• 대한치과기공학회지
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• 제2권1호
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• pp.55-59
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• 1980

이와 같은 세 기술은 많은 도재용착주조관의 수리에 이용된다고 할 수 있고 이런 기술은 완전한 보철물을 다시 만들지 않고 연장된 도재용착주조관의 수리에 적용할 수 있는 것이다. 금속덮개(over casting)와 핀에서 유지를 얻는 금속 전장판에 의한 수리의 성공은 다시 제작한 도재용착주조관의 그것과 비교할 만하다. 그러나 도재에 합성수지(composite resin)를 결합시켜 수리하는 방법은 합성수지(composite resin)가 도재보다 잘 닳을 뿐만 아니라 색깔의 안정성도 좋지 않으며 도재가 금속판에 용착될 때 창조되는 결합력보다 silance bonding agent를 사용하여 창조되는 결합력 즉 화학적 결합(chemical bond)이 약하기 때문에 좋다고 할 수는 없다. 그러므로 silance bond repair에 관한 연구는 앞으로도 여러분들과 함께 더욱 더 연구할 과제가 아닌가 생각되는 바입니다.

• The Journal of Advanced Prosthodontics
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• 제3권4호
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• pp.186-189
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• 2011

PURPOSE. Porcelain fused to metal (PFM) crowns provide the best treatment option for teeth that have a large or defective restoration. More than 20% of teeth with PFM crowns or bridges require non-surgical root canal treatment (NSRCT). This may be due to the effect of restorative procedures and the possible leakage of bacteria and or their by-products, which leads to the demise of the tooth pulp. Thus, this study was planned to compare the ability of the restorative materials to seal perforated PFM specimens. MATERIALS AND METHODS. The study evaluates the ability of amalgam, composite or compomer restorative materials to close perforated PFM specimen's in-vitro. Ninety PFM specimens were constructed using Ni-Cr alloys and feldspathic porcelain, and then they were divided into 3 groups: amalgam (A), composite + Exite adhesive bond (B) and compomer + Syntac adhesive bond (C). All the PFM samples were embedded in an acrylic block to provide complete sealing of the hole from the bottom side. After the aging period, each group was further divided into 3 equal subgroups according to the thermocycling period (one week for 70 cycles, one month for 300 cycles and three months for 900 cycles). Each subgroup was put into containers containing dye (Pelikan INK), one maintained at $5^{\circ}C$ and the other at $55^{\circ}C$, each cycle for 30 sec time. The data obtained was analyzed by SPSS, 2006 using one way ANOVA test and student t-test and significant difference level at (P<.01). RESULTS. The depth of dye penetration was measured at the interfaces of PFM and filling materials using Co-ordinate Vernier Microscope. The lowest levels of the dye penetration for the three groups, as well as subgroups were during the first week. The values of dye leakage had significantly increased by time intervals in subgroups A and C. CONCLUSION. It was seen that amalgam showed higher leakage than composite while compomer showed the lowest level of leakage.

• 소성∙가공
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• 제19권7호
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• pp.423-428
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• 2010

Carbon nanotubes(CNTs) are expected to be ideal reinforcements of metal matrix composite materials used in aircraft and sports industries due to their high strength and low density. In this study, a high pressure torsion(HPT) process at an elevated temperature(473K) was employed to achieve both powder consolidation and grain refinement of aluminummatrix nanocomposites reinforced by 5vol% CNTs. CNT/Al nanocomposite powders were fabricated using a novel molecular-level mixing process to enhance the interface bonding between the CNTs and metal matrix before the HPT process. The HPT processed disks were composed of mostly equilibrium grain boundaries. The CNT-reinforced ultrafine grained microstructural features resulted in high strength and good ductility.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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• pp.1091-1092
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• 2006

Silicon nitride - silicon carbide composite was developed by using an abrasive SiC powders as a raw material. The composites were prepared by mixing abrasive SiC powder with silicon, pressing and sintering at $1400^{\circ}C$ under nitrogen atmosphere in atmosphere controlled vacuum furnace. The proportion of silicon in the initial mixtures varied from 20 to 50 wt%. After sintering, crystalline phases and microstructure were characterized. All composites consisted of ${\alpha}-Si_3N_4$ and ${\beta}-Si_3N_4$ as the bonding phases in SiC matrix. Their physical and mechanical properties were also determined. It was found that the density of the obtained composites increased with an increase in the $Si_3N_4$ content formed in the reaction.

