• 제목/요약/키워드: complex separation

검색결과 451건 처리시간 0.033초

A Study on the Separation of Cerium from Rare Earth Precipitates Recovered from Waste NiMH Battery (폐니켈수소전지에서 회수된 희토류복합 침전분말로부터 세륨 회수에 대한 연구)

  • Kim, Boram;Ahn, Nak-Kyoon;Lee, Sang-Woo;Kim, Dae-Weon
    • Resources Recycling
    • /
    • 제28권6호
    • /
    • pp.18-25
    • /
    • 2019
  • In order to recover the cerium contained in the spent nickel metal hydride batteries (NiMH battery), the recovered rare earth complex precipitates from NIMH were converted into rare earth hydroxides through ion exchange reaction to react with NaOH aqueous solution at a reaction temperature of 70 ℃, for 4 hours. Rare earth hydroxides were oxidized by injecting air at 80 ℃ for 4 hours to oxidize Ce3+ to Ce4+. The oxidation rate of cerium was confirmed to be about 25 % through XPS, and the oxidized powder was separated from the rest of the rare earth using the difference in solubility in dilute sulfuric acid. The finally recovered powder has a crystal phase of cerium hydroxide (Ce(OH)4). The cerium purity of the final product was about 94.6 %, and the recovery rate was 97.3 %.

Transition of Marker Enzymes of Rat Hepatocyte Organelles in Culture (배양중 흰쥐 간세포의 새포소기관 표지효소의 변천)

  • Song, In-Hwan;Kim, Joo-Yung;Sung, Eon-Ki;Lee, Yung-Chang
    • Journal of Yeungnam Medical Science
    • /
    • 제6권2호
    • /
    • pp.133-140
    • /
    • 1989
  • To investigate recovery, growth, and activity of hepatocyte in primary culture after cell separation, the authors followed up the marker enzyme activities of golgi complex, mitochondria and biologic membrane. Thiamine pyrophosphatase, the marker enzyme of golgi complex, activity approached the level of long term culture at 4th day. Succinate dehydrogenase, the marker enzyme of mitochondria, activity decreased with time, then it maintained constant level after 4th day. Alkaline phosphatase, the marker enzyme of biological membrane, activity increased from 3rd day, and after 5th day it showed strong reaction. These data suggested that hepatocytes were stabilized and recovered normal activity 4 day after cell separation, but the main secretory function was speculated to be reduced in culture.

  • PDF

The assessment of the Spatial Variation of the Wind Field using the Meso-velocity Scale and its Contributing Factors (중간 속도 규모를 이용한 바람장의 균질성 평가 및 영향요소 분석)

  • Lee, Seong-Eun;Shin, Sun-Hee;Ha, Kyung-Ja
    • Atmosphere
    • /
    • 제20권3호
    • /
    • pp.343-353
    • /
    • 2010
  • A regional wind network with complex surface conditions must be designed with sufficient space and time resolution to resolve the local circulations. In this study, the spatial variations of the wind field observed in the Seoul and Jeju regional networks were evaluated in terms of annual, seasons, and months to assess the spatial homogeneity of wind fields within the regional networks. The coherency of the wind field as a function of separation distance between stations indicated that significant coherency was sometimes not captured by the network, as inferred by low correlations between adjacent stations. A meso-velocity scale was defined in terms of the spatial variability of the wind within the network. This problem is predictably most significant with weak winds, dull prevailing wind, clear skies and significant topography. The relatively small correlations between stations imply that the wind at a given point cannot be estimated by interpolating winds from the nearest stations. For the Seoul and Jeju regional network, the meso-velocity scale has typically a same order of magnitude as the speed of the network averaged wind, revealing the large spatial variability of the Jeju network station imply topography and weather. Significant scatter in the relationship between spatial variability of the wind field and the wind speed is thought to be related to thermally-generated flows. The magnitude of the mesovelocity scale was significantly different along separation distance between stations, wind speed, intensity of prevailing wind, clear and cloudy conditions, topography. Resultant wind vectors indicate much different flow patterns along condition of contributing factors. As a result, the careful considerations on contributing factors such as prevailing wind in season, weather, and complex surface conditions with topography and land/sea contrast are required to assess the spatial variations of wind field on a regional network. The results in the spatial variation from the mesovelocity scale are useful to represent the characteristics of regional wind speed including lower surface conditions over the grid scale of large scale atmospheric model.

