• Title/Summary/Keyword: compacted materials

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Production of Fe Amorphous Powders by Gas-Atomization Process and Subsequent Spark Plasma Sintering of Fe amorphous-ductile Cu Composite Powder Produced by Ball-milling Process (II) - II. SPS Behaviors of Composite Powders and their Characteristics - (가스분무법에 의한 Fe계 비정질 분말의 제조와 볼밀링공정에 의한 연질 Cu분말과의 복합화 및 SPS 거동 (II) - II. 복합분말의 SPS와 특성 -)

  • Kim, Jin-Chun;Kim, Ji-Soon;Kim, H.J.;Kim, Jeong-Gon
    • Journal of Powder Materials
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    • v.16 no.5
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    • pp.326-335
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    • 2009
  • Fe based (Fe$_{68.2}$C$_{5.9}$Si$_{3.5}$B$_{6.7}$P$_{9.6}$Cr$_{2.1}$Mo$_{2.0}$Al$_{2.0}$) amorphous powder, which is a composition of iron blast cast slag, were produced by a gas atomization process, and sequently mixed with ductile Cu powder by a mechanical ball milling process. The Fe-based amorphous powders and the Fe-Cu composite powders were compacted by a spark plasma sintering (SPS) process. Densification of the Fe amorphous-Cu composited powders by spark plasma sintering of was occurred through a plastic deformation of the each amorphous powder and Cu phase. The SPS samples milled by AGO-2 under 500 rpm had the best homogeneity of Cu phase and showed the smallest Cu pool size. Micro-Vickers hardness of the as-SPSed specimens was changed with the milling processes.

Evaluation of Surface Water-preventing Materials on Stabilization of Contaminants in Tailings (광물찌꺼기에 함유된 오염물질의 안정화를 위한 표면 차폐재의 성능 평가)

  • Kim, Young-Kyu;Jung, Myung-Chae;Kim, Jung-Yul;Kim, Yoo-Sung;Lee, Jin-Soo;Park, Kwan-In
    • Journal of Soil and Groundwater Environment
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    • v.16 no.4
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    • pp.53-61
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    • 2011
  • This study examined evaluation on stabilization of major and trace elements in tailings by various surface water-preventing materials. Six columns were filled with tailings of the Sinlim mine, then covered with tailings only, compacted soils, clay, soil-bentonite mixture, pozzolan and bentonite mat. After injection of artificial rain water, the leachate was sampled with times (3, 6, 9 and 12 pore volume) and analysed for major (Ca, Na, Mg, K) and trace elements (As, Cd, Cu, Pb, Zn) by ICP-AES. With exception to pozzolan type, the pH values of leachate from the other types became stabilized from 5.5 to 7.5, and EC (electric conductivity) of leachate from them decreased with times. For the pozzolan type, however, the pH and EC of leachate increased with time due to its alkalinity producing system. Concentrations of most major and trace elements in leachate decreased and stabilized with time. Consequently, soil-bentonite mixed cover shows the best ability of water-preventing and reducing mobility of elements in tailings site.

Study of Hydrolysis of Al Powder and Compaction of Nano Alumina by Spark Plasma Sintering(SPS) (Al 분말의 수화 반응과 스파크 플라즈마 열처리법으로 제조된 알루미나 성형체 연구)

  • Uhm Y. R.;Lee M. K.;Rhee C. K.
    • Journal of Powder Materials
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    • v.12 no.6 s.53
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    • pp.422-427
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    • 2005
  • The $Al_2O_3$ with various phases were prepared by simple ex-situ hydrolysis and spark plasma sintering (SPS) process of Al powder. The nano bayerite $(\beta-Al(OH)_3)$ phase was derived by hydrolysis of commercial powder of Al with micrometer size, whereas the bohemite (AlO(OH)) phase was obtained by hydrolysis of nano Al powder synthesized by pulsed wire evaporation (PWE) method. Compaction as well as dehydration of both nano bayerite and bohemite was carried out simultaneously by SPS method, which is used to fabricate dense powder compacts with a rapid heating rate of $100^{\circ}C$ per min. under the pressure of 50MPa. After compaction treatment in the temperature ranges from $100^{\circ}C\;to\; 1100^{\circ}C$, the bayerite and bohemite phases change into various alumina phases depending on the compaction temperatures. The bayerite shows phase transition of $Al(OH)_3{\to}{\eta}-Al_2O_3{\to}{\theta}-Al_2O_3{\to}\alpha-Al_2O_3$ sequences. On the other hand, the bohemite experiences the phase transition from AlO(OH) to ${\gamma}-Al_2O_3\;at\;350^{\circ}C.$ It shows AlO(OH) ${\gamma}-Al_2O_3{\to}{\delta}-Al_2O_3{\to}{\alpha}-Al_2O_3$ sequences. The ${\gamma}-Al_2O_3$ compacted at $550^{\circ}C$ shows a high surface area $(138m^2/g)$.

