 1990
  • The purpose of this study was to investigate the physical propertise and determine whether three were any differences in the amount of porosity of the denture base resins cured by microwave irradiation and conventional water bath heating. The resins used in this study were K-33 resin and Acron MC resin. The properties selected were transverse strength, Knoop hardness, and density. A ten-power eyepiece and scanning electron microscope(Magnification of ${\times}$ 30and ${\times}$150)were used to examine the specimens for porosity. Through analyses of the data from this study, the following conclusions were obtained. 1. Microwave energy can be effectively use dtopolymerize poly(methylmethacrylate) denture base resins. 2. In the transverse strength, K-33 resin cured by microwave irradiation was the first highest, water bath cured K-33 resin the second, microwave cured Acron MC resin the third, water bath cured Acron MC resin the fourth. 3. In the Knoop hardness, K-33 resin cured by microwave irradiation was the first hardest, water bath cured K-33 resin the second, water bath cured Acron MC resin the third, microwave cured Acron MC resin the the fourth. 4. No significant difference was found between the density of resin denture bases polymerized by either method. 5. K-33 resin showed the most porosity for the microwave curing. But there was no significant difference in the Acron MC resin and other curing method.

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Evaluation of Physical and Mechanical Characteristics of Korean Epoxy Asphalt Mixtures (국산 에폭시 아스팔트 혼합물의 물리.역학적 특성 평가)

  • Kim, Byung-Hun;Baek, Jong-Eun;Lee, Hyun-Jong;Park, Hee-Mun
    • International Journal of Highway Engineering
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    • v.14 no.1
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    • pp.17-24
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    • 2012
  • This study evaluated the performance of Korean epoxy asphalt mixtures using several laboratory tests. Four types of epoxy asphalt mixtures were manufactured based on 13mm dense graded asphalt mixtures: three Korean and one Japanese epoxy asphalt mixtures where 20% or 40% of asphalt binder was replaced by epoxy resins. Curing time was determined as 3 and 6 hours for the mixtures containing 40% and 20% of epoxy resins, respectively. From the laboratory tests including wheel tracking, indirect tension fatigue, bending beam, and moisture susceptibility tests, it was concluded that the epoxy asphalt mixtures had superior performance than conventional asphalt mixtures except moisture susceptibility. Also, the performance of the Korean epoxy asphalt mixtures was comparable to the Japanese mixtures. Thermal coefficient, bond strength, and indirect tension tests were conducted to examine the applicability of the Korean epoxy asphalt mixtures to concrete repair. Its adhesion was strong enough to be bonded to surrounding concrete materials and its tensile strength was comparable to the concrete, but thermal expansion coefficient was 5 times greater than the surrounding concrete.

A Study on Fabrication of Monolithic Lightweight Composite Electronics Housing for Space Application (우주용 일체형 경량 복합재료 전자장비 하우징 제작에 관한 연구)

  • Jang, Tae Seong;Seo, Jung Ki;Rhee, Juhun
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.41 no.12
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    • pp.975-986
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    • 2013
  • This paper dealt with the fabrication and performance evaluation of the electronics housing made of lightweight composite materials, aiming at the enhancement of satellite mass savings by replacing conventional aluminum alloy widely used for satellite avionics with lightweight composite material. For this purpose, a fabrication process was designed to overcome low machinability of CFRP and to minimize the post-treatment. The composite housing with grid-stiffened and monolithic frame was made using co-curing method. Its performance was also evaluated regarding endurance, stiffness, thermal conductivity, electrical grounding, EMI protection and radiation shielding. The composite housing can provide the considerable mass savings over the aluminum housing with same dimension.

Monitoring of a CFRP-Stiffened Panel Manufactured by VaRTM Using Fiber-Optic Sensors

  • Takeda, Shin-Ichi;Mizutani, Tadahito;Nishi, Takafumi;Uota, Naoki;Hirano, Yoshiyasu;Iwahori, Yutaka;Nagao, Yosuke;Takeda, Nobuo
    • Advanced Composite Materials
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    • v.17 no.2
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    • pp.125-137
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    • 2008
  • FBG (Fiber Bragg Grating) sensors and optical fibers were embedded into CFRP dry preforms before resin impregnation in VaRTM (Vacuum-assisted Resin Transfer Molding). The embedding location was the interface between the skin and the stringer in a CFRP-stiffened panel. The reflection spectra of the FBG sensors monitored the strain and temperature changes during all the molding processes. The internal residual strains of the CFRP panel could be evaluated during both the curing time and the post-curing time. The temperature changes indicated the differences between the dry preform and the outside of the vacuum bagging. After the molding, four-point bending was applied to the panel for the verification of its structural integrity and the sensor capabilities. The optical fibers were then used for the newly-developed PPP-BOTDA (Pulse-PrePump Brillouin Optical Time Domain Analysis) system. The long-range distributed strain and temperature can be measured by this system, whose spatial resolution is 100 mm. The strain changes from the FBGs and the PPP-BOTDA agreed well with those from the conventional strain gages and FE analysis in the CFRP panel. Therefore, the fiber-optic sensors and its system were very effective for the evaluation of the VaRTM composite structures.

