• Title/Summary/Keyword: compound analysis

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Chemical Properties of the Insecticidal Compound Produced by an Actinomycetes, SS-4993 (방선균 SS-4993이 분비하는 살충물질의 화학적 성상 및 작용기작)

  • 이은정;강경돈;황교열;김두호;이상몽;김신덕;성수일
    • Journal of Sericultural and Entomological Science
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    • v.41 no.3
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    • pp.180-184
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    • 1999
  • The insecticidal compound priduced by Streptomyces SS-4993 strain was indicated to be a relatively stable small compound by pancreatin treatment. The active compound was adsorbed on HP20 and eluted with 70% acetone. Then, the eluate was extracted with ethyl acetate. The content of the extract was determined by thin layer chromatography (Silica gel 60 F254, hexane-ethyl ether-acetic acid,80 : 20 :1). Three active bands (Rf 0.08, 0.07, 0.88) were identified by dermal application using Bombyx mori larvae. Electrophoretic analysis revealed that the injection of strain SS-4993 culture broth into B. mori larvae induce the reduction of the hemolymph proteins level. Especially, the level of apolipophorin-I was decreased drastically.

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Performance Efficiency of Compound CVTs with a 2K-H II (2K-H II 형식 복합형 무단변속기의 효율실험)

  • Park J.M.;Kim Y.S.;Lee S.H.;Choi S.H.
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2005.10a
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    • pp.670-673
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    • 2005
  • We designed the compound CVT (Continuously Variable Transmissions) by combining power circulation mode CVT and power split mode CVT, which have been proposed for connecting 2K-H II differential gear to the V- belt type CVU (Continuously Variable Unit), as an input coupled type. With the designed compound CVT, we carried out theoretical analysis and performance experiments. We proved that the compound CVT had a better performance than either of the power circulation mode or power split mode.

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Synthesis, crystal structure, and thermal property of piperazine-templated copper(II) sulfate, {H2NCH2CH2NH2CH2CH2}{Cu(H2O)6}(SO4)2

  • Kim, Chong-Hyeak;Park, Chan-Jo;Lee, Sueg-Geun
    • Analytical Science and Technology
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    • v.18 no.5
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    • pp.381-385
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    • 2005
  • The title compound, $\{H_2NCH_2CH_2NH_2CH_2CH_2\}\{Cu(H_2O)_6\}(SO_4)_2$, I, has been synthesized under solvo/hydrothermal conditions and their crystal structure analyzed by X-ray single crystallography. Compound I crystallizes in the monoclinic system, $P2_1/n$ space group with a = 6.852(1), b = 10.160(2), $c=11.893(1){\AA}$, ${\beta}=92.928(8)^{\circ}$, $V=826.9(2){\AA}^3$, Z = 2, $D_x=1.815g/cm^3$, $R_1=0.031$ and ${\omega}R_2=0.084$. The crystal structure of the piperazine templated Cu(II)-sulfate demonstrate zero-dimensional compound constituted by doubly protonated piperazine cations, hexahydrated copper cations and sulfate anions. The central Cu atom has a elongated octahedral coordination geometry. The crystal structure is stabilized by three-dimensional networks of the intermolecular $O_{water}-H{\cdots}O_{sulfate}$ and $N_{pip}-H{\cdots}O_{sulfate}$ hydrogen bonds between the water molecules and sulfate anions and protonated piperazine cations. Based on the results of thermal analysis, the thermal decomposition reaction of compound I was analyzed to have three distinctive stages.

An Analysis of Concept Description and Model and Student Understanding About Ionic Compound in Textbooks Developed Under the 2009 Revised National Curriculum (2009 개정 교육과정에 따른 교과서에서 이온 화합물의 설명 개념과 모형 및 학생 이해도 분석)

  • Shin, He Young;Woo, Ae Ja
    • Journal of the Korean Chemical Society
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    • v.60 no.5
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    • pp.362-373
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    • 2016
  • In this study, ionic compound in the science textbooks developed under the 2009 revised national curriculum were analyzed in terms of the scientific concept and model description and the student understanding through the questionnaires. Analysis of textbooks was performed for science2 of middle school and chemistry I & II of high school. Questionnaire was carried out with 194 students including middle school 2nd grade and high school 1st-3rd grade. The results are as follows: First, as a result of analysis of textbooks, scientific concepts and models used to explain the ionic compound showed differences depending on the types of textbooks. In addition, scientific models were provided with or without explanation for the scientific concepts. Second, analysis of the questionnaire showed that students didn’t properly understood scientific concepts and models in the ion formation, stoichiometric ratio between ions.