The Effects of Si or Sn on the Sintered Properties of Fe-(Mo,Mn)-P Lean alloy (Fe-(Mo,Mn)-P계 Lean alloy의 소결특성에 미치는 Si와 Sn의 영향)

  • Jung, Woo-Young;Ok, Jin-Uk;Park, Dong-Kyu;Ahn, In-Shup
    • Journal of Powder Materials
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    • v.25 no.4
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    • pp.302-308
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    • 2018
  • A lean alloy is defined as a low alloy steel that minimizes the content of the alloying elements, while maintaining the characteristics of the sintered alloy. The purpose of this study is to determine the change in microstructure and mechanical properties due to the addition of silicon or tin in Fe-Mo-P, Fe-Mn-P, and Fe-Mo-Mn-P alloys. Silicon- or tin-added F-Mo-P, Fe-Mn-P, and Fe-Mo-Mn-P master alloys were compacted at 700 MPa and subsequently sintered under a $H_2-N_2$ atmosphere at $1120^{\circ}C$. The sintered density of three alloy systems decreases under the same compacting pressure due to dimensional expansion with increasing Si content. As the diffusion rate in the Fe-P-Mo system is higher than that in the Fe-P-Mn system, the decrease in the sintered density is the largest in the Fe-P-Mn system. The sintered density of Sn added alloys does not change with the increasing Sn content due to the effect of non-dimensional changes. However, the effect of Si addition on the transverse rupture strengthening enhancement is stronger than that of Sn addition in these lean alloys.

Wetting-Induced Collapse in Fill Materials for Concrete Slab Track of High Speed Railway (고속철도 콘크리트궤도 흙쌓기재료의 Wetting Collapse에 관한 연구)

  • Lee, Sung-Jin;Lee, Il-Wha;Im, Eun-Sang;Shin, Dong-Hoon;Cho, Sung-Eun
    • Journal of the Korean Geotechnical Society
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    • v.24 no.4
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    • pp.79-88
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    • 2008
  • Recently, the high speed railway comes into the spotlight as the important and convenient traffic infrastructure. In Korea, Kyung-Bu high speed train service began in bout 400 km section in 2004, and the Ho-Nam high speed railway will be constructed by 2017. The high speed train will run with a design maximum speed of 300-350 km/hr. Since the trains are operated at high speed, the differential settlement of subgrade under the rail is able to cause a fatal disaster. Therefore, the differential settlement of the embankment must be controlled with the greatest care. Furthermore, the characteristics and causes of settlements which occurred under construction and post-construction should be investigated. A considerable number of studies have been conducted on the settlement of the natural ground over the past several decades. But little attention has been given to the compression settlement of the embankment. The long-term settlement of compacted fills embankments is greatly influenced by the post-construction wetting. This is called 'hydro collapse' or 'wetting collapse'. In spite of little study for this wetting collapse problem, it has been recognized that the compressibility of compacted sands, gravels and rockfills exhibit low compressibility at low pressures, but there can be significant compression at high pressures due to grain crushing (Marachi et al. 1969, Nobari and Duncan 1972, Noorany et al. 1994, Houston et al. 1993, Wu 2004). The characteristics of compression of fill materials depend on a number of factors such as soil/rock type, as-compacted moisture, density, stress level and wetting condition. Because of the complexity of these factors, it is not easy to predict quantitatively the amount of compression without extensive tests. Therefore, in this research I carried out the wetting collapse tests, focusing on various soil/rock type, stress levels, wetting condition more closely.

Reheating Process of Metal Matrix Composites Fabricated by Combined Stirring Process for Thixoforming (복합교반법으로 제조한 금속복합재료의 Thixoforming용 재가열공정)

  • 이동건;강충길
    • Transactions of Materials Processing
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    • v.11 no.1
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    • pp.45-53
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    • 2002
  • The forming process of metal matrix composites by die casting and squeeze casting process are limited in size and dimension In term of final parts. The melt strirring method have the problems that the homogeneous distribution of the reinforcements is difficult due to the low weldability and the density difference between the molten metal and the reinforcement. The thixoforming process for metal matrix composites has numerous advantages compacted to die casting, squeeze casting and compocasting. However, for the thixofoming process, the billet with the desired volume fraction must be heated to obtain a uniform temperature distribution over the entire cross-sectional areas. To obtain the reheating conditions of composites, the particulate reinforced metal matrix composites for thixoforming were fabricated by combined stirring process which is simultaneously performed with electro-magnetic stirring and mechanical stirring process. The matrix alloy and reinforcement are used to aluminum alloy(A357) and SiCp with diameter 14, $25{\mu}m$, respectively. The microstructure characteristics were investigated by changing the volume fraction and reinforcement size. The heating conditions to obtain the uniform temperature distribution in cross section area of fabricated metal matrix composites billet are proposed with heating time, the heating temperature and the holding time.

