• 제목/요약/키워드: complex separation

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금(金) 광산(鑛山) 폐광미(廢鑛尾)로부터 회수(回收)된 금속광물(金屬鑛物) 부산물(副産物) 중의 금속성분(金屬成分) 분리(分離), 제거연구(除去硏究) (Removal and Separation of Metallic Constituents from the By-product Recovered from Gold Mine Tailings)

  • 윤기병
    • 자원리싸이클링
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    • 제19권3호
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    • pp.9-15
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    • 2010
  • 국내 금 광산 폐광미로부터 비금속광물을 분리, 선별하는 공정 중에서 황비철광, 방연광 등이 혼합된 금속광물이 부산물로 회수되며, 이 부산물에는 Au, Pb, As, Fe 성분들이 매우 높게 농축되어진다. 이 부산물로부터 Au의 효율적 회수를 위해서는 우선 금 제련공정에 해로운 거동을 나타내는 금속성분들을 분리, 제거할 필요가 있다. 본 연구에서는 금 광산 폐광미로부터 회수된 금속광물 부산물로부터 Pb, As, Fe등을 제거, 분리하는 실험을 수행하였다. Pb는 알칼리 가압산화침출에 의하여 $120^{\circ}C$, 2M NaOH, 100psi $Po_2$, 250r.p.m., 4 wt.% 고체, 30 min. 침출조건에서 3% 이하 까지 제거시킬 수 있었으며, 침출잔사를 배소 및 자력선별처리하여 As 0.2% 이하, Fe 3% 이하 및 8,000 ppm 이상의 Au 함량을 갖는 비자성산물을 얻을 수 있었다.

Prediction of nonlinear characteristics of soil-pile system under vertical vibration

  • Biswas, Sanjit;Manna, Bappaditya;Choudhary, Shiva S.
    • Geomechanics and Engineering
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    • 제5권3호
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    • pp.223-240
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    • 2013
  • In the present study an attempt was made to predict the complex nonlinear parameters of the soil-pile system subjected to the vertical vibration of rotating machines. A three dimensional (3D) finite element (FE) model was developed to predict the nonlinear dynamic response of full-scale pile foundation in a layered soil medium using ABAQUS/CAE. The frequency amplitude responses for different eccentric moments obtained from the FE analysis were compared with the vertical vibration test results of the full-scale single pile. It was found that the predicted resonant frequency and amplitude of pile obtained from 3D FE analysis were within a reasonable range of the vertical vibration test results. The variation of the soil-pile separation lengths were determined using FE analysis for different eccentric moments. The Novak's continuum approach was also used to predict the nonlinear behaviour of soil-pile system. The continuum approach was found to be useful for the prediction of the nonlinear frequency-amplitude response of full-scale pile after introducing the proper boundary zone parameters and soil-pile separation lengths.

Separation of Text and Non-text in Document Layout Analysis using a Recursive Filter

  • Tran, Tuan-Anh;Na, In-Seop;Kim, Soo-Hyung
    • KSII Transactions on Internet and Information Systems (TIIS)
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    • 제9권10호
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    • pp.4072-4091
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    • 2015
  • A separation of text and non-text elements plays an important role in document layout analysis. A number of approaches have been proposed but the quality of separation result is still limited due to the complex of the document layout. In this paper, we present an efficient method for the classification of text and non-text components in document image. It is the combination of whitespace analysis with multi-layer homogeneous regions which called recursive filter. Firstly, the input binary document is analyzed by connected components analysis and whitespace extraction. Secondly, a heuristic filter is applied to identify non-text components. After that, using statistical method, we implement the recursive filter on multi-layer homogeneous regions to identify all text and non-text elements of the binary image. Finally, all regions will be reshaped and remove noise to get the text document and non-text document. Experimental results on the ICDAR2009 page segmentation competition dataset and other datasets prove the effectiveness and superiority of proposed method.