Wettability of denture relining materials under water storage over time

  • Jin, Na-Young;Lee, Ho-Rim;Lee, Hee-Su;Pae, Ahran
    • The Journal of Advanced Prosthodontics
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    • v.1 no.1
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    • pp.1-5
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    • 2009
  • STATEMENT OF PROBLEM. Poor wettability of denture relining materials may lead to retention problems and patient discomfort. PURPOSE. Purpose of this study is to compare and evaluate wettability of nine denture relining materials using contact angle measurements under air and water storage over time. MATERIAL AND METHODS. Nine denture relining materials were investigated in this study. Two heat-curing polymethyl-methacrylate(PMMA) denture base materials: Vertex RS, Lang, one self-curing polyethyl-methacrylate(PEMA) chairside reline resin: Rebase II, six silicone relining materials: Mucopren soft, Mucosoft, $Mollosil^{{R}}$ plus, Sofreliner Touch, GC $Reline^{TM}$ Ultrasoft, Silagum automix comfort were used in this experiment. Contact angles were measured using high-resolution drop shape analysis system(DSA 10-MK2, KRUESS, Germany) under three conditions(in air after setting, 1 hour water storage, and 24 hours water storage). Nine materials were classified into three groups according to material composition(Group 1: PMMA, Group 2: PEMA, Group 3: Silicone). Mean values of contact angles were compared using independent samples t-test and one-way ANOVA, followed by a Scheffe's post hoc analysis($\alpha$=0.01). RESULTS. Contact angles of materials tested after air and water storage increased in the following order: Group 1(PMMA), Group 2(PEMA), Group 3(Silicone). Heat-cured acrylic denture base resins had more wettability than silicone relining materials. Lang had the highest wettability after 24 hours of water storage. Silicone relining materials had lower wettability due to their hydrophobicity. Wettability of all denture relining materials, except Rebase II and $Mollosil^{{R}}$ plus, increased after 24 hours of water storage. CONCLUSIONS. Conventional heat-cured resin showed the highest wettability, therefore, it can be suggested that heat-cured acrylic resin is material of choice for denture relining materials.

A STUDY ON THE MARGINAL LEAKAGE OF CLASS II COMPOSITE RESIN INLAY (2급 와동 복합레진 인레이 충전 후 변연누출에 관한 연구)

  • Kang, Hyun-Sook;Choi, Ho-Young
    • Restorative Dentistry and Endodontics
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    • v.17 no.1
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    • pp.191-205
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    • 1992
  • The purpose of this study was to evaluate the microleakage of class II composite resin inlays and compare them with the conventional light-cured resin filling restorations. Class II cavities were prepared in 60 extracted human molars with which cervical margins were located below 1.0mm at the cemento-enamel junction using No. 701 tapered fissure carbide bur. All of the prepared cavities were restored as follows and divided into 6 groups. Group I and 2 were restored using direct filling technique and group 3,4,5 and 6 were restored using direct inlay technique that was cemented with dual-cured resin cements. group I: Cavities were restored with light-curing composite resin, Brilliant Lux. group 2. Cavities were restored with light-curing composite resin, Clearfil PhotoPosterior. group 3: Cavities were restored with Clearfil CR Inlay and heat treated at $125^{\circ}C$ for 7 minutes. group 4: Cavities were restored with same material as group 3 and heat treated at $100^{\circ}C$ for 15 minutes. group 5: Cavities were restored with Brilliant (Indirect esthetic system) and heat treated at $125^{\circ}C$ for 7 minutes. group 6: Cavities were restored with same material as group 5 and heat treated at $100^{\circ}C$ for 15 minutes. All specimens were polished with same method and thermocycled between $6^{\circ}C$ and $60^{\circ}C$, then immersed in a bath of 2.0% aqueous solution of basic fuchsin dye for 24 hours. Dyed specimens were sectioned longitudinally and dye penetration degree was read on a scale of 0 to 4 by Tani and Buonocore's method 45). The results were as follows: 1. Microleakage was observed rather at the cervical margins than at the occlusal margins in all groups. 2. Composite resin inlay groups showed significantly less leakage than direct filling groups at the cervical margins (p < 0.001). 3. In composite resin inlay groups, there was no significant difference in microleakage between specimens by heat treating temperature and time (p > 0.05). 4. There was no significant difference in leakage between each groups at the occlusal margins (p > 0.05).

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Fast liquid crystal switching performance on indium zinc oxide films with low curing temperature via ion-beam irradiation (이온빔 조사된 저온 소성 인듐 아연 산화막을 이용한 액정의 고속 스위칭 특성 연구)

  • Oh, Byeong-Yun
    • Journal of IKEEE
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    • v.23 no.3
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    • pp.904-909
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    • 2019
  • Using the ion-beam irradiated indium zinc oxide (IZO) films which was cured at $100^{\circ}C$, uniform LC and homogeneous alignment of liquid crystal (LC) molecules was achieved. The IZO film was deposited on the glass substrate at the curing temperature of $100^{\circ}C$ and irradiated by the ion-beam which is an LC alignment method. To verify the LC alignment characteristics, polarizing optical microscope and the crystal rotation method were used. Additionally, it was confirmed that the LC cell with the IZO films had an enough thermal budget for high-quality LC applications. Field emission scanning electron microscope was conducted as a surface analysis to evaluate the effect of the ion-beam irradiation on the IZO films. Through this, it was revealed that the ion-beam irradiation induced rough surface with anisotropic characteristics. Finally, electro-optical (EO) performances of the twisted-nematic cells with the IZO films were collected and it was confirmed that this cell had better EO performances than the conventional rubbed polyimide. Furthermore, the polar anchoring energy was measured and a suitable value for stable LC device operation was achieved.

