• Title/Summary/Keyword: coating properties

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The properties of $(Ba_{0.7}\;Sr_{0.3})TiO_3$ by Multilayer structure (다층 구조에 의한 $(Ba_{0.7}\;Sr_{0.3})TiO_3$의 물리적 특성)

  • Hong, Kyung-Jin;Cho, Jae-Cheal
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2006.05a
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    • pp.31-34
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    • 2006
  • In this study, $(Ba_{0.7}\;Sr_{0.3})TiO_3$ was coated on Pt/Ti/$SiO_2$/Si wafer by using Sol-Gel method. Coating process was repeated 3~5 times and then sintered at 750[$^{\circ}C$] for 1 hour. Each specimen was analyzed structure and electrical characteristics. In structure characteristics, EDX analyzed the samples ratio of the formation on the structural property. Thermal behavior was observed with TG-DTA and concluded that the heat-treatment of the samples was degreed 750[$^{\circ}C$]. Surface and section of thin films were observed with SEM.

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Growth and characterization of Eu-doped bismuth titanate (BET) thin films deposited by sol-gel method

  • Kang Dong-Kyun;Kim Byong-Ho
    • Proceedings of the Korean Society Of Semiconductor Equipment Technology
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    • 2006.05a
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    • pp.194-197
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    • 2006
  • Lead-free bismuth-layered perovskite ferroelectric europium-substituted $Bi_{4}Ti_{3}O_{12}(BTO)$ thin films have been successfully deposited on Pt/Ti/$SiO_2$/Si substrate by a sol-gel spin-coating process. $Bi(TMHD)_3,\;Eu(THMD)_3,\;Ti(OiPr)_4$ were used as the precursors, which were dissolved in 2-methoxyethanol. The thin films were annealed at various temperatures from $600^{\circ}\;to\;720^{\circ}C$ in oxygen ambient for 1 hr, which was followed by post-annealed for 1 hr after depositing a Pt electrode to enhance the electrical properties. X-ray diffraction (XRD) and scanning electron microscopy (SEM) were used to analyze the crystallinity and surface morphology of layered perovskite phase, respectively. The remanent polarization value of the BET thin films annealed at $720^{\circ}C\;was\;25.95{\mu}C/cm^2$ at an applied voltage of 5 V.

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Synthesis and Characterization of Superparamagnetic Fe3O4@SiO2 Nanoparticles

  • Kulkarni, Sachnin A.;Sawadh, P.S.;Palei, Prakash K.
    • Journal of the Korean Chemical Society
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    • v.58 no.1
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    • pp.100-104
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    • 2014
  • Magnetite nanoparticles were prepared by co-precipitation method and then silica was coated onto the surface of $Fe_3O_4$ by hydrolysis of TEOS. The silica coated magnetite nanoparticles were characterized for its structural, microstructural, optical, vibrational and magnetic properties by X-ray diffraction analysis, Scanning electron microscopy, UV-visible spectroscopy, Infrared spectroscopy and Vibration sample magnetometer, respectively. XRD study confirmed the presence of $SiO_2$ on the surface of magnetite nanoparticles. SEM study indicated that with increase in TEOS content the particles become bigger and mono-disperse. It was also found that the silica coating prevents magnetic particles from aggregation and imparts excellent stability.

The Optical Characteristics of CdS Thin Films and Powders (CdS 분말 및 박막의 광학적 특성)

  • Chang, Ki-Seog
    • Korean Journal of Crystallography
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    • v.19 no.1
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    • pp.25-30
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    • 2008
  • In order to characterize the optical properties of CdS thin films and CdS powders, the following experiments were performed: CdS wurtzite thin films were made using 99.99% CdS (Aldrich) powder and the $AlO_x$ membranes in $7{\times}10^{-6}$ torr(here, the average vacuum coating speed is $1{\AA}/sec$.). The surface states of CdS nano-particles with dimensions of 3.87 nm were studied through the fluorescence spectroscopy. From the resulting spectra exhibited, we can see a sharp fluorescence at 451 nm arising from the excitons on the CdS thin films, compared with the 448nm peak of the CdS powders.

Sensing Behavior and Long-Term Stability of Polyaniline Sensor Coated with Poly(vinylidenefluoride) for Methanol Vapors (폴리비닐리덴플루오라이드로 코팅한 폴리아닐린센서의 메탄올에 대한 감응 특성과 장기안정도 고찰)

  • Sohn Sung-Ok;Kim Jung-Suk;Huh Jeung-Soo
    • Korean Journal of Materials Research
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    • v.14 no.4
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    • pp.260-264
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    • 2004
  • The problem of polyaniline (PANi) sensor has been poor mechanical and chemical stability under atmosphere condition. In order to overcome these problems, the PANi sensor coated with polyvinylidenefluoride ($PVF_2$) was employed. The morphology of $PVF_2$ coated-PANi layer was showed smooth and transparent properties at 15% concentration of coating solution. The resistance of $PVF_2$ coated-PANi was kept at constant value and had a good stability at long-term periods in presence of humidity.

