• The Korean Fashion and Textile Research Journal
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• v.6 no.6
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• pp.778-784
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• 2004

The natural dyeing of silk fabric with natural gardenia blue powder was investigated. The sum of K/S values was increased with increasing the amount of gardenia powder up to 20%,(o.w.b.). The proper time, temperature and pH for the dyeing of silk fabric with gardenia blue powder were 60~80 minutes, $80^{\circ}C$ and pH 4, respectively. The B and BG colors were obtained according to various mordanting methods, mordants and mordant concentrations. The various colorfastness were not improved by mordanting. The colorfastness to light was poor, but the colorfastness to dry cleaning and washing were good.

• Proceedings of the Korean Society of Dyers and Finishers Conference
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• 2008.04a
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• pp.105-107
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• 2008

Dyeing properties of the colorants extracted from pomegranate hull on hair were investigated to study its efficay of natural hair coloring dye. Effect of dyeing condition and mordanting on dye uptake, color change and colorfastness were explored. In addition, tensile strength retention is measured and the surface of the hair was observed by SEM. The water extracted pomegranate hull was concentrated and freeze-dried for preparing colorant powders. It was considered that ionic bonding was involved in the adsorption of pomegranate colorants to hair. Pomegranate hull colorants produced greyish brown colors on hair and the hair mordanted with Fe showed dark brown color. Mordant except Fe did not significantly increased dye uptake. Mordant except Cu increased light fastness, mordant except Cr increased washing fastness. SEM to observe the hair is damaged by ultraviolet light and cleaning. This is consistent with the results of tensile strength retention. From the results of colorfastness th washing and light, it was concluded that colorants from pomegranate hull can be need as a semi-permanent natural hair coloring dye.

• Korean Journal of Human Ecology
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• v.18 no.6
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• pp.1315-1321
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• 2009

The chemical composition of natural powder dye $Pinux^{TM}$ manufactured from Pinus radiata bark and dyeability of dyed silk fabrics with $Pinux^{TM}$ were examined. It is made up of the optimum dyeing condition of silk fabric according to the dyeing concentration, dyeing time, and dyeing temperature. Also, we examined the colorfastness and antibiosis of dyed silk fabrics to washing, rubbing, perspiration and light. For the analysis of the chemical composition of $Pinux^{TM}$, the total contents of phenolic compound, proanthocyanidin(PA) and anti-oxidative activities of the dye were analyzed. As a result, it was found that the main components of the $Pinux^{TM}$ manufactured from Pinus radiata bark is proanthocyanidin, mostly a flavonoid containing a procyanidin structure, and it consists of approximately 63% phenol. As a result of examining the dyeability of silk fabrics with $Pinux^{TM}$, it showed that the dyeability was best under the conditions of the concentration of dye $1{\sim}1.5%$(wt/v%), dyeing time of 90 minutes, and dyeing temperature at $90^{\circ}C$. It was found that the colorfastness of dyed silk fabrics, colorfastness to washing, perspiration for acidic and rubbing were as good as grade 4 or 4-5. However, the colorfastness to light was low at grade 1, the same as the results of other natural dyed fabrics. As a result of the antibiosis measurement for the $Pinux^{TM}$-dyed silk fabrics, it showed high antibacterial properties to Staphylococcus sureus at 99.6%.

• Journal of the Korea Fashion and Costume Design Association
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• v.4 no.1
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• pp.99-110
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• 2002

This study is performed to investigate the effect of the mordant and chitosan on the colorfastness to laundering and physical properties of the mordanted, chitosan treated and natural - dyed cotton, silk and acrylics substrates. Natural dyes are extracted from Gromwell by boiled water. Three different compounds of Al, Cu, Sn and Chitosan are used as mordanting agents. The result of this study is summarized as follows: 1. Color of the fabrics dyed with Gromwell changes redder, bluer and darker after chitosan treated and mordanting. 2. After washing, the color of natural dyes changes more light and gray, Chitosan and Cu mordanting gives better colorfastness in washing than any others. 3. All chitosan treated fabrics improve air permeability. 4. In the chitosan treated fabrics, a half life of the static electricity is shown good result.

• Journal of Fashion Business
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• v.23 no.4
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• pp.100-111
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• 2019

In this study, the dyeing properties and functionalities of Crataegi fructus extract were investigated for the purpose of application to new natural dye resources. The effects of dyeing conditions(concentration of dye, dye bath temperature, dyeing duration and dye bath pH) and mordanting on dye uptake and color changes were also examined. The study also estimated the colorfastness, antibacterial properties, and ultraviolet protection properties of the dyed and mordanted silk fabrics. The dye uptake increased in tandem with the dye concentration and dye bath temperature. The highest K/S values were obtained at the following conditions: a dye concentration of 100%(v/v), a dyeing period of 60 minutes, a dye bath temperature of $90^{\circ}C$, and a dyeing pH of 3. The colorfastness of the material when dry cleaned or rubbed ranged from good to excellent and fastness to light was rated at grade 2-3. The change in the color grade when exposed to washing was not good; however, the stain of washing fastness was good at a range of 4-5. In regards to the functional property aspects, the dyed and mordanted fabrics exhibited excellent results with a 99.9% reduction rate, and excellent ultraviolet protection factors.

