• 제목/요약/키워드: composite ceramic

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Bi-2223/Ag 고온초전도선재의 가공균일성에 미치는 인발공정연구 I (Bi-2223/Ag HTS Drawing Process Study for Uniform Deformation I)

  • 김상철;하홍수;오상수;이동훈;양주생;하동우;권영길;한일용;이종건
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2002년도 춘계학술대회 논문집 초전도 자성체
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    • pp.55-58
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    • 2002
  • PIT method which is used at fabricating Bi-2223/Ag HTS wire includes a drawing process, conventional deformation method. Drawing of meta1(Ag) and ceramic (BiSrCaCuO) composite is also difficult and significant for uniform deformation. In this paper, parameters of uniform deformation was studied at Bi-2223/ Ag multifilamentary HTS wire. Powder and rod as a starting precursor was compared at 55 filament and 54 filament Bi-2223/Ag HTS wire, respectively. Micro-hardness and area COV of the filaments was also evaluated when the diameters were decreased through drawing operations.

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Calcite 필러를 함유한 유리 복합체의 표면형상과 반사율 (Surface Morphology and Reflectance of Calcite Filler in Glass Composites)

  • 전재승;황성진;안지환;김형순
    • 한국재료학회지
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    • 제19권8호
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    • pp.407-411
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    • 2009
  • Reflection properties, such as specular reflection and diffuse reflection, are very important optical properties for the reflector, which has high reflectance in the display and architecture industry. Calcite is lowcost, nontoxic, and stable over a wide temperature range. Therefore, it is one of the most widely using fillers in many industries and has some advantages over titania as a filler to improve reflectance. However, optical properties, especially those of ceramic-filled composites, have not been analyzed. We studied the reflectance of calcite composites with their surface roughness. The reflectance of the composites was determined using a UV-visible spectrometer. The surface morphology and the micro-structure of the composites were investigated by atomic force microscope. The reflectance of the composites was improved by increasing the content of calcite in the calcite-frit composite. The reflectance is related with the surface roughness in the composites. However, the reflectance depends on the calcite contents in materials with similar surface roughness.

도재(陶材)와 도재(陶材) 소부용(燒付用) Ni-Cr계(系) 합금간(合金間)의 결합력(結合力)에 관(關)한 실험적(實驗的) 연구(硏究) (AN EXPERIMENTAL STUDY ON THE BONDING STRENGTH BETWEEN PORCELAIN AND Ni-Cr BASED PORCELAIN ALLOY)

  • 김경선
    • 대한치과보철학회지
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    • 제19권1호
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    • pp.61-73
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    • 1981
  • The effects of the opaque porcelain firing temperature, the bonding agent and the degassing prior to the opaque firing On the bond strength were investigated by means of the tensile shear stIe$. The diffusional behaviours at the interface of the porcelain and the alloy, and .the microstructures of the ceramic and metal composite were studied for understanding the bonding mechanism. The results obtained in this experiment were summarizd as follow; 1. With no application of bonding agent, the tensile shear strength of the specimen firing at $1840^{\circ}F$ was higher than that of the specimen firing at $1760^{\circ}F$. 2. The highest bond strength was obtained by application of bonding agent without degassing prior to the opaque firing. 3. Application of bonding agent after the degassing showed the lowest bond strength. 4. The greater number of pores were observed at the firing temperature of $1840^{\circ}F$ than that of $1760^{\circ}F$ in the porcelain and the interface respectively.

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Pt/Ti/Si 기판에서의 후속열처리에 따른 PZT 박막의 형성 및 특성

  • 백상훈;백수현;황유상;마재평;최진석;조현춘
    • 한국재료학회:학술대회논문집
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    • 한국재료학회 1993년도 춘계학술발표회
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    • pp.64-65
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    • 1993
  • MPB 조성영역인 Zr/Ti=52/48의 composite ceramic target을 사용하여 RF magnetron sputtering 방법으로 기판온도 약 30$0^{\circ}C$에서 RZT 박막을 Pt/Ti/Si 기판위에 증착시켰다. 안정상인 perovskite 구조를 형성시키기 위하여 PbO분위기에서 furnace annealing 과 Repid thermal annealing을 실시하여 열처리 방법에 따른 상형성 및 계면반응과 그에 따른 전기적 특성을 고찰 하였다. Pt 의 두께가 250$\AA$인 경우 furnace annealing 시 $650^{\circ}C$에서 perouskite 상이 형성되었으나 Pt층이 산소의 확산을 방지하지 못하여 상부의 Ti 층이 TiOx로 변태하였으며 하부의 Ti는 Si 과 반응하여 Ti-silicide 롤 변태하였다. 또한 75$0^{\circ}C$,60sec 인 경우 Pt 층의 응집화가 관찰되어 하부전극으로서 적용이 적절하지 못하다. 급속열처리를 실시한 경우에도 마찬가지로 Ti 층이 TiOx 와 silicide 층으로 변태되었다. Pt의 두께가 1000$\AA$인 경우에도 250$\AA$와는 달리 RTA 시 (III)방향으로 Furace annealing 시(001)방향으로 우선 성장하였다. 이는 Ti(001), P(111),PZT(111)면의 lattic mismatch 가 매우 작은데다 RTA 시 계면반응이 거의발생하지 않아 PZT 박막이 (111) 방향으로 우선 성장한 것으로 보인다. Furnace annealing 경우는 심한 계면반응이 발생하여 Pt층에 어느 정도 영향을 주었기 때문에 우선성장 방향이 바뀌었다구 생각한다.

