• Title/Summary/Keyword: contact angle test

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Fabrication and Characterization of an Antistiction Layer by PECVD (plasma enhanced chemical vapor deposition) for Metal Stamps (PECVD를 이용한 금속 스탬프용 점착방지막 형성과 특성 평가)

  • Cha, Nam-Goo;Park, Chang-Hwa;Cho, Min-Soo;Kim, Kyu-Chae;Park, Jin-Goo;Jeong, Jun-Ho;Lee, Eung-Sug
    • Korean Journal of Materials Research
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    • v.16 no.4
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    • pp.225-230
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    • 2006
  • Nanoimprint lithography (NIL) is a novel method of fabricating nanometer scale patterns. It is a simple process with low cost, high throughput and resolution. NIL creates patterns by mechanical deformation of an imprint resist and physical contact process. The imprint resist is typically a monomer or polymer formulation that is cured by heat or UV light during the imprinting process. Stiction between the resist and the stamp is resulted from this physical contact process. Stiction issue is more important in the stamps including narrow pattern size and wide area. Therefore, the antistiction layer coating is very effective to prevent this problem and ensure successful NIL. In this paper, an antistiction layer was deposited and characterized by PECVD (plasma enhanced chemical vapor deposition) method for metal stamps. Deposition rates of an antistiction layer on Si and Ni substrates were in proportion to deposited time and 3.4 nm/min and 2.5 nm/min, respectively. A 50 nm thick antistiction layer showed 90% relative transmittance at 365 nm wavelength. Contact angle result showed good hydrophobicity over 105 degree. $CF_2$ and $CF_3$ peaks were founded in ATR-FTIR analysis. The thicknesses and the contact angle of a 50 nm thick antistiction film were slightly changed during chemical resistance test using acetone and sulfuric acid. To evaluate the deposited antistiction layer, a 50 nm thick film was coated on a stainless steel stamp made by wet etching process. A PMMA substrate was successfully imprinting without pattern degradations by the stainless steel stamp with an antistiction layer. The test result shows that antistiction layer coating is very effective for NIL.

An experimental study on shear mechanical properties of clay-concrete interface with different roughness of contact surface

  • Yang, Wendong;Wang, Ling;Guo, Jingjing;Chen, Xuguang
    • Geomechanics and Engineering
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    • v.23 no.1
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    • pp.39-50
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    • 2020
  • In order to understand the shear mechanical properties of the interface between clay and structure and better serve the practical engineering projects, it is critical to conduct shear tests on the clay-structure interface. In this work, the direct shear test of clay-concrete slab with different joint roughness coefficient (JRC) of the interface and different normal stress is performed in the laboratory. Our experimental results show that (1) shear strength of the interface between clay and structure is greatly affected by the change of normal stress under the same condition of JRC and shear stress of the interface gradually increases with increasing normal stress; (2) there is a critical value JRCcr in the roughness coefficient of the interface; (3) the relationship between shear strength and normal stress can be described by the Mohr Coulomb failure criterion, and the cohesion and friction angle of the interface under different roughness conditions can be calculated accordingly. We find that there also exists a critical value JRCcr for cohesion and the cohesion of the interface increases first and then decreases as JRC increases. Moreover, the friction angle of the interface fluctuates with the change of JRC and it is always smaller than the internal friction angle of clay used in this experiment; (4) the failure type of the interface of the clay-concrete slab is type I sliding failure and does not change with varying JRC when the normal stress is small enough. When the normal stress increases to a certain extent, the failure type of the interface will gradually change from shear failure to type II sliding failure with the increment of JRC.

A study on the identification of underwater propeller singing phenomenon (수중 프로펠러 명음 현상의 규명에 관한 연구)

  • Kim, Taehyung;Lee, Hyoungsuk
    • The Journal of the Acoustical Society of Korea
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    • v.37 no.2
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    • pp.92-98
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    • 2018
  • This paper is a study on the generation mechanism of propeller singing based on the cavitation tunnel test, underwater impact test, finite element analysis and computational flow analysis for the model propeller. A wire screen mesh, a propeller and a rudder were installed to simulate ship stern flow, and occurrence and disappearance of propeller singing phenomenon were measured by hydrophone and accelerometer. The natural frequencies of propeller blades were predicted through finite element analysis and verified by contact and non-contact impact tests. The flow velocity and effective angle of attack for each section of the propeller blades were calculated using RANS (Reynolds Averaged Navier-Stokes) equation-based computational fluid analysis. Using the high resolution analysis based on detached eddy simulation, the vortex shedding frequency calculation was performed. The numerical predicted vortex shedding frequency was confirmed to be consistent with the singing frequency and blade natural frequency measured by the model test.