Bioconversion of Ginsenosides from Red Ginseng Extract Using Candida allociferrii JNO301 Isolated from Meju

  • Lee, Sulhee;Lee, Yong-Hun;Park, Jung-Min;Bai, Dong-Hoon;Jang, Jae Kweon;Park, Young-Seo
    • Mycobiology
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    • v.42 no.4
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    • pp.368-375
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    • 2014
  • Red ginseng (Panax ginseng), a Korean traditional medicinal plant, contains a variety of ginsenosides as major functional components. It is necessary to remove sugar moieties from the major ginsenosides, which have a lower absorption rate into the intestine, to obtain the aglycone form. To screen for microorganisms showing bioconversion activity for ginsenosides from red ginseng, 50 yeast strains were isolated from Korean traditional meju (a starter culture made with soybean and wheat flour for the fermentation of soybean paste). Twenty strains in which a black zone formed around the colony on esculin-yeast malt agar plates were screened first, and among them 5 strains having high ${\beta}$-glucosidase activity on p-nitrophenyl-${\beta}$-D-glucopyranoside as a substrate were then selected. Strain JNO301 was finally chosen as a bioconverting strain in this study on the basis of its high bioconversion activity for red ginseng extract as determined by thin-layer chromatography (TLC) analysis. The selected bioconversion strain was identified as Candida allociferrii JNO301 based on the nucleotide sequence analysis of the 18S rRNA gene. The optimum temperature and pH for the cell growth were $20{\sim}30^{\circ}C$ and pH 5~8, respectively. TLC analysis confirmed that C. allociferrii JNO301 converted ginsenoside Rb1 into Rd and then into F2, Rb2 into compound O, Rc into compound Mc1, and Rf into Rh1. Quantitative analysis using high-performance liquid chromatography showed that bioconversion of red ginseng extract resulted in an increase of 2.73, 3.32, 33.87, 16, and 5.48 fold in the concentration of Rd, F2, compound O, compound Mc1, and Rh1, respectively.

Alteration in Phenolic Compounds and Antioxidant Activities of Aronia melanocarpa Ethanol Extracts following Fermentation Using Different Strains of Leuconostoc mesenteroides to Develop Natural Antibiotic Alternative (항생제 대체 천연물질을 위한 아로니아 주정 추출물 개발에 있어 다양한 Leuconostoc mesenteroides 균주를 이용한 발효가 페놀계 화합물 및 항산화활성 변화에 미치는 영향)

  • Hwang, Joo Hwan;Kang, Ju Hui;Lee, Ki Hwan;Lee, Jae Hoon;Lee, Sang Moo;Kim, Nam Hyung;Kim, Joo Young;Kim, Eun Joong
    • Korean Journal of Organic Agriculture
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    • v.22 no.4
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    • pp.825-839
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    • 2014
  • Antioxidant activity is important for reducing oxidative stress that causes various metabolic disorders. Metabolic disorders are highly related to loss of productivity in livestock. Therefore, development of effective antioxidant compounds originating from plants is important for organic agriculture. Phenolic compounds in edible plants are regarded as major components relevant to antioxidant activity. The present study investigated the changes in antioxidant activity and phenolic compound profiles of Aronia (Aronia meloncarpa) by fermentation using different strains of Leuconostoc mesenteroides. A total of 5 strains of L. mesenteroides were used as starter cultures and their ${\beta}$-glucosidase activities were measured. A total of 6 experiment runs were prepared, one for control (uninoculated) and the others (inoculated) for treatments. For biological activity, antioxidant and antibacterial activities were measured. For phenolic compound profiling, TLC and HPLC analysis were performed. The strains of KACC12313 and KACC12315 showed greater enzyme activity than others. Treatment with KCCM35046 showed strong and broad antibacterial activity against to Listeria monocytogenes. Treatments with KCCM35046 and KACC12315 showed the highest total polyphenol content. The highest antioxidant activity was found in KACC12315 treatment. No remarkable alteration was found in thin layer chromatography (TLC) analysis. In phenolic compound profiling analysis, KCCM35046 showed notable alteration in compound area ratio compared to others and also showed the highest caffeic acid content. In chlorogenic acid, treatments with KCCM35046 and KACC12315 showed great content than others. Treatment with KACC12315 showed the greatest content of trans-ferulic acid. As a result of relative performance indexing analysis, L. mesenteroides KCCM35046 and KACC12315 were selected as the best strain for the fermentation of Aronia.