Monodisperse Micrometer-Ranged Poly(methyl methacrylate) Hybrid Particles Coated with a Uniform Silica Layer

  • Han, Seung-Jin;Shin, Kyo-Min;Suh, Kyung-Do;Ryu, Jee-Hyun
    • Macromolecular Research
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    • v.16 no.5
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    • pp.399-403
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    • 2008
  • Monodisperse, micron-sized, hybrid particles having a core-shell structure were prepared by coating the surface of poly(methyl methacrylate)(PMMA) microspheres with silica and by copolymerizing acrylamide (AAm) to supply the hydrogen bonding effect by means of the amide groups. Tetraethoxysilane (TEOS) was then slowly dropped onto the medium under certain conditions. Because of the hydrogen bonding between the amide of the PMMA particles and the hydroxyl group of the hydrolyzed silanol, a silica shell was generated on the PMMA core particles. The morphology of the hybrid particles was investigated with transmission (TEM) and scanning (SEM) electron microscopy as a function of the medium conditions and the amount of TEOS. Improved thermal properties were observed by TGA analysis.

Fabrication and Characterizations of Thick PZT Films for Micro Piezoelectric Devices (마이크로 압전 소자용 후막 PZT의 제조 및 물성 평가)

  • 박준식;박광범;윤대원;박효덕;강성군;최태훈;이낙규;나경환
    • Transactions of Materials Processing
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    • v.11 no.7
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    • pp.569-574
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    • 2002
  • Recently, thick PZT films are required for the cases of micro piezoelectric devices with high driving force, high breakdown voltage and high sensitivity, and so on. In this work, thick PZT films were fabricated by Sol-Gel multi-coating method. Microstructures, and electrical properties of films were investigated by XRD, FESEM, impedance analyzer, and P-E hysteresis. PZT films with 2.7$mu extrm{m}$ to 4.4${\mu}{\textrm}{m}$ thickness were fabricated. Dielectric constant, loss, remnant polarization and coercive field of them were 880~1650 at 1kHz, 2~3% at 1kHz, 26~32 $\mu$C/$ extrm{cm}^2$, and 33~60kV/cm, respectively. Also a transverse piezoelectric coefficient $(e_{31,f})$ measurement system was fabricated and tested for thick film samples.

A Study on Surface Treatment for Rubber Materials with Low Friction Factor

  • Li, Xiang-Xu;Cho, Ur Ryong
    • Elastomers and Composites
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    • v.51 no.1
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    • pp.43-48
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    • 2016
  • Multi-Surface (MS) treatment is a new technique of surface treatment to reduce the static friction factor on the surface of rubber. MS treatments include 4 methods which names are MS-V (UV-irradiation on the rubber surface), MS-M (doing the chemical reaction with double bond of rubber), MS-Q (dilution of rubber surface by silicone surfactant), and MS-P (coating and heating of rubber surface). The experiment and test of every MS-treatment had been carried out using acrylonitrile-butadiene rubber (NBR), ethylene-propylene-diene rubber (EPDM), and chlorosulphonated rubber (CSM) as rubber materials. It had introduced the steps of every MS-treatment process and the result of the properties test. From the research, it was found that the best method was MS-V treatment because it suited all the samples and the effect was obviously.

Efficiency of Photovoltaic Cell with Random Textured Anti Glare (RTAG) Glass

  • Kim, Geon Ho;Jeon, Bup Ju
    • Applied Science and Convergence Technology
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    • v.25 no.6
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    • pp.133-137
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    • 2016
  • The surface treatment of cover glass for conversion efficiency of photovoltaic cell is important to reduce reflectivity and to increase the incident light. In this work, random textured anti glare (RTAG) glass was prepared by wet surface coating method. Optical properties due to the changes of surface morphology of RTAG glass were compared and conversion efficiency of photovoltaic cell was researched. Grain size and changes of surface morphologies formed with surface etching time greatly affected optical transmittance and transmission haze. Current density (Jsc) were high at the condition when surface morphologies reflection haze were low and transmission haze were high. Jsc was $40.0mA/cm^2$ at glancing angle of $90^{\circ}$. Incidence light source was strongly influenced by surface treatment of cover glass at high incidence angle but was hardly affected light source at the low angle of incidence.

Preparation and Characterization of PVA/SA Blend Nanofiltration membranes

  • Llee, Kew-Ho
    • Korean Membrane Journal
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    • v.1 no.1
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    • pp.86-92
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    • 1999
  • The nanofiltration (NF) membranes based on poly(vinyl alcohol) (PVA) and sodium alginate (SA) were prespared. Homogeneous PVA/SA blend membranes were prepared by casting a PVA/SA (95/5 in wi%) mixture solution on an acryl plate followed by drying at a room temperature and by cros-slinking with glutaraldehyde (GA) for 20 minutes PVA/SA blend composite membranes were also prepared by coating a PVA/SA (95/5 in wi%) mixture solution on microporous polysulfone(PSF) supports. The PVA/SA active layer of the composite membrane was crosslinked at room temperature by using an membranes were characterized with a scanning electron microscopy (SEM) a fourier transform infrared spectroscopy (FTIR) and permeation tests. The permeation properties of the composite membrane were as follows: 1.3{{{{ {m }^{2 } }}}}/{{{{ {m }^{2 } }}}}day of flux and >95% of rejection at 200 psi for a 1000 ppm PEG600 solution.

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