An Analysis about the Behavior of the Wiper Blade Including Incompressibility (비압축성을 고려한 와이퍼 블레이드의 거동 해석)

  • Chung, Won-Sun;Song, Hyun-Seok;Park, Tae-Won;Jung, Sung-Pil;Kim, Wook-Hyeon
    • Transactions of the Korean Society of Automotive Engineers
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    • v.18 no.2
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    • pp.83-90
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    • 2010
  • The windshield wiper consists of 4 parts: a blade, an arm, a linkage and a motor. The wiper blade makes contact with the windshield and is designed to be operated normally at an angle of 30~50 degrees to the front glass. If the contact pressure between the wiper blade and windshield surface is too high, noise and wear of the rubber will result. On the other hand, if the contact pressure is too low, the performance will do badly, since foreign substances such as dust and stains will not be removed well. The pressure and friction of the wiper blade has a great influence on its effectiveness in cleaning the front window. This is due to the contact of the rubber with the window. This paper presents the dynamic analysis method to estimate the performance of the flat type blade of the wiper system. The blade has a nonlinear characteristic since the rubber is an incompressible hyper-elastic and visco-elastic material. Thus, Structural dynamic analysis using a complex contact model for the blade is performed to find the characteristics of the blade. The flexible multi-body dynamic model is verified by the comparison between test and analysis result. Also, the optimization using the central composite design table is performed.

Kinetic Analysis of Golf Fat Shot (골프 Fat shot에 대한 운동역학적 분석)

  • Sohn, Jee-Hoon
    • The Journal of the Korea Contents Association
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    • v.13 no.10
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    • pp.523-532
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    • 2013
  • When the golf club hits the ground prior to making contact with the golf ball, we define it as 'fat shot'. The aim of this research was to investigate the difference between normal shot and fat shot in golf. Five candidates playing as recreational golfer participated in this research and they were all right-handed people. Time phase between each event, wrist cocking angle, elbow extension-flexion angle, backswing height, pelvis angle, thorax angle, L-GRF, R-GRF, pelvis linear velocity, pelvis angular velocity and COG path were calculated. For statistical analysis the paired T-test was used. An early un-cocking, an early right elbow extension and impact with leaving their weight behind foot were not reasons of fat shot. Backswing height, X-Factor, pelvis angle and thorax rotation angle were not different between normal shot and fat shot. But we could find a pattern of abrupt pelvic movement and weight shift to target direction just before impact in case of fat shot. In addition fat shot showed time-delayed and small value of pelvis linear velocity pattern to upward during downswing phase as against normal shot.

Study on the Neunghwaji fabrication techniques and characteristics (능화지(菱花紙) 제작기법 및 그 특성에 관한 연구)

  • Kim, soon kwan;Hong, soon chon
    • 보존과학연구
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    • s.32
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    • pp.5-24
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    • 2011
  • Neunghwaji(Embossed patterned paper) is a unique paper used for a traditional book cover in Korea. The research was carried out to investigate Neunghwaji's features. Physical property was studied through a test of tensile strength and folding endurance. Also, comparative analysis of virus resistance and waterproof ability was undertaken on Neunghwaji. 1. Folding endurance test showed that strength of non-embossed CB and HB decreased during deteriorating duration. Embossed CN and HN showed the strength increasing at early stage and decreasing from the 27th day of the deteriorating duration. Tensile strength was decreasing in both cases as deterioration progressed. 2. Growth of Arthrinium sp. fungus on embossed paper was 10% less than plain paper while Cladosporium sp. showed 20~30% less growth. Amur cork dyeing(H) showed 10~30% lower fungi growth than Gardenia seed dyeing(C). The result indicated that embossed paper has better virus resistance than Hanji, and Amur cork dyeing has better virus resistance than Gardenia seed dyeing. 3. Average contact angle of CN, CB, HN, and HB was $85{\sim}92^{\circ}$ and NON-N and NON-B was $59{\sim}63^{\circ}$. In detail, CN's contact angle was $1{\sim}7^{\circ}$ higher than CB's; HN was $1{\sim}6^{\circ}$ higher than HB. Therefore, it was found that embossed paper has higher contact angle than Hanji thus the former has better waterproof ability. The research suggested production technique of Neunghwaji and studied its features related to the technique. Neunghwaji was confirmed to have superior quality to Hanji though further study regarding above test result is needed to complement the research.

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Evaluation on machining accuracy according to convergence angle and radius of curvature value used for fabricating custom abutments (맞춤형 지대주 제작에 사용되는 수렴 각과 곡률 반경의 값에 따른 가공 정확도 평가)

  • Hong, Min-Ho;Choi, Sung-Min;Kwon, Tae-Yub
    • Korean Journal of Dental Materials
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    • v.44 no.4
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    • pp.329-336
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    • 2017
  • This study evaluates the machining accuracy of the custom abutment design according to the selected convergence angle and radius of curvature value in the CAD program. Ten custom abutments were designed based on dental CAD. And then, the fabricated custom abutment was scanned ten times using a contact scanner. The data of the scanned custom abutment was saved as "Test STL" file. The Geomagic studio software was used to superposition each exported as an "Test STL" file with the CAD-reference-model STL file (CRM) specified by the same name. In the experimental results, the A8 group (convergence angle $8^{\circ}$) showed lower error than the A4 group (convergence angle $4^{\circ}$) . In addition, the higher the radius of curvature, the less error in the top and chamfer regions of the custom abutment (p< 0.05). Overall, the convergence angle and radius of curvature value in the custom abutment design were found to affect the machining accuracy.

