• Title/Summary/Keyword: coating properties

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Effect of Prefiring Time on Epitaxy and crystallinity of Pb(Zr, Ti)O$_3$ Thin Films in Low Temperature Pyrolysis (저온도포열분해에 의해 제조된 Pb(Zr, Ti)O$_3$ 박막의 에피탁시와 결정화도에 미치는 전열처리 시간의 영향)

  • 황규석;이형민;김병훈
    • Journal of the Korean Ceramic Society
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    • v.35 no.9
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    • pp.969-973
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    • 1998
  • Pb(Zr, Ti)O3 (PZT) (Zr:Ti= 52: 48) thin films were prepared on MgO(100) substrates by dipping-py-rolysis process using metal naphthenates as starting materials. Thin films were fabricated by spin coating technique and the precursor films were prefired at 20$0^{\circ}C$ in air for 0.5, 1, 2, 3, and 24 h followed by final heat treatment at 75$0^{\circ}C$ for 30min. Film prefired for 24 h lost orientational properties and pole figure analysis showed the lost of the epitaxial relationship between the films and substrate while highly a/c-axis oriented thin films were obtained for the samples prefired for 1, 2, and 3h.

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Removal of Se(IV) by the Fe(III)-impregnated Sea sand - Zeta potential approach to depict the binding between Fe(III) and Sea sand (표면 처리한 Sea sand를 이용한 Se(IV) 제거 - Zeta potential을 통한 Fe(III)간의 반은 메카니즘 연구)

  • 박상원;강혜정
    • Journal of Environmental Science International
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    • v.8 no.2
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    • pp.205-209
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    • 1999
  • Iron hydroxides are good adsorbents for uncomplexed metals, some metal-ligand complexes and many metal oxyanions. However, their adsorption properties of these precipitations are not fully exploited in wastewater treatment operations because of difficulties associated with their separation from the aqueous phase. This study describes experiments in which iron hydroxides were coated onto the surface of ordinary adsorbents(Sea sand) that are very resistant to acids, The coated adsorbents were used in adsorption of oxyanionic metals. The process was successful in removing some anions such as $SeO_3(-II)$ over a wide range of metal concentrations and sorption of oxyanionic metals increased with decreasing pH. Formation of two surface complexes for oxyanionic metals adsorption on iron hydroxides comprise (1) complexation of the free anion by a positively charged surface site, and (2) protonation of the adsorbed anion (or alternatively adsorption of a protonated form from solution) The coated adsorbents are inexpensive to prepare and could serve as the basis of a useful oxyanionic metal removal.

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The Effect of Heat Treatment Hold Time for Mechanical Properties of Zinc-Magnesium Alloy (아연-마그네슘 합금의 열처리에 따른 기계적 특성 연구)

  • Hwang, Injoo
    • Journal of the Korean Society for Heat Treatment
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    • v.33 no.3
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    • pp.117-123
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    • 2020
  • Due to high corrosion resistance, Zinc has been widely used in the automobile, shipping or construction industries as a galvanizing material. Zinc is popular as a coating element, but its low mechanical strength impede the expansion of applications as a load-bearing structure. The mechanical strength of Zinc can be increased through zinc based alloy process, but the ductility is significantly reduced. In this study, the mechanical strength and ductility of Zinc-Magnesium alloys with respect to heat treatment hold time was investigated. In order to enhance the mechanical strength of Zinc, a Zinc-Magnesium alloy was fabricated by a melting process. The heat treatment process was performed to improve the ductility of Zinc-Magnesium alloy. The microstructure of the heat-treated alloy specimen was analyzed using SEM. The hardness and compressive strength of the specimen were measured by a micro-hardness tester and a nano-indenter, respectively.

Laser Welding of Thermoplastics Using the Absorbing Materials (열가소성 플라스틱의 흡수체를 이용한 레이저 접합)

  • Seo M.H.;Ryu K.H.;Nam G.J.
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2005.06a
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    • pp.430-433
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    • 2005
  • Laser bonding between similar and dissimilar thermoplastics has been investigated by making use of laser transmission weld technique. Spot welding of two layers of plastic materials has been demonstrated by using of a high-quality diode-laser with 808nm wavelength. Weld areas increases according to power density, exposure time. The results of peel out test show that peel strengths increase with the area of molten plastics. Layers, which have the same chemical properties, have good bonding qualities. A bonding method which dye film is coated on the interface is used for laser bonding between plastics with high transmission for laser wavelength. Laser transmission bonding is worthy of attention because it is not in contact, requires a few tooling devices, allows a flexible energy delivery and produces nearly invisible welds

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Microstructure and Tribological Characteristics of AlSi-Al$_2$O$_3$ Composite Coating Prepared by Plasma Spray (플라즈마 용사에 의한 AlSi-Al$_2$O$_3$ 복합재료 코팅층의 미세조직 및 마찰.마모특성)

  • Min Joon-Won;Yoo Seung-Eul;Kim Young-Jung;Suhr Dong-Soo
    • Journal of Welding and Joining
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    • v.22 no.5
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    • pp.46-52
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    • 2004
  • AlSi-Al$_2$O$_3$ composite layer was prepared by plasma spray on steel substrate. The composite powder for plasma spray was prepared by simple mechanical blending. The wear resistance of the composite layers and matrix aluminum alloy were performed in terms of size distribution of ceramic particles. Friction coefficients of AlSi were decreased with incorporation of $Al_2$O$_3$. The tribological properties of coated layers were affected by the size of incorporated $Al_2$O$_3$ particle. The reinforcement of $Al_2$O$_3$ particle into aluminum alloy matrix decreased the friction coefficient as well as wear loss.