Analysis on inundation characteristics by compound external forces in coastal areas (연안 지역의 복합 외력에 의한 침수 특성 분석)

  • Kang, Taeuk;Sun, Dongkyun;Lee, Sangho
    • Journal of Korea Water Resources Association
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    • v.54 no.7
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    • pp.463-474
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    • 2021
  • The various external forces can cause inundation in coastal areas. This study is to analyze regional characteristics caused by single or compound external forces that can occur in coastal areas. Storm surge (tide level and wave overtopping) and rainfall were considered as the external forces in this study. The inundation analysis were applied to four coastal areas, located on the west and south coast in Republic of Korea. XP-SWMM was used to simulate rainfall-runoff phenomena and 2D ground surface inundation for watershed. A coupled model of ADCIRC and SWAN (ADCSWAN) was used to analyze tide level by storm surge and the FLOW-3D model was used to estimate wave overtopping. As a result of using a single external force, the inundation influence due to storm surge in most of the coastal areas was greater than rainfall. The results of using compound external forces were quite similar to those combined using one external force independently. However, a case of considering compound external forces sometimes created new inundation areas that didn't appear when considering only a single external force. The analysis considering compound external forces was required to reduce inundation damage in these areas.

A Compound Term Retrieval Model Using Statistical lnformation (통계적 정보를 이용한 복합명사 검색 모델)

  • 박영찬;최기선
    • Korean Journal of Cognitive Science
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    • v.6 no.3
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    • pp.65-81
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    • 1995
  • Compound nouns as a composition of multiple nouns exhibit diverse occurence patterns in the texts and have varying degree of meaning coherence.The problem of compound nouns in information retrieval is to find a method to represent and identify the compositive patterns of each words.This paper explains how the cooccurrence patterns are related with the meaning of each compound noun and the information of such relations that can be mechanically acquired from texts is used in ranking the candidated documents for a given query.The main theme of the paper is that compound nouns can be categorized according to their occurrence patterns of simple nouns and these occurrence patterns can be formalized by statistical analysis without large dictionary or complex compositive rules.Our suggested model achieved about 7.75% improvement over the best precision of the other methods at each recall measurements on Korean test collection.

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Watertightness and Crack Reduction Property of Concrete added Fluosilicate Salt Based Inorganic Compound for Watertight Concrete (수밀 콘크리트용 규불화염계 무기 조성물을 첨가한 콘크리트 수밀성 및 균열저감 특성)

  • Kim Da-Su;Khil Bae-Su;Choi Se-Jin;Park Min-Yong;Lee Seong-Yeon;Yeo Byung-Chul
    • Proceedings of the Korean Institute of Building Construction Conference
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    • v.y2004m10
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    • pp.33-38
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    • 2004
  • This study was performed to know watertightness and reduction effect and crack occurred by hydration heat, restraint of multiplication of hydration heat, through mechanical test, strength test and crack control test using fluosilicate salt based inorganic compound made from by-product during phosphoric acid manufacturing process. Mix proportions for experiment were modulated at 0.45 of water to cement ratio and $0.5-2.0\%$ of adding ratio of fluosilicate salt based inorganic compound. Evaluation for watertightness of concrete was carried out permeability, absorption test and porosity analysis. Effect of crack reduction was evaluated by length, drying shrinkage as well as stress change of hardened concrete at unrestraint/restraint state and also elucidated crack pattern on the concrete surface. It is ascertained that characteristics of crack resistance and watertightness for concrete was improved by an adequate addition of fluosilicate salt based inorganic compound.

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A Study on the Autofrettage Analysis in Single and Compound Cylinders (단일 및 복합실린더에서 자긴가공 해석에 관한 연구)

  • Shim, Woo-Sung;Kim, Jae-Hoon;Lee, Young-Shin;Cha, Ki-Up;Hong, Suk-Kyun
    • Journal of the Korean Society of Propulsion Engineers
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    • v.12 no.4
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    • pp.7-15
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    • 2008
  • In manufacturing aircraft, safety and lightness of structure are important factors. Utilizing autofrettage technique, these benefits can be obtained. This technique is most frequently applied to a single cylinder. However, the Bauschinger effect reduces the benefits of autofrettage process Therefore, there is increasing interest in the use of compound cylinder that combine shrink fit and autofrettage. In this paper, single and compound cylinders that has same geometry were considered. It was found that compound cylinder which was autofrettaged has lower tangential hoop stress and plastic strain than single cylinder at bore. This means a reduction in the impact of the Bauschinger effect after shrink-fitting which produces the beneficial bore hoop stress.