Thermal Decomposition of Arsenopyrite by Microwave Heating and the Effect of Removal Arsenic with Wet-magnetic separation (마이크로웨이브 가열에 의한 황비철석의 열분해와 습식-자력선별에 의한 비소 제거 효과)

  • On, Hyun-Sung;Kim, Hyun-Soo;Myung, Eun-Ji;Lim, Dae-Hack;Park, Cheon-Young
    • Journal of the Mineralogical Society of Korea
    • /
    • 제30권3호
    • /
    • pp.103-112
    • /
    • 2017
  • In order to transform arsenopyrite into pyrrhotite and to decrease As content by less than 2,000 mg/kg, pulp sample and non-magnetic pulp sample were heated in a microwave oven at different heating times and were separated through wet-magnetic separation. As the microwave heating time increased, the phase of pyrrhotite was extended to become arsenopyrite entirely. The melting pores and micro-cracks occurred on the pyrrhotite due to hot spot phenomenon with microwave heating. The heated raw pulp sample (As content : 19,970.13 mg/kg) and non-magnetic pulp sample (As content : 19,970.13 mg/kg) which were heated in a microwave oven for 10 minutes were separated through wet-magnetic separation and magnetic fraction containing less than 2,000 mg/kg of As content was recovered only from the heated sample of magnetic separation. It was discovered that for the sulfide complex ore with As penalty imposed on, if microwave heating and wet-magnetic separation are effectively utilized, magnetic fraction. We expect to be able to obtain ore minerals with an arsenic content below the penalty charge.

A Study on the POE (Post Occupancy Evaluation) according to the Residential Environment of Mixed-use Apartment Complexes In Seoul

  • Ha, Man Joon
    • International Journal of High-Rise Buildings
    • /
    • 제9권2호
    • /
    • pp.197-212
    • /
    • 2020
  • In this study, POE(Post Occupancy Evaluation) evaluation indexes were selected into six categories through the consideration of theories and prior research. Therefore, qualitative supply can be achieved through POE according to the aspect of residential environment after the quantitative supply of mixed-use apartment complex by the population concentration in Seoul due to industrialization and urbanization. As the evaluation elements, detailed survey contents were selected for livability, convenience, comfort, safety, economy, and sociality. Based on the survey contents, six elements were evaluated and analyzed using Data coding and Likert scale after surveying 12 complexes (Urban areas and non-urban areas) in Seoul. As a result of the study, six categories selected as the POE showed that importance of quality of life and safety was developed in high recognition according to high satisfaction with convenience and safety. Sociality showed the lowest satisfaction in the following order : livability, comfort, economy and sociality. Residents' sense of community, interaction with neighborhood, etc., showed low satisfaction, and it seems that it is necessary to improve and supplement the system for the development of mixed-use apartment complex in the future. The detailed characteristics of livability showed high satisfaction of the living room, the front door and the main room which are main uses of housing, and low satisfaction in storage size. The analysis of convenience is that convenient public transportation was the highest, and educational environment and additional facilities were the lowest, showing the advantages and disadvantages of location characteristics. As a result of the analysis of comfort, satisfaction with the landscape area was low and it seems that green space is needed for the development of mixed-use apartment complex in the future. Lastly, regarding the safety, the satisfaction of the access control, the location of security office, etc. were high, however separation of circulation was low. Therefore, it is necessary to clearly separate the circulation between the residence and other facilities in the mixed-use apartment complex.

A Study on 8-Directional Complex Wavelet Transform for Efficient Image Processing (효율적인 영상처리를 위한 8방향 컴플렉스 웨이브렛 변환에 관한 연구)

  • Shin, Seong;Moon, Sung Ryong
    • Journal of the Institute of Electronics and Information Engineers
    • /
    • 제50권3호
    • /
    • pp.129-138
    • /
    • 2013
  • This paper is a study on Dual Tree Complex Wavelet Transform, which improved directional information for efficient image processing. Dual Tree Complex Wavelet Transform satisfies characteristics of shift invariance, and includes 6 directional information, which is more than previous Discrete Wavelet Transform. However, in images of buildings, there are many horizontal and vertical edge components. Therefore, all the high-frequency components of image are not expressed by 6 directional information subbands. This paper proposes 8-directional Complex Wavelet Transform with excellent high-frequency separation features by creating horizontal vertical($0^{\circ}$, $90^{\circ}$) subband besides 6 directional information subband of previous Dual Tree Complex Wavelet Transform. The proposed method can create and combine various directional information subbands according to features of image. Performance is evaluated by applying the method to noise removal.

