• Title/Summary/Keyword: compaction density

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Fabrication of Fe-Cr-Al Porous Metal with Sintering Temperature and Times (소결 온도와 유지 시간에 따른 Fe-Cr-Al 다공성 금속의 제조)

  • Koo, Bon-Uk;Lee, Su-In;Park, Dahee;Yun, Jung-Yeul;Kim, Byoung-Kee
    • Journal of Powder Materials
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    • v.22 no.2
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    • pp.100-104
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    • 2015
  • The porous metals are known as relatively excellent characteristic such as large surface area, light, lower heat capacity, high toughness and permeability. The Fe-Cr-Al alloys have high corrosion resistance, heat resistance and chemical stability for high temperature applications. And then many researches are developed the Fe-Cr-Al porous metals for exhaust gas filter, hydrogen reformer catalyst support and chemical filter. In this study, the Fe-Cr-Al porous metals are developed with Fe-22Cr-6Al(wt) powder using powder compaction method. The mean size of Fe-22Cr-6Al(wt) powders is about $42.69{\mu}m$. In order to control pore size and porosity, Fe-Cr-Al powders are sintered at $1200{\sim}1450^{\circ}C$ and different sintering maintenance as 1~4 hours. The powders are pressed on disk shapes of 3 mm thickness using uniaxial press machine and sintered in high vacuum condition. The pore properties are evaluated using capillary flow porometer. As sintering temperature increased, relative density is increased from 73% to 96% and porosity, pore size are decreased from 27 to 3.3%, from 3.1 to $1.8{\mu}m$ respectively. When the sintering time is increased, the relative density is also increased from 76.5% to 84.7% and porosity, pore size are decreased from 23.5% to 15.3%, from 2.7 to $2.08{\mu}m$ respectively.

Effect of Coarse mateflal on the mechanical properties of Soil (조립재가 흙의 역학적 성질에 미치는 영향)

  • 윤충섭;김호일
    • Magazine of the Korean Society of Agricultural Engineers
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    • v.31 no.3
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    • pp.57-69
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    • 1989
  • The study was carried out for the strength parameter of coarse grained Soil and slope stability analysis of earth dam. The test samples were taken fifteen kinds of soil from cohesive soil to coarse gravel. The degree of compaction of test samples for shear test and permeability test was chosen 95 percentage of maximum dry density. The results of this study are as follows ; 1.The maximum dry density(Yd) of coarse grained soil increase in proportion to coarse particles(P) with the relation of Y d= 1.609+0.0043P. 2.The coefficients of permeability(k) decrease by the increase of fine particles(n) with the relation of k=0.0426e-0 185n. 3.The cohesions of soil decrease by the increase of coarse particles, but internal friction angles are more increased in same condition. 4.The internal friction angles(${\Phi}$) decrease in inverse proportion to void ratio(e) with the relation of ${\Phi}$ = 73.068 - 69.268e. 5.The strength parameters( Ct ${\Phi}$t) by triaxial compression test are clearly smaller than that (Cd, ${\Phi}$d) by direct shear test in fine grained soil, but the differences between both parameters are a little in coarse grained soil.The relations of both parameters are as follows; Ct = O.544Cd + 0.04 ${\Phi}$t= 1.282${\Phi}$d-2306 6.In cohesive soil, the strength parameters( Cl ${\Phi}$l) by large size shear test apparatus are similar to the strength parameters(Cs , ${\Phi}$s) by small size shear test appratus, but Cs and ${\Phi}$s values are larger than Cl and ${\Phi}$l values from 10 percentage to 20 percentage in coarse grained soil. 7.The fine grained soil is inappropriate to high dam more than 20 meters and it must be taken coarse grained soil with high internal friction angle for high dam.

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Permeability Variation With Lift Thickness of Asphalt Pavement (아스팔트 포장의 시공 포설두께에 따른 투수계수 변화특성)

  • Park, Sang Hyun;Moon, Jun Ho;Bae, Seok Il;Kim, Young Uk
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.16 no.3
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    • pp.2229-2233
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    • 2015
  • The permeability of HMA(hot mixed asphalt) is a major influencing factor for long-term performance of the pavement. Especially, the lift thickness of the pavement during construction causes a wide range of physical properties of HMA. This study investigates the correlationship between the lift thickness and the physical properties of HMA through a series of laboratory experiments. The specimens were cored from a construction site of the dense graded asphalt pavement. The cored samples have various lift thickness and the number of compaction for the study. The results of the study show that the permeability of the sample decreases with the apperant density and t/NMAS, and the air void ratio. Therefore, the commonly used construction method as a constant lift thickness regardless of conditions needs to be reconsidered.