• 대한소아치과학회지
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• 제24권4호
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• pp.805-812
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• 1997

Despite dentistry's attempts to improve the dental health of the public and to minimize the effects of caries, many children still present with extensive destruction of primary anterior teeth. One of dentistry's most challenging tasks is to repair these teeth with restoration which are durable, retentive, and esthetic. Esthetic restoration can often be achieved with polycarbonate crowns, strip crowns, conventional S-S crowns, open-faced S-S crowns, commercially veneered S-S crowns. But, all of these have limitation. Advances in restorative materials and metal-bonding procedures have made possible new restorative techniques that combine the advantages of S-S crowns with the cosmetics of composite restoration methods. The described technique of bonding composite to trimmed and fitted S-S crowns offers many advantages over other techniques currently used to restore primary anterior teeth. 1. If S-S crowns are accurate trimmed and contoured, good retention of crowns is achieved. 2. The patient time required is similar to that of conventional S-S crowns. 3. Good esthetics and high bond strengths are achieved. 4. It is possible to use this veneering technique intraorally on crowns that have fractured veneers.

• Restorative Dentistry and Endodontics
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• 제29권2호
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• pp.170-176
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• 2004

목적 : 본 연구에서는 '전단접착강도 시험법에서 cohesive failure를 줄일 수 있는 것으로 소개된 metal iris를 사용하면, 실제의 1급 와동에서보다 복합 레진과 와동벽의 결합이 없어서 C-factol 적게 작용하고 계면에 발생하는 수축 응력이 감소됨으로써, 임상에서보다 높은 결합력 값이 보고될 것이다.'라는 가설을 검증하기 위하여 dentin ilia를 사용하여 전단접착강도를 측정하였다. 방법 : 64개의 대구치를 4군으로 구분하여 metal iris와 dentin iris군으로 구분하고, 그 각각을 ONE-STEP과 ALL-BOND 2의 두 군으로 나누었다. bonding agent를 적용하고. iris를 고정한 후, 복합 레진을 충전하여 시편을 완성하였다. 이 때 dentin iris의 경우 내면에도 bonding agent를 적용하여 와동벽과의 결합이 발생하게 하였다. 전단접착강도는 24시간 후 측정하였고, 파절의 양상은 주사전자현미경과 입체광학현미경을 이용하여 결정하였다. 결과 : 전단접착강도 측정법에서 iris 법을 이용함으로써 cohesive failure를 줄일 수 있다. 전단접착강도 측정법은 adhesive 두께가 얇은 경우에 와동벽의 영향을 받는다.

• 대한치과보철학회지
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• 제42권6호
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• pp.654-663
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• 2004

Statement of problem. According to the fracture pattern in several reports, fractures most frequently occur in the interface between the ceromer and the substructure. Purpose. The aim of this in vitro study was to compare the macro shear bond strength and microshear bond strength of a ceromer bonded to a fiber reinforced composite (FRC) as well as metal alloys. Material and methods. Ten of the following substructures, type II gold alloy, Co-Cr alloy, Ni-Cr alloy, and FRC (Vectris) substructures with a 12 mm in diameter, were imbedded in acrylic resin and ground with 400, and 1, 000-grit sandpaper. The metal primer and wetting agent were applied to the sandblasted bonding area of the metal specimens and the FRC specimens, respectively. The ceromer was placed onto a 6 mm diameter and 3 mm height mold in the macro-shear test and 1 mm diameter and 2 mm height mold in the micro-shear test, and then polymerized. The macro- and micro-shear bond strength were measured using a universal testing machine and a micro-shear tester, respectively. The macro- and micro-shear strength were analyzed with ANOVA and a post-hoc Scheffe adjustment ($\alpha$ = .05). The fracture surfaces of the crowns were then examined by scanning electron microscopy to determine the mode of failure. Chi-square test was used to identify the differences in the failure mode. Results. The macro-shear strength and the micro-shear strength differed significantly with the types of substructure (P<.001). Although the ceromer/FRC group showed the highest macroand micro-shear strength, the micro-shear strength was not significantly different from that of the base metal alloy groups. The base metal alloy substructure groups showed the lowest mean macro-shear strength. However, the gold alloy substructure group exhibited the least micro-shear strength. The micro-shear strength was higher than the macro-shear strength excluding the gold alloy substructure group. Adhesive failure was most frequent type of fracture in the ceromer specimens bonded to the gold alloys. Cohesive failure at the ceromer layer was more common in the base metals and FRC substructures. Conclusion. The Vectris substructure had higher shear strength than the other substructures. Although the shear strength of the ceromer bonded to the base metals was lower than that of the gold alloy, the micro-shear strength of the base metals were superior to that of the gold alloy.