Development of Liposome Immunoassay for Salmonella spp. using Immunomagnetic Separation and Immunoliposome

  • Shin, Jung-Hee;Kim, Myung-Hee
    • Journal of Microbiology and Biotechnology
    • /
    • 제18권10호
    • /
    • pp.1689-1694
    • /
    • 2008
  • The ability to detect Salmonella spp. is essential in the prevention of foodborne illness. This study examined a Salmonella spp. detection method involving the application of immunomagnetic separation and immunoliposomes (IMS/IL) encapsulating sulforhodamine B (SRB), a fluorescent dye. A quantitative assay was conducted by measuring the fluorescence intensity of SRB that was produced from an immunomagnetic bead-Salmonella spp.-immunoliposome complex. The results indicated detection limits of $2.7{\times}10^{5}$ and $5.2{\times}10^{3}$ CFU/ml for Salmonella enterica subsp. enterica serovar Enteritidis (S. Enteritidis) and Salmonella enterka subsp. enterka serovar Typhimurium (S. Typhimurium), respectivley. The signal/noise ratio was improved by using 4% skim milk as a wash solution rather than 2% BSA. In addition, higher fluorescence intensity was obtained by increasing the liposome size. Compared with the conventional plating method, which takes 3-4 days for the isolation and identification of Salmonella spp., the total assay time of to h only including 6 h of culture enrichment was necessary for the Salmonella detection by IMS/IL. These results indicate that the IMS/ IL has great potential as an alternative rapid method for Salmonella detection.

A Study of an Airfoil for Optimal Aerodynamic Performance of Flapping Motion (Flapping운동의 최적공력성능을 위한 익형 연구)

  • Lee J. S.;Kim C.;Rho O. H.
    • Journal of computational fluids engineering
    • /
    • 제8권2호
    • /
    • pp.24-32
    • /
    • 2003
  • In this work, we propose a new idea of flapping airfoil design for optimal aerodynamic performance from detailed computational investigations of flow physics. Generally, flapping motion which is combined with pitching and plunging motion of airfoil, leads to complex flow features such as leading edge separation and vortex street. As it is well known, the mechanism of thrust generation of flapping airfoil is based on inverse Karman-vortex street. This vortex street induces jet-like flow field at the rear region of trailing edge and then generates thrust. The leading edge separation vortex can also play an important role with its aerodynamic performances. The flapping airfoil introduces an alternative propulsive way instead of the current inefficient propulsive system such as a propeller in the low Reynolds number flow. Thrust coefficient and propulsive efficiency are the two major parameters in the design of flapping airfoil as propulsive system. Through numerous computations, we found the specific physical flow phenomenon which governed the aerodynamic characteristics in flapping airfoil. Based on this physical insight, we could come up with a new kind of airfoil of tadpole-shaped and more enhanced aerodynamic performance.

Effects of Nickel Supports on Hydrogen Permeability of Vanadium based Membrane (니켈 지지체를 이용한 바나듐기 분리막의 수소 투과특성)

  • Cho, Kyoungwon;Choi, Jaeha;Jung, Seok;Kim, Raymundk.I.;Hong, Taewhan;Ahn, Joongwoo
    • Journal of Hydrogen and New Energy
    • /
    • 제24권3호
    • /
    • pp.200-205
    • /
    • 2013
  • The separation of hydrogen depends on porosity, diffusivity and solubility in permeation membrane. Dense membrane is always showing a solution diffusion mechanism but porous membrane is not showing. Therefore, porous membrane has a good hydrogen flux due to pore is carried out transferred media. This mechanism is named as the Knudsen diffusion. Hydrogen molecules or hydrogen atoms are diffused along pore that is a mean free path. In this study, complex layer hydrogen permeation membrane was fabricated by hot press process. And then, it was evaluated and calculated to relationship between hydrogen permeability and membrane porosity.

A Correlative Approach for Identifying Complex Phases by Electron Backscatter Diffraction and Transmission Electron Microscopy

  • Na, Seon-Hyeong;Seol, Jae-Bok;Jafari, Majid;Park, Chan-Gyung
    • Applied Microscopy
    • /
    • 제47권1호
    • /
    • pp.43-49
    • /
    • 2017
  • A new method was introduced to distinguish the ferrite, bainite and martensite in transformation induced plasticity (TRIP) steel by using electron backscatter diffraction (EBSD) and transmission electron microscopy (TEM). EBSD is a very powerful microstructure analysis technique at the length scales ranging from tens of nanometers to millimeters. However, iron BCC phases such as ferrite, bainite and martensite cannot be easily distinguished by EBSD due to their similar surface morphology and crystallographic structure. Among the various EBSD-based methodology, image quality (IQ) values, which present the perfection of a crystal lattice, was used to distinguish the iron BCC phases. IQ values are very useful tools to discern the iron BCC phases because of their different density of crystal defect and lattice distortion. However, there are still remaining problems that make the separation of bainite and martensite difficult. For instance, these phases have very similar IQ values in many cases, especially in deformed region; therefore, even though the IQ value was used, it has been difficult to distinguish the bainite and martensite. For more precise separation of bainite and martensite, IQ threshold values were determined by a correlative TEM analysis. By determining the threshold values, iron BCC phases were successfully separated.