Thermoelectric Properties of Porous Mg3Sb2 Based Compounds Fabricated by Reactive Liquid Phase Sintering (반응성 액상 소결법으로 제조한 다공성 Mg3Sb2계 화합물의 열전물성)

  • Jang, Kyung-Wook;Kim, In-Ki;Kim, Il-Ho
    • Korean Journal of Materials Research
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    • v.25 no.2
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    • pp.68-74
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    • 2015
  • The porous $Mg_3Sb_2$ based compounds with 60~70% of relative density were prepared by powder compaction at room temperature and reactive liquid phase sintering at 1023 K for 4hrs. The stoichiometric $Mg_3Sb_2$ compounds were synthesized from elemental Sb and Mg powder in the mixing range of 61~63 at% Mg. The increased scattering effect due to the micro-pores reduced the mobility of the charge carrier and the phonon, which caused the electrical conductivity and the thermal conductivity to decrease, respectively. But the scattering effect was greater for the electrical conductivity than for the thermal conductivity. Excess Mg alloyed in the $Mg_3Sb_2$ compounds decreased the electrical conductivity, but had no effect on the thermal conductivity. On the other hand, the large increase of the Seebeck coefficient was the result of a decrease in the charge carrier density due to the excess Mg. Dimensionless figure of merit of the porous $Mg_3Sb_2$ compound reached a maximum value of 0.28 at 61 at% Mg. The obtained value was similar to that of $Mg_3Sb_2$ compounds having little pores.

Bi-materials of Al-Mg Alloy Reinforced with/without SiC and Al2O3 Particles; Processing and Mechanical Properties

  • Chang, Si-Young;Cho, Han-Gyoung;Kim, Yang-Do
    • Journal of Powder Materials
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    • v.14 no.6
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    • pp.354-361
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    • 2007
  • The bi-materials with Al-Mg alloy and its composites reinforced with SiC and $Al_2O_3$ particles were prepared by conventional powder metallurgy method. The A1-5 wt%Mg and composite mixtures were compacted under $150{\sim}450\;MPa$, and then the mixtures compacted under 400 MPa were sintered at $773{\sim}1173K$ for 5h. The obtained bi-materials with Al-Mg/SiCp composite showed the higher relative density than those with $Al-Mg/Al_2O_3$ composite after compaction and sintering. Based on the results, the bi-materials compacted under 400 MPa and sintered at 873K for 5h were used for mechanical tests. In the composite side of bi-materials, the SiC particles were densely distributed compared to the $Al_2O_3$ particles. The bi-materials with Al-Mg/SiC composite showed the higher micro-hardness than those with $Al-Mg/Al_2O_3$ composite. The mechanical properties were evaluated by the compressive test. The bi-materials revealed almost the same value of 0.2% proof stress with Al-Mg alloy. Their compressive strength was lower than that of Al-Mg alloy. Moreover, impact absorbed energy of bi-materials was smaller than that of composite. However, the bi-materials with Al-Mg/SiCp composite particularly showed almost similar impact absorbed energy to $Al-Mg/Al_2O_3$ composite. From the observation of microstructure, it was deduced that the bi-materials was preferentially fractured through micro-interface between matrix and composite in the vicinity of macro-interface.

Preparation and Characteristics of $Y_2O_3-CeO_2-ZrO_2$Structural Ceramics ; I. Synthesis and Sinterability of Powder ($Y_2O_3-CeO_2-ZrO_2$ 구조세라믹스의 제조 및 특성 : I 분말의 합성 및 소결성)

  • 오혁상;이윤복;김영우;오기동;박흥채
    • Journal of the Korean Ceramic Society
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    • v.33 no.9
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    • pp.1057-1063
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    • 1996
  • Y2O3-CeO2-ZrO2 powders were prepared from water-soluble salts using a coprecipitation method. The forming process of oxide and the characteristics of the calcined powders treated in different drying conditions were investigated. The oxidation was occurred at the temperature of around 40$0^{\circ}C$ and the main crystallization of ZrO2 around $600^{\circ}C$. On calcination at $600^{\circ}C$ heating lamp-dried powders consisted of agglomerates of globular morphology with average agglomerate size of 2.27${\mu}{\textrm}{m}$ and specific surface area of 68.3m2/g and spray dried powders contained dense spheric particles with average agglomerate size of 1.35${\mu}{\textrm}{m}$ and specific surface area of 11.0m2/g which exhibited low agglomeration tendency. Removal of the water by a freeze-drying technique produced calcined powders containing flake-like secondary particle structures with wide agglomerate size distri-bution of 0.1-60${\mu}{\textrm}{m}$ and specific surface area of 24.5${\mu}{\textrm}{m}$. The 20 MPa-pressed density (36.8-41.4% T,D) of calcined powders did not nealy depend on drying methods whilst compaction ratio of calcined powders derived from freeze-drying was the highest ( 6.24) among three drying methods. On continuous heating up to 150$0^{\circ}C$ the sinterability of calcined powders derived from heating lamp-drying was superior to those derived from spray-and freeze-drying. The final sintered density of calcined powders was the highest (96% T,D at 150$0^{\circ}C$) in case of heating lamp-drying.