Strength Characteristics of Non-Sintered Cement Mortar Utilizing Ferro-Nickel Slag as Fine Aggregate (페로니켈슬래그를 잔골재로 사용한 비소성 시멘트 모르타르의 강도 특성)

  • Ryu, Ji-Su;Jang, Kyung-Su;Na, Hyeong-Won;Hyung, Won-Gil
    • Journal of the Korea Institute of Building Construction
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    • v.23 no.4
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    • pp.359-367
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    • 2023
  • This experimental study investigates the replacement of conventional Portland cement and sand with non-sintered cement and ferro-nickel slag to formulate eco-friendly cement mortar. The examination aimed to understand the strength properties of non-sintered cement mortar using ferro-nickel slag as fine aggregate by classifying mortar production types, fine aggregates, and curing methodologies. From flexural and compressive strength tests, it was observed that non-sintered cement mortars, incorporating ferro-nickel slag as fine aggregate, exhibited superior strength when compared to both plain mortar and steam-cured non-sintered mortar. This increased strength is attributed to the influence of the particle size, density, and absorption capabilities of the ferro-nickel slag. Furthermore, X-ray Diffraction(XRD) analyses of the mortars verified the presence of MgO, a component of ferro-nickel slag, in the form of a composite oxide. This finding substantiates the consistent strength manifestation of non-sintered cement mortars utilizing ferro-nickel slag as a fine aggregate.

Assessing the Dehydration Pervaporation Performance for Purification of Industrially Significant 1, 2 Hexanediol/Water Mixtures Using Crosslinked PVA Membrane (가교된 PVA 분리막을 이용한 1, 2 hexanediol/water 혼합물의 투과증발 탈수 특성 연구)

  • Shivshankar Chaudhari;Se Wook Jo;Min Young Shon
    • Membrane Journal
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    • v.33 no.6
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    • pp.369-376
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    • 2023
  • In this study, the alternative to the energy-intensive conventional vacuum distillation process, an eco-friendly and energy-efficient pervaporation separation was employed in 1,2 hexane diol/water (HDO/water) mixture. The crosslinked PVA-glutaraldehyde was coated inside the alumina hollow fiber membrane (Al-HF). In the HDO/IPA pervaporation separation, optimization of the membrane concerning PVA/GA ratio, curing temperature, and pervaporation operating condition were performed. In the long-term stability test, the sustainable pervaporation separation performance giving flux in the range of 1.90~2.16 kg/m2h, and water content in permeate was higher than 99.5% (separation factor = 68) was obtained from the PVA/GA (molar ratio = 0.08, curing temperature = 80℃) coated Al-HF membrane from HDO/water (25/75, w/w, %) mixture at 40℃. Therefore, this work provides potential and inspiration for PVA-based membranes to mitigate excessive energy requirements in HDO/water separation by pervaporation.

Predicting tensile strength of reinforced concrete composited with geopolymer using several machine learning algorithms

  • Ibrahim Albaijan;Hanan Samadi;Arsalan Mahmoodzadeh;Danial Fakhri;Mehdi Hosseinzadeh;Nejib Ghazouani;Khaled Mohamed Elhadi
    • Steel and Composite Structures
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    • v.52 no.3
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    • pp.293-312
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    • 2024
  • Researchers are actively investigating the potential for utilizing alternative materials in construction to tackle the environmental and economic challenges linked to traditional concrete-based materials. Nevertheless, conventional laboratory methods for testing the mechanical properties of concrete are both costly and time-consuming. The limitations of traditional models in predicting the tensile strength of concrete composited with geopolymer have created a demand for more advanced models. Fortunately, the increasing availability of data has facilitated the use of machine learning methods, which offer powerful and cost-effective models. This paper aims to explore the potential of several machine learning methods in predicting the tensile strength of geopolymer concrete under different curing conditions. The study utilizes a dataset of 221 tensile strength test results for geopolymer concrete with varying mix ratios and curing conditions. The effectiveness of the machine learning models is evaluated using additional unseen datasets. Based on the values of loss functions and evaluation metrics, the results indicate that most models have the potential to estimate the tensile strength of geopolymer concrete satisfactorily. However, the Takagi Sugeno fuzzy model (TSF) and gene expression programming (GEP) models demonstrate the highest robustness. Both the laboratory tests and machine learning outcomes indicate that geopolymer concrete composed of 50% fly ash and 40% ground granulated blast slag, mixed with 10 mol of NaOH, and cured in an oven at 190°F for 28 days has superior tensile strength.