Resolution and Adhesion Properties of Solder Resist for Printed Circuit Board (인쇄회로기판용 solder resist의 해상성과 밀착력)

  • Chol, Sung-Ho;Hwang, Seong-Jin;Kim, Hyung-Sun
    • Korean Journal of Materials Research
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    • v.17 no.12
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    • pp.676-681
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    • 2007
  • According to progress rapidly digitalization, networked and mobilization of electronics industry, there are demands for being smaller, thinner, more light, and more efficient complex functions of electronic devices which are wireless devices, semi-conductors, packages and mobile devices. Therefore, the solder resist on a printed circuit board have been required with the high resolution and the eco-friendly materials in the surface treatments such as high heating process and coating process with electrolysis. In this study, the photoinitiator initiator and monomers of the solder resist were prepared with their contents for reducing the occurrence of the under-cut. We investigated the sample surface by UV/VIS spectrometer, FT-IR, OM after HASL and ENIG process. From our results, it is possible to get a high adhesion of resist with optimal contents between the photoinitiator initiator and monomers after surface treatments.

Field emission properties of carbon nanotubes grown by various methods (다양한 방법에 의해 성장된 탄소 나노튜브의 전계방출 특성)

  • Kim, Bu-Jong;Chang, Han-Beet;Kim, Jong-Pil;Park, Jin-Seok
    • Proceedings of the KIEE Conference
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    • 2011.07a
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    • pp.1408-1409
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    • 2011
  • Carbon nanotubes (CNTs) were grown on conical tip substrates by using various methods such as electrophoretic deposition, dip-coating, and spray. The scanning electron microscope measurement showed that the spray method ascertained the most uniform deposition of CNTs. The CNT-emitter that was fabricated by the spray method revealed the lowest turn on voltage of electron emission and the highest emission current. In addition, the spray-produced CNT emitter showed the most stable long-term emission characteristics.

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A Development on the Non-Photomask Plate Making Technology for Screen Printing (포토 마스크가 필요없는 스크린 제판 기술 개발)

  • Koo, Yong-Hwan;Ahn, Suk-Chul;Kim, Sung-Bin;Nam, Su-Yong
    • Journal of the Korean Graphic Arts Communication Society
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    • v.28 no.1
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    • pp.65-75
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    • 2010
  • Environmentally friendly, stencil and screen printing for cost-effective for maskless. In this study, UV -LED light source for the dispersion characteristics and high competence photoresist coating was prepared. Wavelength of 365nm UV-LED exposure device using the maskless lithography, 1.7kgf/$cm^2$ $2600mmH_2O$ the injection pressure and the suction pressure by using a dry photoconductor symptoms were dry emulsion on the market as a result, curing properties and adhesion, hardness, solvent resistance and excellent reproduction of fine patterns and ecological stencil technology was available and could be confirmed as a possibility.

A study on the Etching and Dielectric Properties of PZT Thin Films with Excess Pb Contents (Pb 함량에 따른 PZT 박막의 식각 및 유전특성에 관한 연구)

  • Kim, Kyoung-Tae;Lee, Sung-Gap;Kim, Chang-Il;Lee, Young-Hie
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2000.04b
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    • pp.56-59
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    • 2000
  • In this study, Ferroelectric $Pb(Zr_x,Ti_{1-x})O_3$(x=0.53) thin films were fabricated by the spin-coating on the Pt/Ti/$SiO_2$/Si substrate using the PZT metal alkoxide solutions with various excess Pb contents. Etching of PZT film was performed using planar inductively coupled Ar(20)$/Cl_2/BCl_3$ plasma. The etch rate of PZT film was 2450 ${\AA}/min$ at Ar(20)$/BCl_3$(80) gas mixing ratio and substrate temperature of $80^{\circ}C$. The leakage current densities of before etching and after etching PZT thin film were $6.25\times10^{-8}A/cm^2$, $8.74\times10^{-7}A/cm^2$ with electric field of 0.07MV/em, respectively.

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Optical Properties of White Light Sources Using Red, Green, Blue Emitting Phosphors and Violet Light Emitting Diodes (적색, 녹색, 청색 발광 형광체와 보라색 발광 다이오드를 이용한 백색 광원의 광 특성)

  • Kweon, Seok-Soon;Park, Jong-Yun;Huh, Young-Duk
    • Korean Journal of Materials Research
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    • v.16 no.3
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    • pp.145-150
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    • 2006
  • Various colors of light emitting diodes(LED) and four-band white light sources are obtained using a violet LED and various phosphor films. $BaMg_2Al_{16}O_{27}:Eu\;(blue),\;SrGa_2S_4:Eu\;(green),\;and\;Eu(TTA)_3(PTA)$ (red) phosphors are dispersed in poly-vinyl-alcohol aqueous solutions, and phosphor films are prepared by coating the suspensions to PET film. The narrow band emission of $Eu(TTA)_3(PTA)$ phosphor has excellent red luminescent property for four-band white light excited by the violet LED.