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풍차형 초음파 전동기의 회전자에 인가된 힘이 회전특성에 미치는 영향 (Effect of Pressing Force Applied to a Rotor on Revolution Characteristics in the Windmill Type Ultrasonic Motor)

  • 김영균;김진수
    • 한국전기전자재료학회논문지
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    • 제13권5호
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    • pp.390-395
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    • 2000
  • The ultrasonic motor have recently begun to be used for certain unique practical utilizations in the fields of industrial medical consumer and automotive applications. Ultrasonic motor stimulated to ultrasonic oscillations by piezoelectrics to drive a rotor via friction contact. The metal and ceramic composite component was used as the stator element to generate ultrasonic vibrations. The ultrasonic motor used here was the windmill type ultrasonic motor operated by single-phase AC source. The windmill type ultrasonic motors has only three components; a stator element of two windmill shape slotted metal endcaps a rotor and a bearing. In this paper a prototype motor with 11.35 mm diameter was fabricated then relationship between the pressing force applied to a rotor and the rotation characteristic of windmill type ultrasonic motor are investigated when stator’s slots was changed from 4, 6, 8 and thickness changed from 0.15, 0.20 mm, respectively. Optimum pressing force applied to a rotor in the six stators was 1.2 mN.

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새롭게 개발된 휴대용 미끄럼 저항 측정기의 성능검증 (The Validation of Newly Developed Portable Slipmeter)

  • 김정수
    • 한국안전학회지
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    • 제28권1호
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    • pp.18-23
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    • 2013
  • The purpose of this study were to develop and validate a prototype slipmeter used on-site floor. The developed slipmeter was dreg sled type. It measured static coefficient of friction(SCOF). The developed slipmeter was evaluated with ASTM 2508-11 which use four different standard surfaces(polished granite, glazed porcelain, vinyl composite tile, and ceramic tile). The SCOF was then measured with developed slipmeter under the three different contaminants and seven different floors. The test results of slipmeter were also compared with those of BOT-3000, floor surface roughness, and human perception. The test results revealed that developed slipmeter successfully ranked all four standard surfaces and differentiated among standard surfaces with varying degrees of slipperiness. The developed slipmeter couldn't properly measure slipperiness under the two kind of floors(polished tile, ground steel plate) and one kind of contaminant(glycerol). The test results of developed slipmeter had stronger correlation with those of BOT-3000 and floor roughness under the water and detergent solution than under the glycerol. The test results of developed slipmeter also showed stronger correlation with those of BOT-3000 and surface roughness than those of human perception. The newly developed slipmeter had been found to give consistent results under the test conditions except for two kind of floors(polished tile, ground steel plate) and one kind of contaminant(glycerol).

다공성 확산층을 이용한 한계전류형 지르코니아 산소센서 (Limit-current type zirconia oxygen sensor with porous diffusion layer)

  • 오영제;이칠형
    • 센서학회지
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    • 제17권5호
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    • pp.329-337
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    • 2008
  • Simple, small and portable oxygen sensors were fabricated by tape casting technique. Yttria stabilized zirconia containing cordierite ceramics (YSZC) were used as a porous diffused layer of oxygen in pumping cell. Yttria stabilized zirconia (YSZ) solid electrolyte, YSZC porous diffusion layer and heater-patterned ceramic sheets were prepared by co- firing method. Limit current characteristics and the linear relationship of current to oxygen concentration were observed. Viscosity variation of the slurries both YSZ and YSZC showed a similar behavior, but micro pores in the fired sheet were increased with increasing of the cordierite amount. Molecular diffusion was dominated due to the formation of large pores in porous diffusion layer. The plateau range of limit current in porous-type oxygen sensor was narrow than the one of aperture-type oxygen sensor. However limit current curve was appeared in porous-type oxygen sensor even at the lower applied voltage. The plateau range of limit-current was widen as increasing the thickness of porous diffusion layer of the YSZ containing cordierite. Measuring temperature of $600{\sim}650^{\circ}C$ was recommended for limit-current oxygen sensor. Porous diffusion layer-type oxygen sensor showed faster response than the aperture-type one and was stable up to 30 days running without any crack at interface between the layers.