• Korean Journal of Rural Living Science
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• v.10 no.2
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• pp.28-36
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• 1999

The purpose of this study was to examine the best condition for dyeing silk in green color used kudzu-vine leaves which were available everywhere in our country except winter. Dyeing experiments were done under various dyeing conditions according to extracting method of dyebath from kudsu-vine leaves, pH of dyebath, dyeing time, concentration of dyebath and mordants which were treated after dyeing. Color difference ($\Delta$E) and Munsell's HV/C and color fastness to drycleaning, washing, perspiration and light were measured. The main results were as follows : 1. The color difference of dyed silk increased in dyebath B & C which were extracted in alkali water comparing with dyebath A which was extracted in distilled water. In dyebath B & C, the color difference was the highest in case of dyebath pH 5.0. 2. The colors of fabrics dyed in dyebath A were mainly yellow and the colors in dyebath B & C were yellow green. 3. The color differences of dyed silk increased according to dyeing time and concentration of dyebath. 4. The color were changed with the treatment of mordants. The most strong green color could get in Cu mordant treatment in dyebath C, pH 5.0, and concentration 4. 5. The peak of reflectance within the visible light of the fabric dyed in the most strong green color could be seen in $\lambda$500-520nm. 6. On the whole, the colorfastness of experimental fabrics dyed in dyebath B, C and Cu mordant treatment was good except the colorfastness to the light.

• The Korean Fashion and Textile Research Journal
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• v.26 no.4
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• pp.411-423
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• 2024

This study examined the dyeability and functionality of silk fabrics dyed using shiitake mushroom pins discarded in large quantities on mushroom farms. FT-IR and UV-Vis spectral analyses showed that polyphenols and flavonoids were present in the hot-water extract of shiitake mushroom pins. Optimal dyeing conditions for silk fabrics were a dye concentration of 50% (v/v), dyeing temperature of 80℃, dyeing time of 60 minutes, and dyebath pH of 5.3. The post-mordant method showed a greater effect on the increase in dye uptake and color change than the pre-mordant method. Unmordanted fabrics appeared as a YR Munsell color. Except for the Cu-mordant, all post-mordanted fabrics produced a Y Munsell color. The FE-SEM/EDX analysis confirmed that the natural iron solution and mud contained various metal ions. The Fe component was found to have the greatest effect on the dye uptake and color properties. The colorfastness of the unmordanted fabrics to washing, dry cleaning, rubbing, and perspiration was excellent (above grade 4), whereas light was grade 3-4. In the case of post-mordanted fabrics with a natural iron solution, the colorfastness to washing, wet rubbing, and light improved by 0.5 grades. For post-mordanted fabrics with mud, the colorfastness to light and sweat improved by 0.5 grades. The bacterial reduction rate for staphylococcus aureus in fabrics dyed with shiitake mushroom pin extract was excellent at over 99.9%, the bacterial reduction rate for klebsiella pneumoniae was 98.1%, and the deodorization rate was excellent at 90%. These results indicate that shiitake mushroom pins can be used as a sustainable, functional natural dye.

• The Korean Fashion and Textile Research Journal
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• v.9 no.1
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• pp.103-112
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• 2007

The purpose of this study was to investgate dyeing, moradnting properties and colorfastness activities of silk, polyamide, acetate treated black soybean extracts. The color of extract by buffer solution (pH=1) red, but the higher pH of extracted black soybean solution the paler of color strength. Black soybean extracts was approved anthocyanin of 3type(Delphinidin3-glucoside, Cyanidin 3-glucoside, Petunidin 3-glucoside) by chemiclal analysis. This anthocynin, in acid condition, is oxinium structure (red color, soluable) but, in alkali condition quinoid structure(dark brown, in soluable). The optimum dyeing condition of black soybean anthocynin was 10min at $30^{\circ}C$, pH -1. Colorfastness to washing and light showed generally low but crocking fastness was excellent.

• Textile Coloration and Finishing
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• v.23 no.3
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• pp.187-194
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• 2011

This study used Jeju scoria to dye cotton fabric and measured its dyeability, colorfastness, antibacterial activity, deodorization efficiency, ultraviolet protection, and far-infrared emission. The cotton fabric was colored to yellowish red and optimal dyeing can be achieved at a temperature of $80^{\circ}C$ for a dyeing time of 120 minutes with a colorant concentration of 25%(o.w.b). The colorfastness to light, rubbing, perspiration, and washing was 8, 5, 5, and 4~5 ratings respectively, where the wash colorfastness remained after 15 wash cycles. The cotton fabric dyed with Jeju scoria demonstrated excellent antimicrobial activity to Staphylococcus aureus and high deodorization efficiency. Ultraviolet protection factor was as high as 50+. The Jeju scoria can be used as a new colorant for the natural dyeing of silk.

• The Korean Fashion and Textile Research Journal
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• v.14 no.2
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• pp.304-310
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• 2012

The natural dyeing of silk fabric with Scutellaria baicalensis extract was investigated. The proper colorant concentration, dyeing temperature, dyeing time, and pH for the dyeing of silk fabric with Scutellaria baicalensis extract were 90% v/v, $90^{\circ}C$, 60 minutes and pH 3, respectively. In various mordanted methods, the K/S values of mordanted methods were higher than those of unmordanted methods. Light colorfastness and washing colorfastness of Fe mordanted silk fabric was improved by mordanting. The antibacterial properties of dyed and mordanted silk fabric showed a high reduction rate, and Scutellaria baicalensis extract was showed effective bacterial reduction.