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Influence of Backfill Condition on Force Components of Gravity Walls During Earthquakes (지진시 배면지반 조건이 중력식 안벽의 하중성분에 미치는 영향)

  • Kim Sung-Ryul;Hwang Jae-Ik;Kim Myoung-Mo
    • Journal of the Korean Geotechnical Society
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    • v.22 no.1
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    • pp.15-23
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    • 2006
  • During earthquake, force components acting on quay walls consist of inertia force, earth pressure and water pressure. The earth pressure is largely influenced by the backfill condition such as soil density and the installation of gravel backfill. Therefore, shaking table tests were performed by using four different model sections, which were designed by varying the soil density and the backfill materials. The magnitude and the phase of force components acting on quay wall were analyzed. Test results showed that the gravel backfill and the soil compaction were effective to reduce the excess pore pressure in backfill and the magnitude and phase of backfill thrust were much influenced by the excess pore pressure in backfill. When the input acceleration was 0.10g, the average ratios of the inertia force, the front dynamic water force and the thrust to the total force were $64\%,\;21\%\;and\;16\%$, respectively. As the excess pore pressure increased, the ratio of the thrust to the total force increased.

Effect of Zinc Stearate Addition on Apparent Density, Blending and Compaction of $UO_{2}$ (Zinc stearate의 첨가가 $UO_{2}$분말의 겉보기밀도, 혼합 및 성형에 미치는 효과)

  • Na, Sang-Ho;Kim, Si-Hyeong;Lee, Yeong-U;Yang, Myeong-Seung;Son, Dong-Seong
    • Korean Journal of Materials Research
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    • v.5 no.4
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    • pp.426-432
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    • 1995
  • 윤활제인 zinc stearate의 첨가량 (0~4wt%)을 변화시켜 U$O_{2}$분말의 겉보기밀도, 성형시의 분말입자간 마찰과 입자/다이벽 마찰간의 상관관계를 조사하였다. 소량의 윤활제 첨가시에는 U$O_{2}$분말입자간 박막의 윤활제 도포층이 형성되어 겉보기밀도가 증가한 반면 다량의 윤활제를 첨가한 경우에는 U$O_{2}$ 분말입자에 두꺼운 윤활제 도포층이 형성되고 미혼합된 윤활제가 존재하여 겉보기밀도는 감소하는 경향을 보였다. 윤활제를 첨가혼합한 상태에서 다이벽 윤활도포 유무에 따라 구한 U$O_{2}$ 성형체의 성형압력/성형밀도 자료로부터 분말입자간 마찰, 입자/다이벽 마찰 그리고 성형시 lubrication/inhibition등의 상대적 중요성을 조사하였다. 입자/다이벽 마찰에 의한 압력손실은 입자간 마찰에 의한 압력손실보다 크게 나타났다. 입자/다이벽 마찰에 의한 압력손실은 다이벽 윤활제 도포에 의해 최소화될 수 있지만 상대적으로 바람직하지 않은 성형시의 inhibition이 야기되는 것으로 나타났다.

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Briquetting of Waste Silicon Carbide Obtained from Silicon Wafer Sludges (실리콘 wafer sludge로부터 얻어진 SiC의 단광화 기술)

  • Koo, Seong Mo;Yoon, Su Jong;Kim, Hye Sung
    • Journal of Powder Materials
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    • v.23 no.1
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    • pp.43-48
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    • 2016
  • Waste SiC powders obtained from silicon wafer sludge have very low density and a narrow particle size distribution of $10-20{\mu}m$. A scarce yield of C and Si is expected when SiC powders are incorporated into the Fe melt without briquetting. Here, the briquetting variables of the SiC powders are studied as a function of the sintering temperature, pressure, and type and contents of the binders to improve the yield. It is experimentally confirmed that Si and C from the sintered briquette can be incorporated effectively into the Fe melt when the waste SiC powders milled for 30 min with 20 wt.% Fe binder are sintered at $1100^{\circ}C$ upon compaction using a pressure of 250 MPa. XRF-WDS analysis shows that an yield of about 90% is obtained when the SiC briquette is kept in the Fe melt at $1650^{\circ}C$ for more than 1 h.

Microstructure and Mechanical Properties of CNT/Al Composite Fabricated by a Powder-in-Sheath Rolling Method utilizing Copper Tube as a Sheath (구리튜브를 피복재로 이용한 분말시스압연법에 의해 제조된 CNT/Al 복합재료의 미세조직 및 기계적 특성)

  • Lee, Seong-Hee
    • Journal of Powder Materials
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    • v.21 no.5
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    • pp.343-348
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    • 2014
  • A powder-in-sheath rolling (PSR) process utilizing a copper alloy tube was applied to a fabrication of a multi-walled carbon nanotube (CNT) reinforced aluminum matrix composite. A copper tube with an outer diameter of 30 mm and a wall thickness of 2 mm was used as a sheath material. A mixture of pure aluminum powders and CNTs with the volume contents of 1, 3, 5 vol% was filled in the tube by tap filling and then processed to 93.3% height reduction by a rolling mill. The relative density of the CNT/Al composite fabricated by the PSR decreased slightly with increasing of CNTs content, but showed high value more than 98%. The average hardness of the 5%CNT/Al composite increased more than 3 times, compared to that of unreinforced pure Al powder compaction. The hardness of the CNT/Al composites was some higher than that of the composites fabricated by PSR using SUS304 tube. Therefore, it is concluded that the type of tube affects largely on the mechanical properties of the CNT/Al composites in the PSR process.