칩 기반 미세관 HPLC를 이용한 단백체 분석 (Chip-based microcapillary HPLC for proteomic analysis)

  • 김보라;박종문;이후근
    • 분석과학
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    • 제24권6호
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    • pp.407-413
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    • 2011
  • 지난 10년간 고해상도 탠덤질량분석기에 사용되는 다양한 미세관 HPLC들이 개발되어 단백체분석연구에 사용되어져 왔다. 질량분석에 앞선 분리과정은 샘플 중의 불순물을 제거하며, 분석물을 좁은 용리 피크 내에 농축함으로써 이어지는 질량분석의 민감도를 향상시킬 수 있다. 본 총설에서는 복잡한 단백체 분석에 사용되는 미세유체 칩을 기반으로 하는 고성능 분리 기술들의 최근 개발 동향을 고찰하였다.

공동주택단지내 상업시설의 변화요인에 관한 연구 (Research about commerce equipment change factor in apartment house complex)

  • 최용준;김한수
    • 한국주거학회논문집
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    • 제12권4호
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    • pp.105-113
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    • 2001
  • This research indicates to controversial point that store equipments were not applying correct development factor in the each apartment house by that change rate by scale and uniformity of form and inefficiency, effect of discount store is increasing in apartment house and progressed research. The result are as follows; First, interior main point of store of that influence greatly to change rate number of store be. Second, being lot area in jar in outside factor of store. Third, discount store separation appeared by leading person who influence greatly to change rate in middle who is contiguity market singleness residential quarter and contiguity existence of commercial district and nonexistence and discount store separation of only outside right near at hand. Construction of commerce equipment may have to consist in practical apartment house after examine various kinds factor such as store indoor, store outside and only outside while plan practical use of systematic and efficient commerce equipment focusing more in efficient utilization of commerce institution that consist after plan that is not planed commerce equipment focusing in development in plan of commerce equipment in apartment house hereafter accordingly.

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질산은을 산소 캐리어로 하는 CA막의 제조 (Preparation of Cellulose Acetate Containing Silver Nitrate as Oxygen Carrier)

  • 안필성;이우태
    • 한국산업융합학회 논문집
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    • 제2권2호
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    • pp.83-90
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    • 1999
  • A cellulose acetate membrane containing silver nitrate was prepared by gelatinizing in water at $2^{\circ}C$ after evaporating solvent from the casting solution on a glass plate. Permeation experiments for oxygen and nitrogen were conducted in the ranges of temperature, $5-40^{\circ}C$ and pressure difference, $1-5kg/cm^2$ in order to investigate the effects of temperature and pressure difference on permeation characteristics of the membrane. When the evaporation time was increased, the permeability of oxygen decreased but the separation factor of oxygen against nitrogen increased since a more dense layer was formed on the membrane surface. When the silver nitrate was added, the permeation flux was doubled and the separation factor was improved from 3.0 to 3.3. This implies that silver nitrate acts as an oxygen carrier in the membrane.

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Morphology of Sub-Microscale Atmospheric Aerosols composed of Two Liquid Phases According to the Loading Ratio of Organics/Water

  • Yoo, Kee-Youn
    • Korean Chemical Engineering Research
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    • 제55권1호
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    • pp.130-134
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    • 2017
  • Organic aerosols dispersed in the atmosphere likely undergo phase separation. Such internally mixed particles are often described as comprising an organic phase and an aqueous phase separately. We studied the morphology of two liquid separated aerosols in the sub-microscale by using a simple thermodynamic model with Russian doll geometry. The morphology of particles can be easily predicted from the simple criteria on the surface tension and two algebraic equations (the volume constraint and Young equation). This result may give the potential explanation about the complex morphology of the organic airborne particles.