The Electromagnetic and Thermal Properties of Magnetic Core Materials for the Power Line Communication as the function of Additives (첨가제에 따른 전력선 통신용 자심 재료의 전자기적 특성 및 발열거동)

  • 오영우;이혜연;김현식;허정섭;민복기;김종령
    • The Transactions of the Korean Institute of Electrical Engineers C
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    • v.52 no.2
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    • pp.61-66
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    • 2003
  • The electromagnetic properties and thermal behavior of Mn-Zn ferrite cores used for the blocking filter in he Power Line Communication(PLC) application were investigated as the function of additives. The highest density and permeability of 4.98 g/㎤) and 8,221 respectively were obtained to the specimen with composition of MnO 24 mol%, ZnO 25 mol% and Fe$_2$O$_3$ 51 mol% added MnO$_3$ 400 ppm, SiO$_2$ 100 ppm and CaO 200 ppm since the uniform grains were organized and the microstructures were compacted through reduction of pores. The permeability was increased up to 13,904 as temperature of specimen increased to 11$0^{\circ}C$, however, it was decreased precipitously under 100 over 11$0^{\circ}C$. The exothermic behavior was observed in the frequency range from 1 kHz to 1 MHz that the maximum temperature of specimens became 102$^{\circ}C$ at 1 MHz. In the consequence, the Mn-Zn ferrite core developed by this research will maintain the stable electromagnetic properties since the temperature of ferrite core rose to 93$^{\circ}C$ in the range of 10 kHz to 450 kHz bandwidth qualified for PLC.

A Study on the Radio-activity Reduction Method for the Decladding Hull

  • Kim, Jong-Ho;Jung, In-Ha;Park, Jang-Jin;Shin, Jin-Myeong;Lee, Ho-Hee;Yang, Myung-Seung
    • Proceedings of the Korean Radioactive Waste Society Conference
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    • 2004.02a
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    • pp.130-139
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    • 2004
  • The cladding materials remaining after reprocessing process of the nuclear fuel, generally called as hulls, are classified as a high-level radioactive waste. They are usually packaged in the container for disposal after being compacted, melted, or solidified into the matrix. The efforts to fabricate a better ingot for a more favorable disposal to the environment have failed due to the technical difficulties encountered in the chemical decontamination method. In the early 1990s, the accumulation of radio-chemical data on hulls and the advent of new technology such as a laser or plasma have made the pre-treatment of the hulls more efficient. This paper summarizes the information regarding the radio-chemical analysis of the hull through a literature survey and determines the characteristics of the hull and depth profile of the radio-nuclides within the hull thickness. The feasibility study was carried out to evaluate the reduction of the radioactivity by peeling off the surface of the hull with the application of laser technology.

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A Study on the Mechanical Compaction of Fill Dam (Fill Dam의 기계 전압효과에 관한 연구)

  • 윤충섭;김주범
    • Magazine of the Korean Society of Agricultural Engineers
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    • v.21 no.3
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    • pp.92-103
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    • 1979
  • The compaction of core zone of the fill dam is very important foe increasing of the Strength of soil mass and reduction of permeability of the core. The principal objects of this study are to give the construction criteria of tamping rollers and to find out the relationships between density and permeability of soil after compaction. The results in this study are summarized as follows. 1. The core zone of fill dam should be compacted more than 8 passed because the compaction effects of clayey soil increase sharply in about 8 passes of roller. 2. The coefficient of permeability (K) increases with the thickness of compaction of soil even though the density is same. 3. The effect of compaction increases with the quantity of coarse materials such as coarse sand and gravel. 4. If D values change from 100 percent to 98 percent and from 100 percent to 95 percent, K values become 2 times and 5 times of initial K value respectively. 5. The coefficient of permeability in the field soil is very high comparing with the result of laboratory test at the same 100 percent compaction ratio, but differences between both results decrease with the decrease of compaction ratio. 6. Thickness of soil layer for the compaction should be increased for heavier compaction machine. 7. In order to get the compaction ratio of 98 percent or more, 10 to 12 passes of roller is generally required with the thickness of soil from 20cm to 30cm.

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An Experimental Study on the Ultrasonic Testing for Determinig Dynamic Soil Moduli (초음파를 이용한 흙의 동적계수측정에 관한 실험적 연구)

  • 민덕기;김문득
    • Geotechnical Engineering
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    • v.7 no.1
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    • pp.7-14
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    • 1991
  • Determination of dynamic shear modulus of soil was made by measuring directly the velocity of ultrasonic shear waves transmitted through the specimen. The PUNDIT, a generator and detector of ultrasonic waves, has been used to measure the propagation velocity. Forty -six tests of compacted soil at seven different void ratios and seven varying degrees of saturation with four types of materials were made in this study. The primary importance in this study was the investigation of the relations among the para meters which influenced G-modulus, As a results of analysis, the dynamic shear modulus of soil tends to decrease with an increase of void ratio, and also it is affected by soil types. In case of using PUNDIT, the proper range of the specimen length is from 5cm to 8cm. And the degree of saturation doesn't affect the dyn- amic shear modulus of soil.

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