Effect of Post Surface Modifications on Tribological Properties of Electrodeposited Ni/Ni-SiC coatings

  • Gyawali, Gobinda;Joshi, Bhupendra;Tripathi, Khagendra;Lee, Soo Wohn
    • 한국표면공학회:학술대회논문집
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    • 한국표면공학회 2015년도 춘계학술대회 논문집
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    • pp.43-44
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    • 2015
  • Electrodeposited Ni and Ni-SiC composite coatings were prepared on Cu substrates by using the Ni-Sulfamate electrolytic bath. Thus prepared samples were subjected for the two different types of post surface modification techniques; i.e. Laser Surface Texturing (LST) and Ultrasonic Nano Surface Modification (UNSM), respectively in order to investigate their effects on surface and interface related properties of the coatings. Hemispherical dimples, with 80 to 200 um dimple spacing, were created and examined on the surfaces of the materials studied. The results revealed that micro-surface texturing with 150 um dimple spacing considerably improved the coefficient of friction. Dimple spacing accuracy and incorporated second phase ceramic particles both contributed significantly to reduction in coefficient of friction. On the other hand, application of UNSM considerably modified the surface topography, led to increase the Vickers microhardness, and reduced the wear and coefficient of friction as compared to non UNSM treated Ni and Ni-SiC samples.

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$Al_2O_3-ZrO_2/A_2O_3$-TZP 세라믹스의 제조 및 기계적.전기적 특성 (Mechanical and Electrical Characteristics of $Al_2O_3-ZrO_2/A_2O_3$-TZP Structural Ceramics)

  • 박재성;남효덕;이희영
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 1999년도 추계학술대회 논문집
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    • pp.335-338
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    • 1999
  • The effect of monoclinic $ZrO_2$(pure) and tetragonal $ZrO_2$ containing 5.35wt% $Y_2$$O_3$(Y-TZP) addition on the mechanical properties and thermal shock resistance of $Al_2$$O_3$ ceramic were investigated. The addition of $ZrO_2$(m) and Y-TZP increased sintering density of $Al_2$$O_3$. The vickers hardness increased with increasing the volume fraction of Y-TZP going through a maximum at 20wt%. The hardness of the specimens was found to be depend on the sintering density. With increasing the volume fraction of $ZrO_2$(m) and Y-TZP, the fracture toughness of the composite is increased. This result may be taken as evidence that toughening of ${Al_2}{O_3}$ can also be achieved by the transformation toughening and microcrack toughening of $ZrO_2$. The property of the& shock for ${Al_2}{O_3}$-$ZrO_2$ composites was improved by increasing the volume fraction of monoclinic $ZrO_2$(pure).Grain size increased with increasing the volume fraction of $ZrO_2$.

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Up-conversion Luminescence Characterization of CeO2:Ho3+/Yb3+ Particles Prepared by Spray Pyrolysis

  • Jung, Kyeong Youl;Min, Byeong Ho;Kim, Dae Sung;Choi, Byung-Ki
    • Current Optics and Photonics
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    • 제3권3호
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    • pp.248-255
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    • 2019
  • Spherical $CeO_2:Ho^{3+}/Yb^{3+}$ particles were synthesized using spray pyrolysis, and the upconversion (UC) properties were investigated with changing the preparation conditions and the infrared pumping power. The resulting particles had a size of about $1{\mu}m$ and hollow structure. The prepared $CeO_2:Ho^{3+}/Yb^{3+}$ particles exhibited intense green emission due to the $^5F_4/^5S_2{\rightarrow}^5I_8$ transition of $Ho^{3+}$ and showed weak red or near-IR peaks. In terms of achieving the highest UC emission, the optimal concentrations of $Ho^{3+}$ and $Yb^{3+}$ were 0.3% and 2.0%, respectively. The UC emission intensity of prepared $CeO_2:Ho^{3+}/Yb^{3+}$ particles had a linear relationship with crystallite size and concentration quenching was caused by dipole-dipole interaction between the same ions. Based on the dependency of UC emission on the pumping power, the observed green upconversion was achieved through a typical two-photon process and concluded that the main energy transfer from $Yb^{3+}$ to $Ho^{3+}$ was involved in the ground-state adsorption (GSA) process.