The Aging Characteristics of Polymer Electrical Insulation Materials bv UV Radiation and Salt Water Spray (옥외용 고분자 전기절연재료의 염수 및 UV조사에 의한 열화 특성)

  • 최남호;한상일;한상옥;박강식;김종석;박양범
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1997.11a
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    • pp.221-224
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    • 1997
  • In this study we investigated the acting characteristics of Polymers for electrical insulation by UV radiation and salt water spray treatment. We used the Polymers such as EPDM, SR. PTFE. EVA. We measured contact angle and surface resistance to know the aging characteristic of Polymer surface. And we use SEM to observe the change of the surface shape. Dry flashover voltage test impulse voltage test were carried for the polymer insulator(EVA) . Through this experiment and the analysis we could know the polymers have a good resistance to weathering conditions like as salt spray UV irradiation and mix of them. And we can compare the aging characteristics between Polymers. As a result, we could know that the surface characteristics of PTFE is better than the other. And the degree, electrical characteristics is affected by change of surface shape is not big.

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Hydrophilic Coating and Characterization of PVDF Membrane with Flower Type Cross-section made from Thermally Induced Phase Separation (열유도 상분리로 제조한 플라워 형태 단면을 갖는 PVDF 분리막의 친수성 코팅 및 특성평가)

  • Im, Kwang Seop;Lee, Jeong Woo;Jang, Jae Young;Nam, Sang Yong
    • Membrane Journal
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    • v.29 no.6
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    • pp.362-376
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    • 2019
  • In this study, hydrophilic coating characteristics of PVDF [poly(vinylidene fluoride)] hollow fiber membranes with flower type cross-section prepared by thermally induced phase separation were studied. The hollow fiber used in this study was provided from PureEnvitech Co. Ltd., and the hydrophilic coating experiment was performed with different concentration and number of coating of PEBAX 1657, 2533 and 3533 block copolymer solution using a dip coating method. The hydrophilic coated hollow fiber membrane was characterized to scanning microscope and contact angle measurements to determine the degree of hydrophilization. As a result of SEM characterization, it was confirmed that the thickness of the coating layer increased as the coating concentration increased and the number of coatings increased. Contact angle of surface of hollow fibers decreased as the concentration of the coating solution increased and the number of coatings increased. Gas permeance of oxygen gas was measured for the application of the hydrophilized hollow fiber to Membrane Areated Biofilm Reactor. As a result of gas permeation test, it was confirmed that gas permeance decreased with increasing coating concentration and number of coatings, and the more hydrophilized hollow fiber coated with PEBAX 1657 showed lower gas permeance than those coated with PEBAX 2533 and 3533.

Surface Modification of Polystyrene (PS) by Atmospheric Pressure Plasma (상압 플라즈마를 이용한 Polystyrene (PS)의 표면개절)

  • Lee, Jong-Su;Shin, Hyun-Seok;Seok, Jin-Woo;Jang, Gyu-Wan;Beag, Yeong-Hwan
    • Journal of the Korean Vacuum Society
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    • v.18 no.1
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    • pp.1-8
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    • 2009
  • Hydrophilic Surface modification of Polysarene (PS) was performed by Atmospheric Pressure Plasma (APP). Air or 0, gases were used for carrier gases and RF power was changed from 150 to 350 W. We controlled the treatment time as 1 time to 4 time passing through the plasma region. when the carrier gas was air, the water contact angle on the PS surface was decreased from $91^{\circ}$ to $20^{\circ}$. And the surface energy increased from 45.74 dyne/cm to 68.48 dyne/cm. In case of the $O_2$ plasma treatment, at 300 W of RF power and 4 times treatment, the water contact angle on the PS. Surface was decreased from $91^{\circ}$ to $17^{\circ}$ and the surface energy was increased from 45.74 dyne/cm to 69.73 dyne/cm. The surface energy was increased by polar force not by dispersion force. Improvement of surface properties can be explained by the formation of new hydrophilic groups which is identified as C-O, C=O by XPS analysis. The contact angle of APP treated PS surface kept in air was increased with time elapse, but maintained same value when it was kept in water. We treated the PS surface by APP and deposited Cu as $4,000\;{\AA}$ and $8,000\;{\AA}$ by thermal evaporation. The adhesion between sample and Cu thin film improvement of treated PS surface against untreated sample. could be verifiable by Tape test (ASTM D3359)