평판에 충돌하는 음속/초음속 제트유동에 관한 연구 (Study on Sonic/Supersonic Impinging Jets on a Flat Pate)

  • 김희동;이호준;서태원;금기헌
    • 한국추진공학회:학술대회논문집
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    • 한국추진공학회 1998년도 제10회 학술강연회논문집
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    • pp.15-15
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    • 1998
  • The problem of the impingement of a sonic or a supersonic jet on a flat surface has not only wide applications but has also interesting and very complex flow phenomena. The main applications of this impinging jet include prediction of solid surface erosion, design of launcher systems, stage separation of multi-stage rocket system, V/STOL operations, thermal spray system, and manufacturing technologies of materials. Much have been learned about the supersonic impinging jet flow field but many fundamental questions have not been answered satisfactorily. The problem encompasses many facets of fluid dynamics which, in combination, present the compressibility effect and the viscous-inviscid interaction, coupled with flow separation and reattachment. What is more, there are many flow parameters that have on the impinging jet flow field, for example, Mach number, Reynolds number, pressure ratio, distance between the nozzle exit and flat plate, jet shock structure, nozzle diameter and etc. Thus the existing data on the supersonic impinging jet flow present considerable disagreement in which quantitative comparison between one result and another is often impossible.

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Optical Resolution of Dansyl Amino Acids with Addition of Benzyl-L-Hydroxyproline Copper(II) Chelate by High Performance Liquid Chromatography

  • Sun Haing Lee;Tae Sub Oh;Sang Hyun Bak
    • Bulletin of the Korean Chemical Society
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    • 제10권6호
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    • pp.491-495
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    • 1989
  • Resolution of enantiomers of DNS-amino acids has been achieved by a reversed phase liquid chromatography with an addition of a copper(Ⅱ) complex of N-benzyl-L-hydroxyproline to the mobile phase. N-Benzyl-L-hydroxyproline was prepared and used as a chiral ligand of copper(Ⅱ) chelate for the optical resolution. The pH and the concentration of copper(Ⅱ) chelate, organic solvent, and buffer agent in the mobile phase all affect the optical resolutions of dansyl amino acids. The elution orders between D and L-DNS-amino acids were different depending on the structure of the side chain of the amino acids. The retention mechanism for the chiral separation of the dansyl amino acids can be illustrated by the equilibrium of ligand exchange and by hydrophobic interaction with $C_{18}$ stationary phase. The chiral separation can be illustrated with cis and trans effect of the ligand exchange reaction.

FT-Raman Studies on Ionic Interactions in ${\pi}$-Complexes of Poly(hexamethylenevinylene) with Silver Salts

  • Kim Jong-Hak;Min Byoung-Ryul;Won Jong-Ok;Kang Yong-Soo
    • Macromolecular Research
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    • 제14권2호
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    • pp.199-204
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    • 2006
  • Remarkably high and stable separation performance for olefin/paraffin mixtures was previously reported by facilitated olefin transport through ${\pi}$-complex membranes consisting of silver ions dissolved in poly(hexamethylenevinylene) (PHMV). In this study, the ${\pi}$-complex formation of $AgBF_4,\;AgClO_4\;and\;AgCF_{3}SO_3$ with PHMV and their ionic interactions were investigated. FT-Raman spectroscopy showed that the C=C stretching bands of PHMV shifted to a lower frequency upon incorporation of silver salt, but the degree of peak shift depended on the counter-anions of salt due to different complexation strengths. The symmetric stretching modes of anions indicated the presence of only free ions up to [C=C]:[Ag]=1:1, demonstrating the unusually high solubility of silver salt in PHMV. Above the solubility limit, the ion pairs and higher-order ionic aggregates started to form. The coordination number of silver ion for C=C of PHMV was in the order $AgBF_4$ > $AgClO_4$ > $AgCF_{3}SO_3$, but became similar at [C=C]:[Ag]=1:1. The different coordination number was interpreted in terms of the different transient crosslinks of silver cations in the complex, which may be related to both the interaction strength of the polymer/silver ion and the bulkiness of the counteranion.