• 마이크로전자및패키징학회지
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• 제20권4호
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• pp.13-16
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• 2013

양극산화(anodization)공정으로 제작된 규칙성 나노구조의 다공성 산화알루미늄(Aluminum Anodic Oxide, AAO)는 공정이 적용된 LED 모듈은 비교적 쉽고 경제적이므로 최근 LED용 방열소재로 응용하기 위하여 다양하게 연구가 진행되고 있다. 일반적으로 LED 모듈은 알루미늄/폴리머/구리 회로층으로 구성되며 절연체 역할을 하는 폴리머는 히트스프레더로 구성되어있다. 그러나 열전도도가 낮은 폴리머로 인하여 LED부품의 열 방출이 원활하지 못하므로 LED의 수명단축 및 오작동에 영향을 미친다. 따라서, 본 연구에서는 폴리머 대신 상대적으로 열전도도가 우수한 AAO를 양극산화 공정으로 제작하여 히트스프레더(heat spread)로 사용하였다. 이때, AAO와 금속인 구리 회로층간의 접착력을 향상시키기 위하여 스퍼터링 DBC(direct bonding copper)법으로 시드층(seed layer)을 형성한 뒤 최종적으로 전해도금공정으로 구리회로층을 형성하였다. 본 연구에서는 양극 산화공정으로 AAO와 금속간의 접착강도를 개선하여 1.18~1.45 kgf/cm와 같은 우수한 peel strength 값을 얻었다.

• 대한치과보철학회지
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• 제29권2호
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• pp.85-101
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• 1991

The purpose of this study was to determine the optimum range of laser energy density to the enamel surface of permanent incisors when they are irradiated with the pulsed Nd : YAG laser, Laser impacts on each experimental group were made at energy density of $20\sim50J/cm^2$ by 20 pulses of the pulse width 1.2 msec. The author investigated the enamel surface with the sunning electron microscope(SEM) and the surface roughness tester, and measured the shear bond strength between electrolytically etched Ni-Cr-Be alloy casting and composite resin. The obtained results were as follows: 1. The surface roughness of enamel after laser irradiation showed the significant difference level from the energy density $40J/cm^2(P<0.05)$. 2. The mean shear bond strength of etched-metal resin-bonded specimens were $154.23{\pm}33.30kg/cm^2$ at unlased enamel surface and $195.72{\pm}29.56kg/cm^2$ at lased energy density $30J/cm^2$, and showed a significant difference(P<0.05). 8. SEM photographs showed the irregular microcracks and the structural changes of lased enamel surface. 4. SEM photographs of the fracture surface after testing the shear bond strength showed the aspect of interfacial fracture between bonding agent and composite resin at the metal sides.

• Composites Research
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• 제30권3호
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• pp.209-214
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• 2017

본 연구에서는 용융가압함침 공정을 통해 고체적율의 TiC 입자가 균일 분산된 SKD11 금속복합재료를 제조하고, 미제조직, 기계적 특성 및 내마모 특성에 대해 분석하였다. 약 60 vol%의 TiC가 균일하게 분산된 TiC-SKD11 복합재료를 제조함으로써 SKD11 대비 약 24% 경량화에 성공하였고 경도 및 압축항복강도는 증가하였다. 내마모 시험 결과 복합소재의 우수한 내마모 특성을 확인하였으며, 이는 높은 경도를 가지는 TiC 입자가 SKD11 기지와 강한 계면 결합력을 가지면서 높은 체적율로 존재함으로 인한 분산강화 효과와 TiC에 의한 SKD11의 산화 억제가 원인으로 판단된다.